DOI: 10.1055/s-00000083

Synlett

eFirst

Publication Date: 06 February 2026

Letter

  • Genova, Jason; Cabrera Allpas, Rodrigo; Nicewicz, David A.; ter Horst, Marc:

    A J-resolved 13C–19F {1H, 19F} Experiment with Broadband Fluorine Decoupling for the Characterization of Polyfluorinated Organic Compounds

    Image for article: A <i>J</i>-resolved <sup>13</sup>C–<sup>19</sup>F {<sup>1</sup>H, <sup>19</sup>F} Experiment with Broadband Fluorine Decoupling for the Characterization of Polyfluorinated Organic Compounds
    Supplementary Material (PDF)

    • Letter

  • Li, Chunfeng; Pan, Chenhong; Liu, Bin; Shen, Chunwei; Zhang, Xingxian:

    Ruthenium-catalyzed C–H Sulfonamidation of 4-Aryl-7H-pyrrolo[2,3-d] pyrimidine with Sulfonyl Azides Under Aerobic Atmosphere

    Image for article: Ruthenium-catalyzed C–H Sulfonamidation of 4-Aryl-7H-pyrrolo[2,3-d] pyrimidine with Sulfonyl Azides Under Aerobic Atmosphere

    • Letter

  • Romero, Daisy C.; Tapia, Ruben; Botana, Enrique; Martinez Cuezva, Alberto; Alajarin, Mateo; Wagen, Corin; Wagen, Arien; Villalgordo, Jose M.:

    A Practical and Efficient Asymmetric Synthesis of the Tobacco Natural Alkaloids (S)-Anatabine and (S)-Anabasine via an Allylation/Metathesis-based Approach

    Image for article: A Practical and Efficient Asymmetric Synthesis of the Tobacco Natural Alkaloids (S)-Anatabine and (S)-Anabasine via an Allylation/Metathesis-based Approach
    Supplementary Material (PDF)

    • Publication Date: 05 February 2026

    Account

  • Diaz, Jordan; Chan, Philip Wai Hong:

    Site-Selective Copper-Catalyzed Halogenation at an Unactivated C(sp3)–H Bond: Mechanistic Insights and Advances

    Image for article: Site-Selective Copper-Catalyzed Halogenation at an Unactivated C(sp<sup>3</sup>)–H Bond: Mechanistic Insights and Advances

    • Letter > Published as part of the Special Section 16th EuCheMS Organic Division Young Investigator Workshop

  • Song, Kun-Long; Pilet, Guillaume; Medebielle, Maurice; Merad, Jérémy:

    Dication Diselenides as Reservoirs of Open-Shell Catalysts in Covalent Radical Catalysis

    Image for article: Dication Diselenides as Reservoirs of Open-Shell Catalysts in Covalent Radical Catalysis
    Supplementary Material (PDF)

    • Perspectives > Published as part of the Special Section 16th EuCheMS Organic Division Young Investigator Workshop

  • Tran, Tu Anh; Dai, Chaodi; Day, Craig S.:

    Carbon Dioxide-Derived Materials

    Image for article: Carbon Dioxide-Derived Materials

    • Synpacts

  • Lin, Jiaxin; Quan, Yangjian:

    A Formal Aldehydic C–H Borylation

    Image for article: A Formal Aldehydic C–H Borylation

    • Publication Date: 03 February 2026

    Letter > Alkynes in Organic Synthesis

  • Gupta, Vanshika; Rana, Tamanna; Das, Arnab; Pawar, Amit B.:

    Cp*Co(III)-Catalyzed Regioselective Redox-Neutral Synthesis of 3-Alkenylated Isoquinolones from N-Chlorobenzamides with 1,3-Diynes at Room Temperature

    Image for article: Cp*Co(III)-Catalyzed Regioselective Redox-Neutral Synthesis of 3-Alkenylated Isoquinolones from <i>N</i>-Chlorobenzamides with 1,3-Diynes at Room Temperature
    Supplementary Material (PDF)

    • Publication Date: 30 January 2026

    Letter

  • Yang, Yong-Qing; Ruan, Wenhua; Lu, Zheng; Li, Xiaoqian; Xu, Ximing:

    The Improved Synthesis of 2-[Dimethylphenylsilyl]ethanol (DMPSE-OH) and Its Utility in Carboxyl Protection

    Image for article: The Improved Synthesis of 2-[Dimethylphenylsilyl]ethanol (DMPSE-OH) and Its Utility in Carboxyl Protection
    Supplementary Material (PDF)

    • Synpacts

  • Lin, Kejun; Zhu, Tingshun:

    N-Heterocyclic Selone-Generated Selenium-Centered Radical for Covalent Radical Catalysis

    Image for article: N-Heterocyclic Selone-Generated Selenium-Centered Radical for Covalent Radical Catalysis

    • Synpacts

  • Shelar, Santosh; Fisch, Kyle; Walczak, Maciej:

    Silicon as a Strategic Element in Carbohydrate Chemistry: Glycomimetic Design, Reductive Migration, and Ring Editing

    Image for article: Silicon as a Strategic Element in Carbohydrate Chemistry: Glycomimetic Design, Reductive Migration, and Ring Editing

    • Publication Date: 29 January 2026

    Letter > Published as part of the Special Section dedicated to Prof. Masakatsu Shibasaki

  • Watanabe, Takayuki; Katsuta, Rina; Higashida, Kosuke; Yoshino, Tatsuhiko; Matsunaga, Shigeki:

    Synthesis of Sulfonyl Fluorides from Tertiary Sulfonamides via N-Methylation Using Me-λ3-Iodane

    Image for article: Synthesis of Sulfonyl Fluorides from Tertiary Sulfonamides via <i>N</i>-Methylation Using Me-λ<sup>3</sup>-Iodane
    Supplementary Material (PDF)

    • Publication Date: 23 January 2026

    Letter > Published as part of the Special Topic Alkynes in Organic Synthesis

  • Uhlmann, Anselm; Guyon, Jacques; Werz, Daniel B.:

    Photochemical Synthesis of 7,14-Dialkynyl-10,11-Dimethyl[5]Helicene via Flow Chemistry and Comparison with its Bromo Analog

    Image for article: Photochemical Synthesis of 7,14-Dialkynyl-10,11-Dimethyl[5]Helicene via Flow Chemistry and Comparison with its Bromo Analog
    Supplementary Material (PDF)

    • Letter

  • Zhang, Xinran; Wei, Yan; Ling, Huilin; Yin, Qikun; Fang, Xianhe:

    The Synthesis of Amides by Photoexcited o-Nitrophenyl Benzyl Ethers and Evaluation of Biological Activity

    Image for article: The Synthesis of Amides by Photoexcited <i>o</i>-Nitrophenyl Benzyl Ethers and Evaluation of Biological Activity
    Supplementary Material (PDF)

    • Synpacts

  • Lu, Hongjian; Cui, Zhangkai:

    Unlocking Tertiary Halides from Primary Alkylamines through Deamination

    Image for article: Unlocking Tertiary Halides from Primary Alkylamines through Deamination

    • Publication Date: 22 January 2026

    Account > Published as part of the Special Topic Alkynes in Organic Synthesis

  • Peters, Sven Erik; Xu, Yang; Gerlich, Felix; Ackermann, Lutz:

    Tuning Proton-Electron Synergy for Electrooxidative Alkyne Annulation: Mechanistic Insights and Synthetic Application

    Image for article: Tuning Proton-Electron Synergy for Electrooxidative Alkyne Annulation: Mechanistic Insights and Synthetic Application
    Open Access

    • Publication Date: 20 January 2026

    Account

  • Rajai-Daryasarei, Saideh; Fathi Vavsari, Vaezeh; Jamshidi, Elmira; Balalaie, Saeed:

    Recent Advances in Cyclization Reactions of 1,5-Enynones and 1,6-Enynones

    Image for article: Recent Advances in Cyclization Reactions of 1,5-Enynones and 1,6-Enynones

    • Publication Date: 16 January 2026

    Letter

  • Li, Xiaochen; Sakamoto, Aina; Aranaga, Rinka; Murakami, Suguru; Matsubara, Ryosuke; Hayashi, Masahiko:

    Preparation of Nitrones by Hydrogenation of 2-(2-Nitro-1-phenylethyl)cyclohexanones

    Image for article: Preparation of Nitrones by Hydrogenation of 2-(2-Nitro-1-phenylethyl)cyclohexanones
    Supplementary Material (PDF)

    • Publication Date: 15 January 2026

    Account > Published as part of the Special Issue dedicated to Prof. S. Chandrasekaran on his 80th birthday

  • Sharma, Kumari Swati; Ranjan, Sushil Kumar; Pandey, Ganesh:

    Benzylic C(sp3)–H Functionalization by Photo Redox Catalysis

    Image for article: Benzylic C(sp<sup>3</sup>)–H Functionalization by Photo Redox Catalysis

    • Letter > Published as part of the Special Topic Alkynes in Organic Synthesis

  • Budwitz, Jessica E.; Newton, Christopher G.:

    Stable Vicinal Bisketene Equivalents for Aryne Diels–Alder Reactions

    Image for article: Stable Vicinal Bisketene Equivalents for Aryne Diels–Alder Reactions
    Supplementary Material (PDF)
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