Synthesis

Category: psp

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Issue 23/2019

Zilate, Bouthayna; Fischer, Christian; Schneider, Lukas; Sparr, Christof: Scalable Synthesis of Acridinium Catalysts for Photoredox Deuterations
https://www.thieme-connect.de/media/synthesis/201923/i_t0475_ga_10-1055_s-0039-1690694.gif

Issue 20/2019

Ashida, Yuya; Kondo, Shoichi; Arashiba, Kazuya; Kikuchi, Takamasa; Nakajima, Kazunari; Kakimoto, Seizo; Nishibayashi, Yoshiaki: A Practical Synthesis of Ammonia from Nitrogen Gas, Samarium Diiodide and Water Catalyzed by a Molybdenum–PCP Pincer Complex
https://www.thieme-connect.de/media/synthesis/201920/i_f0353_ga_10-1055_s-0039-1690151.gif

Issue 17/2019

Issue 16/2019

Issue 15/2019

Issue 13/2019

Yin, Lingfeng; Mao, Yongjun; Liu, Yaowei; Bu, Lehao; Zhang, Long; Chen, Wenxin: New Synthetic Route to Tucatinib
https://www.thieme-connect.de/media/synthesis/201913/i_h0022_ga_10-1055_s-0037-1610706.gif

Issue 12/2019

Rouzier, Florian; Sillé, Rosanne; Nourry, Arnaud; Tessier, Arnaud; Pipelier, Muriel; Guillarme, Stéphane: Practical Gram-Scale Synthesis of Either α- or β-Anomer of C-Vinyl Glycosides
https://www.thieme-connect.de/media/synthesis/201912/i_z0104_ga_10-1055_s-0037-1611800.gif

Issue 07/2019

Nakura, Ryo; Inoue, Kazuki; Okano, Kentaro; Mori, Atsunori: Practical Synthesis of Precursors of Cyclohexyne and 1,2-Cyclohexadiene
https://www.thieme-connect.de/media/synthesis/201907/i_f0697_ga_10-1055_s-0037-1610356.gif

Issue 04/2019

Morales-Chamorro, Maricela; Vázquez, Alfredo: A Facile Synthesis of N-Boc-azocan-5-one
https://www.thieme-connect.de/media/synthesis/201904/i_m0548_ga_10-1055_s-0037-1611018.gif

Issue 02/2019

Shirinian, Valerii Z.; Lonshakov, Ilya A.; Zakharov, Alexey V.; Lvov, Andrey G.; Krayushkin, Mikhail M.: Practical Deoxygenation of Oxazole N-Oxides by PCl3/Collidine
https://www.thieme-connect.de/media/synthesis/201902/i_z0479_ga_10-1055_s-0037-1610278.gif

Issue 23/2018

Issue 17/2018

Olmos, Andrea; Pereira, Ana; Belderrain, Tomás R.; Pérez, Pedro J.: Multigram Synthesis of Thallium Trispyrazolylborate Compounds
https://www.thieme-connect.de/media/synthesis/201817/i_z0273_ga_10-1055_s-0037-1610106.gif
Fearraigh, Martin P. Ó; Matlock, Johnathan V.; Illa, Ona; McGarrigle, Eoghan M.; Aggarwal, Varinder K.: Synthesis of Isothiocineole and Application in Multigram-Scale Sulfur Ylide Mediated Asymmetric Epoxidation and Aziridination
https://www.thieme-connect.de/media/synthesis/201817/i_z0422_ga_10-1055_s-0037-1609580.gif

Issue 09/2018

Khan, Imran; Luo, Zhi-Bin; Valeru, Anil; Xu, Yin; Liu, Bin; Sangepu, Bhavanarushi; Xie, Ji-Min: Dihydroxylation of Olefins with Potassium Permanganate Catalyzed­ by Imidazolium Salt
https://www.thieme-connect.de/media/synthesis/201809/i_h0825_ga_10-1055_s-0036-1591763.gif

Issue 08/2018

Issue 05/2018

Matoba, Kazutaka; Eizawa, Aya; Nishimura, Shunsuke; Arashiba, Kazuya; Nakajima, Kazunari; Nishibayashi, Yoshiaki: Practical Synthesis of a PCP-Type Pincer Ligand and Its Metal Complexes­
https://www.thieme-connect.de/media/synthesis/201805/i_f0710_ga_10-1055_s-0036-1589153.gif

Issue 04/2018

Plevová, Kristína; Mudráková, Brigita; Šebesta, Radovan: A Practical Three-Step Synthesis of Vinylferrocene
https://www.thieme-connect.de/media/synthesis/201804/i_t0640_ga_10-1055_s-0036-1589142.gif

Issue 02/2018

Issue 24/2017

Hamper, Bruce C.; Sullivan, Brendan T.; Rath, Nigam P.; Spilling, Christopher D.: A Practical Gram-Scale Synthesis of Acrylohydroxamic Acid
https://www.thieme-connect.de/media/synthesis/201724/i_m0463_ga_10-1055_s-0036-1589103.gif

Issue 18/2017

Weiberth, Franz J.; Bourque, Andre J.; Elenbaas, Steven; Hanna, Reda; Powers, Matthew R.; Siegel, Craig S.; Zhao, Jin: Scalable Syntheses of Chirally Pure Mono-protected and Orthogonally Di-protected cis-3,4-Diaminotetrahydrofurans
https://www.thieme-connect.de/media/synthesis/201718/i_m0298_ga_10-1055_s-0036-1588459.gif

Issue 14/2017

Kotthaus, Andreas F.; Ballaschk, Frederic; Stakaj, Vjoni; Mohr, Fabian; Kirsch, Stefan F.: Synthesis and Resolution of a Chiral Diamine: 2,2′-(Propane-2,2-diyl)dipyrrolidine
https://www.thieme-connect.de/media/synthesis/201714/i_z0188_ga_10-1055_s-0036-1589023.gif

Issue 13/2017

Denmark, Scott E.; Chi, Hyung Min: Synthesis of 2-Alkenyl-Tethered Anilines
https://www.thieme-connect.de/media/synthesis/201713/i_n0071_ga_10-1055_s-0036-1589002.gif

Issue 11/2017

van der Haas, Richard N. S.; Dekker, Jeroen A.; Hassfeld, Jorma; Hager, Anastasia; Fey, Peter; Rubenbauer, Philipp; Damen, Eric: Synthesis and Properties of 2-Oxa-6-azaspiro[3.3]heptane Sulfonate Salts
https://www.thieme-connect.de/media/synthesis/201711/i_t0855_ga_10-1055_s-0036-1588733.gif

Issue 09/2017

De Angelis, Sonia; Celestini, Paolo; Rebuzzini, Gabriele; Degennaro, Leonardo; Luisi, Renzo: A Practical 11B NMR Evaluation of BH3 Titer in Commercial Solutions
https://www.thieme-connect.de/media/synthesis/201709/i_z0873_ga_10-1055_s-0036-1588710.gif

Issue 03/2017

Issue 21/2016

Luo, Zhi-bin; Zhao, Chen; Xie, Jimin; Lu, Hong-fei: An Efficient and Practical Method for Olefin Dihydroxylation
https://www.thieme-connect.de/media/synthesis/201621/i_h0270_ga_10-1055_s-0035-1562783.gif

Issue 20/2016

Godeau, Julien; Martinet, Anthony; Levacher, Vincent; Fruit, Corinne; Besson, Thierry: Efficient Microwave-Assisted Synthesis of Methyl 4- or 5-Nitro­anthranilate
https://www.thieme-connect.de/media/synthesis/201620/i_z0369_ga_10-1055_s-0035-1562484.gif

Issue 18/2016

Issue 14/2016

Issue 13/2016

Castillo-Rangel, Norma; Pérez-Díaz, José Oscar H.; Vázquez, Alfredo: An Expeditious Synthesis of 8-Methoxy-1-tetralone
https://www.thieme-connect.de/media/synthesis/201613/i_m0117_ga_10-1055_s-0035-1561601.gif

Issue 11/2016

Issue 09/2016

Mao, Yongjun; Zhu, Chunping; Zhu, Guoqing; Wang, Han; Ren, Xinfeng: Kilogram Synthesis of Crebinostat
https://www.thieme-connect.de/media/synthesis/201609/i_f0094_ga_10-1055_s-0035-1561917.gif

Issue 08/2016

Herrera, Alberto; Linden, Anthony; Heinemann, Frank W.; Brachvogel, René-Chris; von Delius, Max; Dorta, Romano: Optimized Syntheses of Optically Pure P-Alkene Ligands: Crystal Structures of a Pair of P-Stereogenic Diastereomers
https://www.thieme-connect.de/media/synthesis/201608/i_t0045_ga_10-1055_s-0035-1560410.gif

Issue 07/2016

Issue 02/2016

Correia, Henrique D.; Cicolani, Renato S.; Moral, Raphael F.; Demets, Grégoire J. F.: Easy Synthesis of trans-4,5-Dihydroxy-2-imidazolidinone and 2,4-Dimethylglycoluril
https://www.thieme-connect.de/media/synthesis/201602/i_m0510_ga_10-1055_s-0035-1560831.gif

Issue 01/2016

Varjosaari, Sami E.; Suating, Paolo; Adler, Marc J.: One-Pot Synthesis of O-Aryl Carbamates
https://www.thieme-connect.de/media/synthesis/201601/i_m0500_ga_10-1055_s-0035-1560726.gif

Issue 24/2015

Issue 23/2015

Roy, Sudeshna; Sutivisedsak, Nongnuch; Hamper, Bruce C.; Lyss, Alexander M.; Spilling, Christopher D.: A Practical and Scalable Synthesis of (S)- and (R)-1-(Dimethoxyphosphoryl)allyl Methyl Carbonates
https://www.thieme-connect.de/media/synthesis/201523/i_m0469_ga_10-1055_s-0035-1560487.gif

Issue 20/2015

Mao, Yongjun; Zhu, Chunping; Kong, Ziyang; Wang, Jiao; Zhu, Guoqing; Ren, Xinfeng: New Synthetic Process for Bosutinib
https://www.thieme-connect.de/media/synthesis/201520/i_f0453_ga_10-1055_s-0035-1560471.gif

Issue 18/2015

Issue 17/2015

Lei, Xiangyang; Jalla, Anusha; Abou Shama, Mhd A.; Stafford, Jamie M.; Cao, Billy: Chromatography-Free and Eco-Friendly Synthesis of Aryl Tosylates and Mesylates
https://www.thieme-connect.de/media/synthesis/201517/i_m0308_ga_10-1055_s-0034-1378867.gif

Issue 15/2015

Issue 14/2015

Marelli, Enrico; Fernández Salas, José A.; Nolan, Steven P.: Synthesis of an Intermediate of Nafoxidine via Nickel-Catalyzed Ketone Arylation
https://www.thieme-connect.de/media/synthesis/201514/i_t0194_ga_10-1055_s-0034-1380813.gif

Issue 13/2015

Issue 11/2015

Issue 10/2015

Mao, Yongjun; Jiang, Luobin; Chen, Tianyun; He, Haijun; Liu, Gang; Wang, Han: A New and Practical Synthesis of Vortioxetine Hydrobromide
https://www.thieme-connect.de/media/synthesis/201510/i_f0054_ga_10-1055_s-0034-1380505.gif

Issue 09/2015

Kurata, Kaoruko; Inoue, Kumiko; Nishimura, Kazuhiko; Hoshiya, Naoyuki; Kawai, Nobuyuki; Uenishi, Junichi: Synthesis of Optically Pure (R)- and (S)-Tetrahydroisoquinoline-1- and -3-Carboxylic Acids
https://www.thieme-connect.de/media/synthesis/201509/i_f0041_ga_10-1055_s-0034-1380289.gif

Issue 08/2015

Molnár, Katalin; Takács, László; Kádár, Mihály; Kardos, Zsuzsanna; Faigl, Ferenc: A Practical Route for the Preparation of Bis(2,2,2-trifluoroethyl) 2-Oxoalkylphosphonates
https://www.thieme-connect.de/media/synthesis/201508/i_z0724_ga_10-1055_s-0034-1380162.gif

Issue 07/2015

Issue 03/2015

Tummatorn, Jumreang; Thongsornkleeb, Charnsak; Ruchirawat, Somsak; Thongaram, Phanida; Kaewmee, Benyapa: Convenient and Direct Azidation of sec-Benzyl Alcohols by Trimethylsilyl Azide with Bismuth(III) Triflate Catalyst
https://www.thieme-connect.de/media/synthesis/201503/i_z0553_ga_10-1055_s-0034-1379967.gif

Issue 01/2015

Daniels, David S. B.; Smith, Siobhan R.; Lebl, Tomas; Shapland, Peter; Smith, Andrew D.: A Scalable, Chromatography-Free Synthesis of Benzotetramisole
https://www.thieme-connect.de/media/synthesis/201501/i_t0523_ga_10-1055_s-0034-1378931.gif