Synfacts

Issue 03 · March 2017

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Syntheses of Sarcandrolide J and Shizukaol D
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Synthesis of (+)-Sieboldine A

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Syntheses of (–)-Rotenone and (–)-Dalpanol

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Asymmetric Cyclopropanation Using Engineered Myoglobin Catalysts

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Conductively Heated Sealed-Vessel Reactor: Synthesis of Olanzapine

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Synthesis of (+)-Mikanokryptin

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Synthesis of (+)-Pseudoanisatin

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Synthesis of (–)-Histrionicotoxin

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Synthesis of Idasanutlin (RG7388)

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Synthesis of BMS-986104

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Synthesis of Heterocycles
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Photoredox Nitroso-Diels–Alder Reactions

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Acridones by Double C–H Carbonylation of Diphenylamines

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A New Class of Enantiopure Oxathiazines

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Photochemical Stereoselective Synthesis of Azetidines

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Multicomponent Synthesis of Substituted 3H-1,4-Benzodiazepines

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Synthesis of Hexahydropyrazolo[1,5-a]-pyridines

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Palladium-Catalyzed Benzazetidine Synthesis with a Rationally Designed Oxidant

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Synthesis of Imidazo[1,5-a]pyrazin-8(7H)-ones

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Indole Synthesis through Dizincioindole Formation

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Squaramide-Catalyzed Synthesis of 3-Chroman Derivatives

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Chromones and Benzofurans by a Divergent Rhodium-Catalyzed Annulation

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An Aza-Prins Reaction in the Synthesis of Tricyclic Benzazocines

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Synthesis of Indazoles and Indoles from Azobenzenes through C–H Activation

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Trifluoromethylated 1,3,4-Thiadiazoles by [2+3] Cycloaddition

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Substituted Oxindoles and Dibenzoazepinones through Aryne Insertion

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Synthesis of Materials and Unnatural Products
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Three Benzynes and the Ynolate
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K-Region Annulative π-Extension with Alkynes

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Serendipity in the Reactions of Indole-3-carboxaldehyde with Grignard Reagents

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Supercharged Relay Race to Spirodiazafluorenes

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Reaction Update: A McMurry Coupling with Silicon

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Recipe for a More Aromatic Pi

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HF Finally Completely Trapped

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Gold and Ruthenium Hand in Hand

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Hooping it up with Furans

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New C–H Arylation Saves Steps for Small-Molecule Organic Semiconductors

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Suzuki–Miyaura Cross-Coupling of Aromatic Esters

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O–H/C–H Difunctionalization of Phenols

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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Ruthenium-Catalyzed Asymmetric Photocycloaddition of 2′-Hydroxychalcones
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One-Pot Synthesis of Chiral Tricycles by Amine and Ytterbium Catalysis

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Asymmetric Radical Cyclopropanation of Alkenes
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Rhodium-Catalyzed Stereodivergent Cyclization of Allenyl Sulfonylcarbamates

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Diastereoselective Intermolecular Rhodium-Catalyzed Hydroalkylation

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Palladium-Catalyzed Asymmetric Allylic Substitution with 1,3-Dithianes

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Iridium-Catalyzed Asymmetric Hydrogenation of Exocyclic C=C Bonds

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Palladium-Catalyzed Asymmetric Synthesis of Chiral Fused Azabicycles

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Iron-Catalyzed Enantioselective Synthesis of BINOLs

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Asymmetric Arylation of Alkyl Nitriles Catalyzed by Palladium

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Palladium-Catalyzed Regioselective Thiocarbonylation

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Rhodium-Catalyzed Enantiospecific [4+3] Cycloaddition of Vinyl Aziridines and Dienes

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Palladium-Catalyzed Asymmetric Synthesis of Dispirooxindoles

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Iridium-Catalyzed Asymmetric Dearomatization of β-Naphthols with Allylic Alcohols

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Enantioselective Oxa-Heck Reaction of Phenols with Allylic Alcohols

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Ruthenium-Catalyzed Cycloisomerization of 1,6-Enediyenes

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Palladium-Catalyzed Asymmetric Allylic Alkylation Generating Butyrolactones

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Au(I)/Ni(II)-Catalyzed Stereoselective Synthesis of α-Allyl β-Keto Esters

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Palladium-Catalyzed Asymmetric Allylation of Allylic Acetates

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Photocatalytic Asymmetric Epoxidation with a Chiral Manganese Complex

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Development of a Palladium-Catalyzed Stereoretentive Stille Coupling Reaction

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Copper-Catalyzed Asymmetric [3+4] Cycloaddition of Nitrones to Azoalkenes

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Copper-Catalyzed Synthesis of Homoallylic Alcohols

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Chiral Aluminum Catalyzed Enantioselective Vinylation of Aldehydes

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Palladium-Catalyzed Asymmetric Mannich-Type Reaction of Dichloroacetonitrile

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Ruthenium-Catalyzed Asymmetric Synthesis of cis-β-Heteroaryl Amino Alcohols

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Stereodivergent Pd–Au Sequential Catalysis Forming Tetrahydropyrans

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Rhodium-Catalyzed Asymmetric Hydrogenation of Enamides

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Metal-Mediated Synthesis
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C_sp2–C_sp2 Coupling of Poly(pseudo)halogenated Arenes in Air

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Amination of Internal Alkynes

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Asymmetric Petasis Borono-Mannich Allylation

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Palladium-Catalyzed Cascade Reaction of Bisallenes

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ortho-Selective C–H Borylation of Aryl Sulfides

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Asymmetric Arylation of 2-Indolylacrylates

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Terminal Hydroboration of Branched Alkenes

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Synthesis of Isonitriles via One-Step Transformation of Trichloroacetamides

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0301
Transformation of Homopropargyl Sulfonamides

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Dephosphonylation of α-Diazo-β-Carbonyl Phosphonates

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Reductive Nickel-Catalyzed Coupling of Enones with Alkyl Bromides

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Copper-Catalyzed Chan–Lam Cross-Coupling

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α-Arylation of α-Amino Acid Derivatives

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Oxidative Cross-Coupling of Arylsilanes

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Iron(II) Chloride Promoted Radical Cascade

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Organo- and Biocatalysis
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Nonnatural Reactivity of Cofactor-Dependent Enzymes upon Light Irradiation
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Catalytic Asymmetric Umpolung Reactions of Imines with Enones

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Asymmetric Catalytic Polyene Bromocyclization

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0312
Optically Switchable Helicenes for an Enantiodivergent Steglich Rearrangement

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0313
Cation Binding Catalysis for Enantioenriched Dioxazinanes and Dioxazepanes

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0314
Large-Scale Biocatalytic Oxidation of a Sulfone to a Chiral Sulfoxide

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0315
Organocatalytic Stereoselective [8+2] and [6+4] Cycloaddtions

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0316
1,1,3,3-Tetratriflylpropene: A Strong Brønsted or Lewis Acid Catalyst

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0317
Asymmetric Synthesis of Rauhut–Currier-type Products by Bifunctional Catalysis

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Polymer-Supported Synthesis
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0319
Hydrogenations with Hydrotalcite-Supported Gold–Ceria Nanocomposites
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0320
C–H and C–C Bond Activation by Iron–Silver Nanoparticles

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0321
Spirocyclization of Alkyne-Tethered Indoles on Supported Silver Nanoparticles

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0322
Gold-Catalyzed Aerobic Oxidative α,β-Dehydrogenation of Ketones

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0323
Iridium–Porphyrin Metal–Organic Framework Catalyzed Si–H Insertion of α-Diazo Esters

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0324
Controlled Reduction of Nitroarenes Catalyzed by Ruthenium Nanoparticles

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0325
Synthesis of Propargylamines with Gold Nanoclusters

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0326
Semihydrogenation of Alkynes to Alkenes on Silica-Supported Copper Nanoparticles

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0327
Solid-Supported Alkynes for an Unsymmetrical Glaser–Hay Reaction

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0328
Synthesis of Dihydropyrimidines with Ferrite-Supported Sulfonated PEG

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0329
Synthesis of Quinolines on a Supported Bismuth(III) Catalyst

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0330
Palladium–Nickel/Zirconia Catalyst for Hydrogenolysis of 2-Aryloxy-1-arylethanols

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Thiosemicarbazide–Formaldehyde Resin as a Nucleophilic Scavenger

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0332
Asymmetric Ring Opening of Epoxides with a Supported Cobalt–Salen Complex

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0333
Hexagonal Boron Nitride Supported Palladium Catalyst for Suzuki and Heck Reactions

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0334
Chiral VO(salen) Metal–Organic Framework for Asymmetric Cyanosilylation of Aldehydes

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