Synlett

Issue 01 · January 2009

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Chapyshev, Sergei V.: Selective Reactions on the Azido Groups of Aromatic Polyazides

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El Kharrat, Salem; Laurent, Philippe; Blancou, Hubert: The Stability/Reactivity Effects of Trifluoromethyl and Perfluoroalkyl Chains in a Masked 1,3-Dicarbonyl Derivative: The Case of 1-Acetoxy-1-iodo-2-(perfluoroalkyl)ethanes

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23
Morton, Jason G. M.; Kwon, Laura D.; Freeman, John D.; Njardarson, Jon T.: Thieme Chemistry Journal Awardees - Where are They Now? Efforts towards the Total Synthesis of Vinigrol

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Sato, Akinori; Yorimitsu, Hideki; Oshima, Koichiro: Thieme Chemistry Journal Awardees - Where are They Now? Regio- and Stereoselective Radical Additions of Thiols to Ynamides

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32
Srikrishna, A.; Ravi, G.; Venkata Subbaiah, D. R. C.: Enantioselective First Total Syntheses of 2-(Formylamino)trachyopsane and ent-2-(Isocyano)trachyopsane via a Biomimetic Approach

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35
Asano, Keisuke; Matsubara, Seijiro: N-Alkylimidazole as Amphiphilic Organocatalyst: ‘Catalytic’ Morita-Baylis-Hillman Reaction on Water without Organic Solvent

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Jung, Ji-Young; Taher, Abu; Kim, Hyun-Jin; Ahn, Wha-Seung; Jin, Myung-Jong: Heck Reaction Catalyzed by Mesoporous SBA-15-Supported Ionic Liquid-Pd(OAc)₂

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Yadav, Jhillu S.; Gayathri, Kamakolanu Uma; Reddy, Basi V. Subba; Prasad, Attaluri R.: Modular Total Synthesis of Lamellarin G Trimethyl Ether

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47
Cardullo, Francesca; Donati, Daniele; Merlo, Giancarlo; Paio, Alfredo; Petricci, Elena; Taddei, Maurizio: Microwave-Assisted Aminocarbonylation of Aryl Bromides at Low Carbon Monoxide Pressure

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51
Bertolini, Ferruccio; Woodward, Simon: Rapid 1,4-Alkynylation of Acyclic Enones Using K[F₃BCCR]

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55
Khoshkholgh, Malihe Javan; Balalaie, Saeed; Bijanzadeh, Hamid Reza; Gross, Jürgen H.: Copper(I) Iodide Catalyzed Domino Knoevenagel Hetero-Diels-Alder Reaction of Terminal Acetylenes: Synthesis of Pyrano[2,3-c]pyrazoles

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59
Donald, James R.; Taylor, Richard J. K.: Tandem Meinwald Rearrangement-Fischer Indolisation: A One-Pot Conversion of Epoxides into Indoles

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63
Sluiter, Jonas; Christoffers, Jens: Synthesis of 1-Methylbenzimidazoles from Carbonitriles

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67
Rauhut, Christian B.; Cervino, Christian; Krasovskiy, Arkady; Knochel, Paul: Stereoselective Preparation of Cyclopropylmagnesium Reagents via a Br-Mg Exchange Using i-PrMgCl×LiCl in the Presence of Dioxane

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71
Hanessian, Stephen; Riber, Ludivine; Marin, Julien: Diastereoselective Synthesis of Functionally Diverse Substituted Pipecolic Acids

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75
Vale, Juliana A.; Zanchetta, Daniel F.; Moran, Paulo J. S.; Rodrigues, J. Augusto R.: Efficient α-Methylenation of Carbonyl Compounds in Ionic Liquids at Room Temperature

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Park, Hee Joong; Lee, Jong Chan: Oxidation of Benzylic Alcohols with Urea-Hydrogen Peroxide and Catalytic Magnesium Bromide

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81
Cho, Chang Ho; Lee, Jin Young; Kim, Sunggak: Radical Cyanation of Alkyl Iodides with Diethylphosphoryl Cyanide

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85
Kuroboshi, Manabu; Kobayashi, Ryoto; Nakagawa, Takayuki; Tanaka, Hideo: Electroreductive Generation of Recyclable Organic Reductant from N,N′-Dioctyl-4,4′-bipyridinium and Pd-Catalyzed Reductive Coupling of Aryl Halides

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Feray, Laurence; Perfetti, Patricia; Bertrand, Michèle P.: Mild Stereoselective Hydrohalogenation Leading to (Z)-Halopropenamides at Room Temperature

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92
Hajbi, Youssef; Suzenet, Franck; Khouili, Mostafa; Lazar, Said; Guillaumet, Gérald: General Synthetic Approach to 4-Substituted 2,3-Dihydrofuro[2,3-b]pyridines and 5-Substituted 3,4-Dihydro-2H-pyrano[2,3-b]pyridines

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97
Grigg, Ronald; Somasunderam, Anoma; Sridharan, Visuvanathar; Keep, Ann: Palladium-Catalysed Cascades Triggered by Dehydrogenation of Secondary or Tertiary Amines: Access to Bridged- and Fused-Ring Heterocycles

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100
Lundhaug, Kamilla; Skattebøl, Lars; Aasen, Arne Jørgen: Synthesis of (1S,3R,5R,7S)-Sordidin, the Main Component of the Aggregation Pheromone of the Banana Weevil Cosmopolites sordidus

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103
Cordaro, Massimiliano; Grassi, Giovanni; Risitano, Francesco; Scala, Angela: A New Construction of Diversely Functionalized Oxazoles from Enolizable Cyclic 1,3-Dicarbonyls and 5(4H)-Oxazolones

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106
Hugenberg, Verena; Haufe, Günter: Oxidative Desulfurization-Difluorination of Alkyl Aryl Thioethers: Synthesis of ω-Substituted 1,1-Difluoroalkanes

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109
Sälinger, Daniel; Brückner, Reinhard: High-Yielding Large-Scale Syntheses of Enantiomerically Pure NOBIN and a NOBIN-Based Enantiomerically Pure NHC Precursor

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112
Gillis, H. Martin; Greene, Lana; Thompson, Alison: Preparation of Sulfenyl Pyrroles

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117
Ojha, Lawanya R.; Kudugunti, Shashi; Maddukuri, Padma P.; Kommareddy, Amitha; Gunna, Meena R.; Dokuparthi, Praveen; Gottam, Hima B.; Botha, Kiran K.; Parapati, Divya R.; Vinod, Thottumkara K.: Benzylic Carbon Oxidation by an in situ Formed o-Iodoxybenzoic Acid (IBX) Derivative

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122
Arai, Masaki; Miyauchi, Yayoi; Miyahara, Tadashi; Ishikawa, Teruhiko; Saito, Seiki: Synthesis of 4-Acetoxyindoles and Related Derivatives by Means of Air Oxidation of 4-Oxo-4,5,6,7-tetrahydroindoles Obtained from Nitroalkenes and Cyclohexane-1,3-diones

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129
Lovely, Carl J.; Flores, Jaime A.; Meng, Xiaofeng; Dias, H. V. Rasika: Silver-Catalyzed C-H Insertion Reactions with Donor-Acceptor Diazoacetates

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133
Pillekamp, Marcus; Aniol, Alexandra; Heppekausen, Johannes; Neukirchen, Saskia; Seel, Stephanie; Oppel, Iris M.; Dyker, Gerald: Palladium-Catalyzed Four-Membered Ring Annelation Reactions at Dibenzobarrelene

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138
Yoo, Woo-Jin; Correia, Camille A.; Zhang, Yuhua; Li, Chao-Jun: Oxidative Alkylation of Cyclic Benzyl Ethers with Malonates and Ketones Using Oxygen as the Terminal Oxidant

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143
Zalatan, David N.; Du Bois, J.: Oxidative Cyclization of Sulfamate Esters Using NaOCl - A Metal-Mediated Hoffman-Löffler-Freytag Reaction

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147
Harrisson, Peter; Morris, James; Steel, Patrick G.; Marder, Todd B.: A One-Pot, Single-Solvent Process for Tandem, Catalyzed C-H Borylation-Suzuki-Miyaura Cross-Coupling Sequences

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151
Nadeau, Etienne; Li, Zhanjie; Morton, Daniel; Davies, Huw M. L.: Rhodium Carbenoid Induced Intermolecular C-H Functionalization at Tertiary C-H Bonds

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spotlight
155
Amarante, Giovanni Wilson: Ozone: A Versatile Oxidizing Agent in Academic Syntheses and Industrial Processes FREE ACCESS

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157
Iglesias-Sigüenza, Francisco Javier: Carbon Disulfide (CS₂) FREE ACCESS

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addenda and errata
e1
Oxidative Desulfurization-Difluorination of Alkyl Aryl Thioethers:
Synthesis of ω-Substituted 1,1-Difluoroalkanes FREE ACCESS

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