Synfacts

Issue 08 · August 2007

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A25
SYNFORM ISSUE 2007/03
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Synthesis of Natural Products and Potential Drugs
0781
Synthesis of Papulacandin D
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0782
Synthesis of (-)-Hennoxazole A

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0783
Synthesis of Spirotenuipesine A

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0784
Synthesis of (6E)-2′-O-Methylmyxalamide D

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0785
Synthesis of (-)-Alstonerine

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0786
Synthesis of (+)-ξ-Clausenamide and(-)-Balasubramide

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0787
Formal Synthesis of Biotin

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0788
Synthesis of (±)-Polygalolides A and B

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0789
Synthesis of (-)-Belactosin C

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0790
Synthesis of Jerangolid D

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0791
Synthesis of (+)-Lyconadin A

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0792
Synthesis of Attenol B

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0793
Synthesis of (±)-Marcfortine B

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0794
Total Synthesis of Paecilomycine A

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0795
Synthesis of UCS 1025A

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Synthesis of Heterocycles
0797
Synthesis of N-Arylimidazoles by Catalytic Cross-Cycloaddition of Isocyanides

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0798
Palladium-Catalyzed Cyanation of Aryl and Heteroaryl Chlorides

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PDF (72 kb)
0799
Synthesis of Furans, Pyrroles and Thiophenes Using Ynolate Building Blocks

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0800
Cu-Mediated Synthesis of Pyrazoles via 1,3-Dipolar Cycloaddition

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0801
Asymmetric, exo-Selective Synthesis of trans-4,5-Disubstituted Pyrrolidines

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0802
Selective Amination of Trihalopyridines

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0803
Direct Pd-Catalyzed Arylation of Triazoles

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0804
Synthesis of Isoquinolines via 1,3-Dipolar Cycloaddition-Heck Coupling

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0805
Synthesis of 2-Aminopyridines and 2-Amino-Quinolines from Their N-Oxides

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PDF (73 kb)
0806
Rh-Catalyzed C-H Activation Route to 2-Alkylpyridines and 2-Alkylquinolines

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0807
Regioselective Synthesis of Functionalized 3-Hydroxypyridines

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0808
Symmetric 3,4-Disubstituted Pyrroles via Piloty-Robinson Synthesis

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0809
Microwave-Assisted Biginelli Synthesis of Dihydropyrimidine-2-ones

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0810
One-Pot Synthesis of Substituted 2-Aminobenzo[b]thiophenes

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Synthesis of Materials and Unnatural Products
0811
Triptycene-Based Macrocycles

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0812
Helical Polymers via Asymmetric Coordination Polymerization

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0813
Carbomer of Benzene - A Tour de Force
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0814
Tetracene Sulfoxides and Sulfones via a Cascade Cyclization

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0815
Template Synthesis of a 90-Membered Macrocycle

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PDF (80 kb)
0816
Peryleneimide-Fused Polythiophene

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PDF (66 kb)
0817
A Molecular Basket with a Silver Lock

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0818
Efficient Synthesis of Dendrimers via A Chemoselective Approach

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0819
Conjugated Polymers Formed via Bergman Cyclopolymerization

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0820
Replication of A Single-Stranded Polynorbornene

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0821
Low-Band-Gap Bowls

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
0823
Titanium-Mediated Olefin Epoxidation Using Hydrogen Peroxide

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0824
Enantioselective Ru(II)-Catalyzed Hydrogenation of Ketones

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0825
Copper-Catalyzed Allylic Alkylations for the Synthesis of Chiral Allylsilanes

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PDF (74 kb)
0826
Desymmetrization of meso-Anhydrides with Organozinc Reagents

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PDF (71 kb)
0827
Enantioselective Carbonyl Ylide Formation/1,3-Dipolar Cycloaddition

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PDF (76 kb)
0828
Enantioselective Conjugate Addition of Indoles to Enones

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PDF (73 kb)
0829
Cycloheptane-1,4-diones by an Asymmetric Ring-Expanding Allylation

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PDF (68 kb)
0830
Highly Enantioselective Hydrogenation of Quinolines

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PDF (67 kb)
0831
Mixed Organobismuth/Dialkylzinc Reagents for Aryl Transfers

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PDF (64 kb)
0832
Enantioselective Rh-Catalyzed Intermolecular Hydroacylation

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PDF (71 kb)
0833
Storable Zirconium Complex for Aldol and Hetero-Diels-Alder Reactions

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PDF (67 kb)
0834
[4+2] Carbocyclization of Vinylarylaldehydes with Alkenes and Alkynes

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PDF (70 kb)
0835
Domino Asymmetric Ring-Opening/Cross Metathesis Reaction

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PDF (72 kb)
0836
Cyclopropanation: Silver-Catalyzed Reactions of Aryldiazoacetates

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PDF (67 kb)
0837
Au-Catalyzed Diastereoselective [3+2] Cycloaddition
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PDF (98 kb)
0838
Synthesis of Chiral syn-α-Substituted β-Amino Ketones

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0839
Palladium-Mediated Synthesis of α-Vinylstannanes

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PDF (98 kb)
0840
Ortho-Substituted Axially Chiral Biaryl Phosphorus Compounds

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PDF (67 kb)
0841
Stereoselective Synthesis of 1,3-Enynes from Diiodoalkenes

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PDF (73 kb)
0842
Reduction of Nitroalkene Isomers by Base-Induced Equilibration

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PDF (68 kb)
0843
Quaternary Centers Formation via Alkene Isomerization/Claisen Rearrangement

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PDF (71 kb)
0844
Stereo- and Regioselective Silylation of Alkenes Using Silacyclobutanes

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PDF (67 kb)
0845
Catalytic Desymmetrization of 1,4-Cyclohexadienyltriisopropoxysilane

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PDF (80 kb)
0846
Ni-Catalyzed Cycloaddition of Nitrones and Cyclopropanes

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PDF (66 kb)
0847
Tetrahydropentalene Ligands for Rh-Catalyzed Arylation of Arylimines

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PDF (68 kb)
0848
Calcium Complexes as Brønsted Base Catalysts for Conjugate Additions

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0849
Enantioselective Synthesis of Propargylic Alcohols

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Metal-Mediated Synthesis
0851
Iron-Catalyzed Alkylations of Aromatic Grignard Reagents
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0852
Novel Cobalt-Catalyzed Hydrocyanation of Olefins

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0853
Fe(III)-Catalyzed Friedel-Crafts-Type Alkenylation with Aryl-Substituted Alkynes

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0854
Stereoselectivity in Cross-Coupling of α-Bromo Sulfoxides and Arylboronic Acids

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0855
Efficient Reagents for Non-Cryogenic Br-Li Exchange in Bromopyridines

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0856
First Catalytic Functionalization of Unreactive Aryl C-N Bonds in Anilines

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0857
Magnesiation of Electron-Rich Aryl Bromides and Cross-Coupling Reactions

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0858
Fe(II)-Catalyzed sp³-sp³ Cross-Coupling Reactions

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0859
Coupling Reactions of Cyclic Thioamides and Thioureas with Arylboronic Acids

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0860
MPBH: A New Easily Accessible Borane for the Hydroboration of Alkynes

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0861
Direct Amidocyclopropanation of Alkenes Using Organozinc Carbenoids

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0862
Synthesis of (E)-α,β-Unsaturated Esters from 2,2-Dichloroesters and Aldehydes

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0863
Reactions of Epoxides with LiTMP and Organolithium or Grignard Reagents

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0864
Synthesis of Conjugated Enynes and Substituted Indoles from 1-Alkynes

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Organo- and Biocatalysis
0865
Enzymatic Asymmetric Isomerization of α- to β-Amino Acids
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0866
Asymmetric Organocatalytic Cyclopropanation of Enals

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PDF (69 kb)
0867
Application of an Enantioselective Benzoin Cyclization: Synthesis of (+)-Sappanone B

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PDF (70 kb)
0868
Concise Synthesis of Vinyl Glycines

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PDF (79 kb)
0869
Organocatalytic Reaction Cascade

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PDF (73 kb)
0870
Organocatalytic Friedel-Crafts Reactions of Naphthols and Nitroolefins

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PDF (71 kb)
0871
Organocatalytic Asymmetric Tandem Michael-Henry Reaction

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PDF (77 kb)
0872
Neutral π-Nucleophile Catalyzed Cyanation of Aldehydes and Ketones

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PDF (63 kb)
0873
Enantioselective [3+2] Cycloaddition of Azomethine Ylides and α,β-Unsaturated Aldehydes

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PDF (70 kb)
0874
Asymmetric α-Arylation of Aldehydes

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PDF (70 kb)
0875
Yet Another Direct Aldol Reaction in Water

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PDF (65 kb)
0876
Enzyme Catalysis towards Optically Pure β-Hydroxy Nitriles

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PDF (75 kb)
0877
Enantioselective α-Enolation of Aldehydes by SOMO Activation

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PDF (74 kb)
Polymer-Supported Synthesis
0879
Asymmetric Synthesis of Propargyl Amines with Immobilized Cu(Pybox) Complexes

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PDF (87 kb)
0880
Neoglycopeptide Dendrimer Library for Lectin Binding

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PDF (80 kb)
0881
Non-Kolbe Electrolysis Using Solid-Supported Bases

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PDF (86 kb)
0882
p-Nitromandelic Acid Linked Peptide Synthesis

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PDF (94 kb)
0883
PS-Supported Palladium-Phosphine Complexes

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PDF (72 kb)
0884
C2-Aryl-PDB Library

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PDF (69 kb)
0885
Solid-Phase Synthesis of Glu⁷-Phalloidin

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PDF (84 kb)
0886
N-Acyl Sulfonamide Linker for Peptide Synthesis

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PDF (86 kb)
0887
3-Methyl-1-p-Tolyltriazene: A Novel Methyl Esterification Agent

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PDF (63 kb)
0888
Catalytic Pauson-Khand Reaction Using PEG-Stabilized Cobalt Nanoparticles

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PDF (65 kb)
0889
Xerogel-Supported Alcohol Dehydrogenase for Asymmetric Reduction

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PDF (66 kb)
0890
Solid-Phase Synthesis of Thiophenes

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0891
Silica-Supported Acidic Ionic Liquid

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