Synlett

Issue 10 · June 2017

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synpacts
1121
Sasaki, Kaname; Hashimoto, Yusuke:
2,6-Lactones as a New Entry in Stereoselective Glycosylations

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1127
Heinze, Robert C.; Heretsch, Philipp:
Synthesis of Secosterols as an Arena for C–H Functionalization and C–C Manipulation Tactics

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PDF (1549 kb)
account
1134
Chen, Lei; Chen, Fen-Er:
Total Synthesis of Camptothecins: An Update

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PDF (547 kb)
1151
Singh, Priyanka; Guo, Qi; Kohen, Amnon:
Chemoenzymatic Synthesis of Ubiquitous Biological Redox Cofactors

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PDF (1164 kb)
letter
1160
Jebli, Nejib; Debrouwer, Wouter; Berton, Jan K. E. T.; Van Hecke, Kristof; Stevens, Christian V.; Touil, Soufiane:
Direct Regio- and Diastereoselective Diphosphonylation of Cyclic Enamines: One-Pot Synthesis of α,α′-Bis(diphenylphosphoryl)- and α,α′-Bis(diphenylphosphorothioyl)cycloalkanones

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1165
Bakulina, Olga; Dar’in, Dmitry; Krasavin, Mikhail:
o-Phenylenediacetic Acid Anhydride in the Castagnoli–Cushman Reaction: Extending the Product Space to ε-Lactams

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1170
Williamson, Jill B.; Smith, Emily R.; Scheerer, Jonathan R.:
A Merged Aldol Condensation, Alkene Isomerization, Cycloaddition/Cycloreversion Sequence Employing Oxazinone Intermediates for the Synthesis of Substituted Pyridines

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PDF (151 kb)

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1173
Baghery, Saeed; Zolfigol, Mohammad Ali; Schirhagl, Romana; Hasani, Masoumeh:
Application of Triphenylammonium Tricyanomethanide as an Efficient and Recyclable Nanostructured Molten-Salt Catalyst for the Synthesis of N-Benzylidene-2-arylimidazo[1,2-a]pyridin-3-amines

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PDF (513 kb)

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1177
Borah, Raju Kumar; Raul, Prasanta Kumar; Mahanta, Abhijit; Shchukarev, Andrey; Mikkola, Jyri-Pekka; Thakur, Ashim Jyoti:
Copper Oxide Nanoparticles as a Mild and Efficient Catalyst for N-Arylation of Imidazole and Aniline with Boronic Acids at Room Temperature

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PDF (1432 kb)

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1183
Obara, Nobuhiro; Watanabe, Takeshi; Asakawa, Tomohiro; Kan, Toshiyuki; Tanaka, Takao:
Efficient Synthesis of 3-Amino-1,5-benzodiazepine-2-one Derivatives

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PDF (154 kb)

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Supporting Information (PDF)
1187
Tang, Xiaohang; Tong, Le; Yao, Mengyi; Liang, Qiaoli; Wang, Xiaolong; Yu, Haitao:
A New Process for the Total Synthesis of Sparstolonin B

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Primary Data
Primary Data (ZIP)
1191
Huang, Hua-Hsuan; Chen, Yu-Feng; Niu, Guang-Hao; Chuang, Gary J.:
Photoinduced Reduction of Nitrobenzenes to Primary Aromatic Amines

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1195
Zhang, Rongxing; Yan, Zhaohua; Wang, Dingyi; Wang, Yuanxing; Lin, Sen:
NaI-Mediated Acetamidosulfenylation of Alkenes with Bunte Salts as Thiolating Reagent Leading to β-Acetamido Sulfides

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PDF (197 kb)

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Supporting Information (PDF)
1201
Chen, Yanyu; Peng, Qiujun; Zhang, Rong; Hu, Jian; Zhou, Yijun; Xu, Lanting; Pan, Xianhua:
Ligand-Controlled Chemoselective One-Pot Synthesis of Dibenzothiazepinones and Dibenzoxazepinones via Twice Copper-Catalyzed Cross-Coupling

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PDF (206 kb)

Supplementary Material

Supporting Information (PDF)

CIF File (OTHER)

Primary Data
Primary Data (ZIP)
1209
Mäkinen, Mari Ella; Mallik, Rosy; Siitonen, Juha H.; Kärki, Katja; Pihko, Petri M.:
Towards Waltheriones C and D: Synthesis of the Oxabicyclic Core

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1214
Ramezanpour, Sorour; Bigdeli, Zahra; Alavijeh, Nahid S.; Rominger, Frank:
Application of Saccharin as an Acidic Partner in the Ugi Reaction for the One-Pot Synthesis of 3-Iminosaccharins

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PDF (300 kb)

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Supporting Information (PDF)
1219
Bouchez, Laure C.; Gerbeaux, Cyril; Rusch, Marion; Patoor, Maude; Livendahl, Madeleine; Press, Neil J.:
‘Wake-Up Call of A Sleeping Beauty’: Straightforward Synthesis of Functionalized β-(2-Pyridyl) Ketones from 2,6-Lutidine

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PDF (202 kb)

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1224
Rahmani, Fariba; Darehkordi, Ali:
Synthesis of Trifluoromethylated Pyrroles via a One-Pot Three-Component Reaction

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PDF (143 kb)

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Supporting Information (PDF)
1227
Yang, Jingya; Li, Tianyuan; Zhou, Hongyan; Li, Nana; Xie, Dongtai; Li, Zheng:
Potassium Hydroxide Catalysed Intermolecular Aza-Michael Addition of 3-Cyanoindole to Aromatic Enones

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PDF (785 kb)

Supplementary Material

Supporting Information (PDF)
1232
Zhao, Jun-Long; Chen, Xiang-Xiang; Xie, Hu; Ren, Jiang-Tao; Gou, Xiao-Feng; Sun, Meng:
Palladium-Catalyzed Highly Regioselective ortho-Halogenation of 2-Pyridyl Sulfoxides

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PDF (192 kb)

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errata
e5
Heinze, Robert C.; Heretsch, Philipp:
Synthesis of Secosterols as an Arena for C–H Functionalization and C–C Manipulation Tactics
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Synlett

2,6-Lactones as a New Entry in Stereoselective Glycosylations

Synthesis of Secosterols as an Arena for C–H Functionalization and C–C Manipulation Tactics

Total Synthesis of Camptothecins: An Update

Chemoenzymatic Synthesis of Ubiquitous Biological Redox Cofactors

Direct Regio- and Diastereoselective Diphosphonylation of Cyclic Enamines: One-Pot Synthesis of α,α′-Bis(diphenylphosphoryl)- and α,α′-Bis(diphenylphosphorothioyl)cycloalkanones

o-Phenylenediacetic Acid Anhydride in the Castagnoli–Cushman Reaction: Extending the Product Space to ε-Lactams

A Merged Aldol Condensation, Alkene Isomerization, Cycloaddition/Cycloreversion Sequence Employing Oxazinone Intermediates for the Synthesis of Substituted Pyridines

Application of Triphenylammonium Tricyanomethanide as an Efficient and Recyclable Nanostructured Molten-Salt Catalyst for the Synthesis of N-Benzylidene-2-arylimidazo[1,2-a]pyridin-3-amines

Copper Oxide Nanoparticles as a Mild and Efficient Catalyst for N-Arylation of Imidazole and Aniline with Boronic Acids at Room Temperature

Efficient Synthesis of 3-Amino-1,5-benzodiazepine-2-one Derivatives

A New Process for the Total Synthesis of Sparstolonin B

Photoinduced Reduction of Nitrobenzenes to Primary Aromatic Amines

NaI-Mediated Acetamidosulfenylation of Alkenes with Bunte Salts as Thiolating Reagent Leading to β-Acetamido Sulfides

Ligand-Controlled Chemoselective One-Pot Synthesis of Dibenzothiazepinones and Dibenzoxazepinones via Twice Copper-Catalyzed Cross-Coupling

Towards Waltheriones C and D: Synthesis of the Oxabicyclic Core

Application of Saccharin as an Acidic Partner in the Ugi Reaction for the One-Pot Synthesis of 3-Iminosaccharins

‘Wake-Up Call of A Sleeping Beauty’: Straightforward Synthesis of Functionalized β-(2-Pyridyl) Ketones from 2,6-Lutidine

Synthesis of Trifluoromethylated Pyrroles via a One-Pot Three-Component Reaction

Potassium Hydroxide Catalysed Intermolecular Aza-Michael Addition of 3-Cyanoindole to Aromatic Enones

Palladium-Catalyzed Highly Regioselective ortho-Halogenation of 2-Pyridyl Sulfoxides

Synthesis of Secosterols as an Arena for C–H Functionalization and C–C Manipulation Tactics