Synthesis

Ausgabe 23 · Dezember 2016

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A175
Zanda, Matteo:
SYNFORM ISSUE 2016/12
FREIER ZUGRIFF

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review
4017
Gao, Yangguang; He, Xianran; Ding, Fei; Zhang, Yongmin:
Recent Progress in Chemical Syntheses of Sphingosines and Phytosphingosines

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short review
4038
Tian, Qingshan; Zhang, Guozhu:
Recent Advances in the Asymmetric Nozaki–Hiyama–Kishi Reaction

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PDF (872 kb)
4050
Moni, Lisa; Banfi, Luca; Riva, Renata; Basso, Andrea:
External-Oxidant-Based Multicomponent Reactions

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4060
Pons, Amandine; Poisson, Thomas; Pannecoucke, Xavier; Charette, André B.; Jubault, Philippe:
Synthesis and Applications of Fluorocyclopropanes

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paper
4072
Ashida, Yuichiro; Sato, Yuka; Honda, Atsushi; Nakatsuji, Hidefumi; Tanabe, Yoo:
A General and Robust Method for the Preparation of (E)- and (Z)-Stereodefined Fully Substituted Enol Tosylates: Promising Cross-Coupling Partners
FREIER ZUGRIFF

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4081
Thiemermann, Jutta; Andrä, Michal Sascha; Schnaubelt, Jürgen; Lentz, Dieter; Zimmer, Reinhold; Reissig, Hans-Ulrich:
A Modular Four-Component Route to Substituted 1,7,9-Decatrien-3-ones Using a Chloro-Substituted Phosphorane as Key C₃ Building Block

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Supporting Information (PDF)
4091
Kaya, Uğur; Mahajan, Suruchi; Schöbel, Jan-Hendrik; Valkonen, Arto; Rissanen, Kari; Enders, Dieter:
Diastereoselective Synthesis of Spiro[pyrazolone-4,3′-tetrahydrothiophenes] via a Sulfa-Michael/Aldol Domino Reaction
Open Access

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PDF (327 kb)

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Supporting Information (PDF)
4099
Uchida, Keisuke; Yoshida, Suguru; Hosoya, Takamitsu:
Controlled Generation of 3-Triflyloxyarynes

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4110
Delgue, Elisa; Brovetto, Margarita; Seoane, Gustavo:
Concise Preparation of the Bis-THF Core of Annonaceous Acetogenins

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Supporting Information (PDF)
4117
Kotali, Antigoni; Maniadaki, Anna; Kotali, Elvira; Harris, Philip A.; Różycka-Sokołowska, Ewa; Bałczewski, Piotr; Joule, John A.:
Synthesis of Bicyclic Boron Heterocycles Containing [1,3,4,2]Oxadiazaborole and [1,3,2]Oxazaborine

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PDF (1005 kb)
4126
Park, Kyung Hyun; Park, Joon Bum; Zong, Kyukwan:
A Convenient Synthesis of Dithieno[3,2-b:2′,3′-d]thiophenes from Thiophene

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PDF (834 kb)
4131
Kwak, Se Hun; Lim, Su-Jeong; Yoo, Hyun-Jeong; Ha, Ji-Eun; Gong, Young-Dae:
Intramolecular Mizoroki–Heck Reaction of 2-Thiosubstituted Acrylates for the Synthesis of 3-Substituted Benzo[b]thiophene-2-carboxylates

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PDF (290 kb)

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Supporting Information (PDF)
4143
Ogiwara, Yohei; Ono, Yuji; Sakai, Norio:
Indium(III) Isopropoxide as a Hydrogen Transfer Catalyst for Conversion of Benzylic Alcohols into Aldehydes or Ketones via Oppenauer Oxidation

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PDF (171 kb)

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4149
Nakao, Michiyasu; Tsuji, Shunsuke; Kitaike, Syuji; Sano, Shigeki:
Synthesis of Erythrochelin: A Hydroxamate-Type Siderophore from Saccharopolyspora erythraea

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Supporting Information (PDF)
4155
Wei, Xu; Lu, Junzhu; Duan, Wei-Liang:
Palladium-Catalyzed Asymmetric 1,6-Addition of Diarylphosphines to Allylidenemalonates for Chiral Phosphine Synthesis

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PDF (184 kb)

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4161
Ren, Jiangmeng; Zhao, Pu; Xiao, Xiong; Chen, Tianqi; Zeng, Bu-Bing:
Synthesis of Typical Isocopalane Diterpenes: ent-Spongian-16-one, ent-Isoagatholactone, and Anisodorin 5

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PDF (192 kb)

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4167
Vempala, Naresh; Venkateswara Rao, Settipalli; Shree, Anireddy Jaya; Pradhan, Braja S.:
An Asymmetric Synthesis of Rosuvastatin Calcium

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4175
Patir, Süleyman; Tezeren, Mustafa A.; Salih, Bekir; Ertürk, Erkan:
Stereoselective Total Synthesis of (±)-Dasycarpidol and (±)-Dasycarpidone

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4181
Bredihhin, Aleksei; Luiga, Sirvo; Vares, Lauri:
Application of 5-Ethoxymethylfurfural (EMF) for the Production of Cyclopentenones

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PDF (198 kb)

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4189
Kröger, Denis; Stalling, Timo; Martens, Jürgen:
The Concept of Sequential Multicomponent Reactions: A Short Synthesis of Thiazolo- and Oxazolo[1,4]benzodiazepine-2,5-diones

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PDF (249 kb)

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4199
Dawra, Nisha; Ram, Ram Nath:
Facile Synthesis of Some Chlorinated and Heteroatom-Rich Monocyclic β-Lactams via the Staudinger Reaction of Acyclic S-Alkylisothioureas

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PDF (303 kb)

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Supporting Information (PDF)
4207
Divya, K. Vijay L.; Meena, A.; Suja, Thachapully D.:
Unified Approach to Pyrazole-Fused Heterocyclic and Carbocyclic Motifs through One-Pot Condensation and Intramolecular Dipolar Cycloaddition Reaction

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PDF (178 kb)

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Supporting Information (PDF)
4213
Manikanta, Gembali; Nagaraju, Tumula; Radha Krishna, Palakodety:
Total Synthesis of the Proposed Structures of the Novel Antimalarial Pyranone Cryptorigidifoliol E

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PDF (200 kb)

Zusatzmaterial

Supporting Information (PDF)
4221
Lu, Zheng; Yang, Yong-Qing; Li, Hong-Xia:
Photoinduced Aromatization of Dihydropyridines

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PDF (178 kb)

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Supporting Information (PDF)
4228
Tao, Lili; Xu, Zhiliang; Han, Jing; Deng, Hongmei; Shao, Min; Chen, Jie; Zhang, Hui; Cao, Weiguo:
Copper-Catalyzed Cyclization/Oxidation/Aromatization Cascade: Efficient Synthesis of Trifluoromethylated Pyrrolo[2,1-a]isoquinolines

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PDF (404 kb)

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4237
Peralta-Hernández, Eduardo; Cordero-Vargas, Alejandro:
Model Studies Toward the Enantioselective Synthesis of Perhydrohistrionicotoxin: A Free-Radical Approach to the Azaspirocycle Core

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PDF (288 kb)

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4246
Vidal, Matías; García-Arriagada, Macarena; Rezende, Marcos Caroli; Domínguez, Moisés:
Ultrasound-Promoted Synthesis of 4-Pyrimidinols and Their Tosyl Derivatives

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PDF (189 kb)

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4253
Carlson, Emily; Hong, Daniel; Tam, William:
Type 2 Ring-Opening Reactions of Cyclopropanated 7-Oxabenzonorbornadienes with Carboxylic Acid Nucleophiles

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4260
Dhara, Kalyan; Kapat, Ajoy; Ghosh, Tridev; Dash, Jyotirmayee:
Transition-Metal-Free Terminal Alkyne Addition to Isatins

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PDF (408 kb)

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4269
Tverdiy, Dmytro O.; Chekanov, Maksym O.; Savitskiy, Pavlo V.; Syniugin, Anatolii R.; Yarmoliuk, Sergiy M.; Fokin, Andrey A.:
Efficient Preparation of Imidazo[1,5-a]pyridine-1-carboxylic Acids

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Primärdaten
Primary Data (ZIP)
4278
Nedolya, Nina A.; Tarasova, Olga A.; Albanov, Alexander I.; Trofimov, Boris A.:
One-Pot Synthesis and Intramolecular Cyclization of 5-(Prop-2-ynylsulfanyl)-1H-pyrrol-2-amines: A Simple Approach to 2,7-Dihydrothiopyrano[2,3-b]pyrrol-6-amines

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PDF (346 kb)

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4295
Tamaddon, Fatemeh; Tafti, Arefeh Dehghani; Pooramini, Farzaneh:
An Improved Synthesis of Multi-Substituted Pyrazines under Catalyst- and Solvent-Free Conditions

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PDF (173 kb)
4300
Ramesh, Perla:
Protecting-Group-Free Total Synthesis of 8-Methoxygoniodiol

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Synthesis

SYNFORM ISSUE 2016/12

Recent Progress in Chemical Syntheses of Sphingosines and Phytosphingosines

Recent Advances in the Asymmetric Nozaki–Hiyama–Kishi Reaction

External-Oxidant-Based Multicomponent Reactions

Synthesis and Applications of Fluorocyclopropanes

A General and Robust Method for the Preparation of (E)- and (Z)-Stereodefined Fully Substituted Enol Tosylates: Promising Cross-Coupling Partners

A Modular Four-Component Route to Substituted 1,7,9-Decatrien-3-ones Using a Chloro-Substituted Phosphorane as Key C₃ Building Block

Diastereoselective Synthesis of Spiro[pyrazolone-4,3′-tetrahydrothiophenes] via a Sulfa-Michael/Aldol Domino Reaction

Controlled Generation of 3-Triflyloxyarynes

Concise Preparation of the Bis-THF Core of Annonaceous Acetogenins

Synthesis of Bicyclic Boron Heterocycles Containing [1,3,4,2]Oxadiazaborole and [1,3,2]Oxazaborine

A Convenient Synthesis of Dithieno[3,2-b:2′,3′-d]thiophenes from Thiophene

Intramolecular Mizoroki–Heck Reaction of 2-Thiosubstituted Acrylates for the Synthesis of 3-Substituted Benzo[b]thiophene-2-carboxylates

Indium(III) Isopropoxide as a Hydrogen Transfer Catalyst for Conversion of Benzylic Alcohols into Aldehydes or Ketones via Oppenauer Oxidation

Synthesis of Erythrochelin: A Hydroxamate-Type Siderophore from Saccharopolyspora erythraea

Palladium-Catalyzed Asymmetric 1,6-Addition of Diarylphosphines to Allylidenemalonates for Chiral Phosphine Synthesis

Synthesis of Typical Isocopalane Diterpenes: ent-Spongian-16-one, ent-Isoagatholactone, and Anisodorin 5

An Asymmetric Synthesis of Rosuvastatin Calcium

Stereoselective Total Synthesis of (±)-Dasycarpidol and (±)-Dasycarpidone

Application of 5-Ethoxymethylfurfural (EMF) for the Production of Cyclopentenones

The Concept of Sequential Multicomponent Reactions: A Short Synthesis of Thiazolo- and Oxazolo[1,4]benzodiazepine-2,5-diones

Facile Synthesis of Some Chlorinated and Heteroatom-Rich Monocyclic β-Lactams via the Staudinger Reaction of Acyclic S-Alkylisothioureas

Unified Approach to Pyrazole-Fused Heterocyclic and Carbocyclic Motifs through One-Pot Condensation and Intramolecular Dipolar Cycloaddition Reaction

Total Synthesis of the Proposed Structures of the Novel Antimalarial Pyranone Cryptorigidifoliol E

Photoinduced Aromatization of Dihydropyridines

Copper-Catalyzed Cyclization/Oxidation/Aromatization Cascade: Efficient Synthesis of Trifluoromethylated Pyrrolo[2,1-a]isoquinolines

Model Studies Toward the Enantioselective Synthesis of Perhydrohistrionicotoxin: A Free-Radical Approach to the Azaspirocycle Core

Ultrasound-Promoted Synthesis of 4-Pyrimidinols and Their Tosyl Derivatives

Type 2 Ring-Opening Reactions of Cyclopropanated 7-Oxabenzonorbornadienes with Carboxylic Acid Nucleophiles

Transition-Metal-Free Terminal Alkyne Addition to Isatins

Efficient Preparation of Imidazo[1,5-a]pyridine-1-carboxylic Acids

One-Pot Synthesis and Intramolecular Cyclization of 5-(Prop-2-ynylsulfanyl)-1H-pyrrol-2-amines: A Simple Approach to 2,7-Dihydrothiopyrano[2,3-b]pyrrol-6-amines

An Improved Synthesis of Multi-Substituted Pyrazines under Catalyst- and Solvent-Free Conditions

Protecting-Group-Free Total Synthesis of 8-Methoxygoniodiol