Synfacts

Issue 09 · September 2008

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Synthesis of (±)-Rhazinicine

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Formal Synthesis of (+)-Laurallene

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Formal Synthesis of Fostriecin

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Synthesis of (-)-Pestalotiopsin A

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0901
Synthesis of Spirastrellolide A Methyl Ester

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0902
Synthesis of Salinamide A

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Synthesis of Clausamines A-C

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0904
Synthesis of (±)-Minfiensine

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0905
Synthesis of (±)-Dysibetaine

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0906
Synthesis of (±)-Vibralactone

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0907
Formal Synthesis of Fluvirucinine A₁

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0908
Synthesis of (±)-Desoxyhypnophilin

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0909
Synthesis of (±)-Cylindricine C

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Synthesis of Heterocycles
0911
Pd-Catalyzed Synthesis of 4-Quinolones

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0912
Synthesis of 1,5-Benzothiazepines from Aziridines and 2-Aminothiophenol

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0913
Synthesis of Tetrahydrofurans from Aldehydes and Cyclopropanes
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0914
Synthesis of 5-Alkynylproline Derivatives via Intramolecular Nicholas Reaction

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0915
Mild Complementary Cycloisomerization Reactions to N-Fused Heterocycles

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0916
Synthesis of Pyridines via Rh-Catalyzed Ring Expansion of Isoxazoles

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0917
Pd-Catalyzed Cyclization of Propargylamides to Oxazoles

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0918
Gold-Catalyzed Synthesis of Benzothio-phenes with Chirality Transfer

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0919
Synthesis of 2-Arylpyridines via Stille Coupling-Azaelectrocyclization

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0920
Synthesis of Chiral Tetrahydropyridines via a Three-Component Reaction

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0921
Four-Component Synthesis of 3,4-Dihydro-coumarin Derivatives

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0922
Pd-Catalyzed Cyclization to Form Benzo-pyranones from Enediynes

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0923
Proline-Catalyzed Friedländer Synthesis of Quinolines

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0924
Ag-Catalyzed Synthesis of Pyrazoles from Propargyl N-Sulfonylhydrazones

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Synthesis of Materials and Unnatural Products
0925
Cargo-Filled Nanocapsules

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0926
Perfluorophenyl Polyynes

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0927
Synthetic Double-Stranded Helical Polymers
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0928
Hg^²+-Gated Molecular Switch

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0929
Self-Standing Proton-Conducting Polymer Membrane

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0930
Stitching Alkynes Together in Sequence

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0931
A High-Spin (S = 2) Macrocycle

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0932
Molecular Nanocubes

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0933
Fluorene Macrocycle

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0934
Pentaphenylbenzene Stops Concentration Quenching

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0935
Donor-Acceptor Quateraryls: A Solution for the OLED Blues

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0936
Domino Friedel-Crafts Cyclization for Helicene Synthesis

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0937
Stacked Paracyclophanes

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
0939
Synthesis of Substituted Enol Ethers and Their Synthetic Application
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0940
Rhodium-Catalyzed Double [2+2+2] Cycloaddition

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0941
New Ligand for Asymmetric Catalytic Hydrogenation of Alkenes

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0942
Palladium-Catalyzed Asymmetric Decarboxylative [4+2] Cycloaddition

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0943
Synthetic Application of Asymmetric [3+2] Cycloaddition

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0944
Asymmetric Cotrimerization Leading to Furylcyclopropanes

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0945
Stereocontrolled Thermal Pericyclic Cascade Rearrangement

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0946
Michael Reaction of Keto Esters with Camphor-Derived Acrylate

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0947
Asymmetric Transfer Hydrogenation in Aqueous Media of Acetophenone

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0948
Rh-Catalyzed Enantioselective Addition of Arylboronic Acids to Aliphatic Imines

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0949
An Improved Lanthanum Catalyst System for Asymmetric Amination

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0950
Enantioselective Sc(III)-Catalyzed Direct Allylation of Aldimines

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0951
Synthesis of Substituted Tetrahydrofurans by [3+2] Cycloadditions

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0952
Nickel-Catalyzed Stereoselective Synthesis of Z-Enol Silanes

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0953
Cu-Catalyzed Tandem Friedel-Crafts/Henry Reaction

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0954
Rh-Catalyzed [2+2+2] Cycloaddition of
1,6-Diynes

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0955
Chiral Spiroborate-Catalyzed Borane Reduction of Ketoxime Ethers

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0956
Palladium-Catalyzed Asymmetric Baeyer-Villiger Oxidation

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0957
Enantioselective Iridium-Catalyzed Carbonyl Allylations with Allyl Acetate

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0958
Enantioselective Reduction of Biaryl Lactones via DKR

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0959
Mild Lewis Acid Catalyzed Ring Opening of Nitro-Cyclopropanes

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0960
Enantioselective Pd-Catalyzed Allylation of Fluorinated Allyl Enol Carbonates

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0961
Self-Assembled Bifunctional Catalyst for the Hydrophosphonylation of Aldehydes

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0962
Enantioselective Zn-Catalyzed Alkynylation of N-Sulfonyl Aldimines

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0963
Enantioselective Conjugate Allylation of Activated a,b-Enones

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0964
Pincer-type Ligands for Enantioselective Catalysis

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0965
Improved Cr-Catalyzed Enantioselective Allylation of Aldehydes

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0966
Diastereoselective Cyclopropanation of Alkenes with α-Alkyl-α-diazoesters

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0967
Enantioselective Arylzinc Addition to Aldehydes

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Metal-Mediated Synthesis
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Highly Diastereoselective Ni-Catalyzed Reductive Aldol Cyclizations

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0970
Pt-Catalyzed Addition of Arylboronic Acids to Aldehydes and Enals

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Negishi Cross-Couplings of Unprotected Phenols, Anilines, and Alcohols
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0972
Co-Catalyzed Cyclooctatriene Synthesis by [4+2+2] Cycloaddition

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Direct Cu(II)-Catalyzed Arylation of Indoles: Switchable Regioselectivity

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1,3-Diketones via Rh-Catalyzed Reductive Acylation of Enones

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Mild Transesterification of Methyl Esters Catalyzed by a Zinc Cluster

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0976
Directed Remote Metalation via N-Carbamoyl N Æ C Translocation

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0977
Pd-Catalyzed ortho Halogenation of C-H Bonds

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0978
Cu(II)-Catalyzed Synthesis of Alkylcyclo-pentanes from CpMgBr

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0979
Ni- and Pd-Catalyzed Organozinc Coupling with CO₂

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0980
Fe-Catalyzed Cross-Coupling of Dienol Phosphates with Grignard Reagents

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0981
1,2-Rearrangement of α,α-Disubstituted α-Siloxy Aldehydes: Switchable Regioselectivity

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0982
Benzene Synthesis by Mn-Catalyzed Dehydrative [2+2+2] Coupling

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0983
Cross-Alkyne Cyclotrimerization Using Liquid Enol Ethers and Acetates

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Organo- and Biocatalysis
0985
Combining Two Organocatalysts in One

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0986
Selective Formation of 1 out of 64 Stereoisomers

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0987
Organocatalytic Asymmetric Claisen Rearrangement
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0988
Highly anti-Selective Asymmetric Nitro-Mannich Reactions

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0989
Organo- and Metal Catalysis Complement Each Other

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0990
Truncated Cinchona Alkaloids

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0991
A New Chiral Brønsted Acid Catalyst

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0992
Catalytic Asymmetric Isoindoline Synthesis

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0993
Enantioselective Protonation

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0994
Enantioselective, Brønsted Acid Catalyzed Reaction Cascade

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Polymer-Supported Synthesis
0995
Recyclable Au Nanoparticle Supported Palladium(II) Catalyst
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0996
Aldol-Type Coupling of Ethyl Diazoacetate with SiO₂-TMG

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0997
Preparation of a,b-Unsaturated Ketones from Alkynes and Aldehydes

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0998
Hydrogen-Transfer Amination of Aldehydes

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0999
Sonogashira Reaction Catalyzed by Cobalt Hollow Nanospheres

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1000
Incorporation of CO₂ into Oxazolidinones with PEG-Supported Catalyst

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1001
Heterogeneous Asymmetric Reduction of Ketimines with Trichlorosilane

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1002
Umpolung Reaction via Polymer-Supported Dithianes

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1003
Preparation of b-Keto Esters Using Mesoporous Silica Catalyst

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1004
Heteropoly Acid Catalyzed Alkylation of
1,3-Dicarbonyl Compounds

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1005
Oxidation of Alcohols Catalyzed by Au(0)-Pd(0)/PI Membrane

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1006
Palladium/Lipase-Catalyzed Asymmetric Reductive Acylation of Ketoximes

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1007
Silica-Supported Alkyne Metathesis Catalyst: Synthetic Application

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1008
Synthesis of b-Arylpropanoates and Cinnamaldehydes

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