Synfacts

Issue 09 · September 2016

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Synform
A126
SYNFORM ISSUE 2016/09
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Synthesis of Natural Products and Potential Drugs
z883
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0883
Synthesis of Millingtonine

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0884
Synthesis of a MK-8876 Fragment

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0885
Total Synthesis of (−)-Communesin F
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0886
Organocatalytic Synthesis of Enantiopure 2H- and 3H-Pyrroles

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0887
Synthesis of Letermovir by an Asymmetric Aza-Michael Reaction
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0888
Synthesis of (+)-SCH 351448

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0889
Synthesis of (±)-Integrifolin

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0890
Synthesis of Lotronex through anti-Azacarboxylation of a 2-Alkynylaniline

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0891
Synthesis of a PDE4 Inhibitor by C–H Activation

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0892
Synthesis of Calophyline A

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0893
Total Synthesis of (±)-Aplydactone

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0894
Synthesis of the CHK1 Inhibitor MK-8776

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0895
Synthesis of Thailanstatin A

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0896
Formal Synthesis of HIV Integrase Inhibitor BI 224436

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Synthesis of Heterocycles
z897
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0897
Synthesis of Palbociclib: An S_NAr Reaction on a Kilogram Scale

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0898
Pyrimido[4,5-d]pyridazines by the Reaction of Pyrimidines with Tetrazines

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0899
Four-Component Synthesis of 1-Pyrimidin-2-yl-3,4-dihydropyridin-2(1H)-ones

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0900
Synthesis of Trifluoromethylated Isoxazoles by [2+3] Cycloaddition

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0901
Synthesis of Azabicycloalkanes by Gold(I)-Catalyzed Amination of Ynones

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0902
Microwave-Assisted Synthesis of 1-Arylnaphtho[2,1-b]furans

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0903
Regiocontrolled Synthesis of Benzo-Fused (Hetero)aromatics from Dihydrofuran Acetals

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0904
Copper(I)-Promoted Synthesis of Halogenated Tetrahydrothiophenes

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0905
Synthesis of Pyrrolidines and Piperidines with Tin Amine Reagents

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0906
Synthesis of Oxindoles from α,β-Unsaturated Amides and Aldehydes

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0907
Rhodium-Catalyzed Synthesis of Fused Heterocycles

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0908
Synthesis of Functionalized 1,4-Oxazines by Activation of Diazoenals

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0909
Functionalized Isoquinolines by Rh(III)-Catalyzed C–H Conjugate Addition

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0910
Synthesis of 2-Quinolinones by Lactamization of 2-Alkenylanilines with CO₂

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Synthesis of Materials and Unnatural Products
z911
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0911
Molecular Knot Inducing Allosteric Control of Catalysis
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0912
Let the Acid Do the Job

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0913
Oligomeric Ferrocene Rings

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0914
First Experimental Evidence for the Formation of the Cyclic Carbon Dioxide Trimer

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0915
Neutral Diboron Analogues of Archetypal Aromatic Species by Cycloaddition

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0916
Five- and Seven-Membered Rings Containing Isomeric Pentacene

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0917
Combinations of 1,2- and 1,4-Additions to an Acene Dione

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0918
Between Diamond and Graphene

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0919
A Creative Route to Perfluororubrene

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0920
Embedding Nitrogen Atoms in Polymers to generate n-Type FETs

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0921
One-Pot Synthesis of Complex Polymers via Copper Catalysis

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0922
Palladium-Catalyzed Annulation of Internal Alkynes to Ullazines

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z923
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0923
Copper-Catalyzed Asymmetric Nucleophilic Addition to Ketones
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0924
Asymmetric Hydroarylation of Vinylarenes with CuH and Pd Catalysts

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0925
Copper-Catalyzed Asymmetric [4+1] Annulation of Sulfur Ylides
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0926
Kinetic Resolution by Asymmetric Amide Addition

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0927
Neodymium-Catalyzed [3+2] Cycloaddition of Aziridines and Aldehydes

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0928
Iridium-Catalyzed Asymmetric Hydroalkynylation of Enamides

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0929
Rhodium-Catalyzed Enantioselective Macrolactonization

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0930
Rhodium-Catalyzed E-Selective Hydro-formylation of Alkynes

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0931
Noncovalent Ion Pair Interaction in Rhodium-Catalyzed Asymmetric Hydrogenation

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0932
Enantioselective Synthesis of α-Allyl-α-Aryl-cyclopentanones

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0933
Nickel-Catalyzed Asymmetric C-Acylation of Lactams

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0934
Enantio- and Diastereoselective Addition of 1,1-Diborylalkanes to α-Keto Esters

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0935
Rhodium-Catalyzed Asymmetric Hydrogenation of Acroleins

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0936
Asymmetric Desymmetrization of meso-Epoxy Diketones

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0937
Asymmetric Rearrangement of N-Acylaziridines to Oxazolines

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0938
Iridium-Catalyzed Asymmetric Hydrogenation of Simple Ketones

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0939
Enantioselective C–H Activation for the Formation of Chiral Isochromans

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0940
Synthesis of Chiral Tryptamines under Cu(I) Catalysis

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0941
Rhodium-Catalyzed Asymmetric Radical Amination Activated by Visible Light

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0942
Asymmetric Benzylic Alkylation of Active Methylene Compounds

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0943
Nickel-Catalyzed Asymmetric Synthesis of Imidazolines

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0944
Asymmetric Hydroformylation by Rh-BIBOP Complex

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0945
Supported Copper(II) Catalysts for the Asymmetric Henry Reaction

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0946
Rhodium-Catalyzed Synthesis of trans-Dimethylenecyclobutane-1,2-diamines

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0947
Iridium-Catalyzed Asymmetric Allylation of Fluorinated Methylene Derivatives

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0948
Copper-Catalyzed Aerobic Asymmetric Cross-Dehydrogenative Coupling

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0949
Copper-Catalyzed Cycloaddition for the Synthesis of Chiral Bicycloprolines

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0950
Cyclization of Dearomatized Alkylidene Dihydropyridines

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0951
Copper-Catalyzed Cascade Aldol-Cyclization Reaction

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0952
Catalytic Asymmetric [2+2+2] Cycloaddition

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Metal-Mediated Synthesis
z953
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0953
Palladium-Catalyzed Alkynylation

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0954
Synthesis of 1,3-Dienes

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0955
Direct Cross-Couplings of Propargylic Diols
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0956
Ruthenium-Catalyzed Hydroboration of Pyridines

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0957
anti-Carbometalation of Alkynes via Alkenylnickel Intermediates

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0958
O-Acylation of Alcohols and Phenols by Using Cp₂TiCl

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0959
Copper-Catalyzed Isomerization of α-Hydroxy Ynamides

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0960
Oxidative β,β-Fluoroarylation

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0961
Nickel-Catalyzed Borylation

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0962
Enantioselective Construction of Quaternary Carbon Stereocenters

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0963
Stereoselective Cycloaddition of Nitrone Ylides with Aldehydes using n-BuLi

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0964
Oxidative Cyclization of Diarylalkynes to Indoloindole Derivatives

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0965
Regioselective Functionalization of 2-Phenyltetrahydropyran

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0966
Oxyarylation of Furans

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0967
Direct Amidation of Unprotected Amino Acids

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Organo- and Biocatalysis
z969
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0969
Single-Step Enzymatic Synthesis of β-Methyltryptophans
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0970
Brønsted Acid Catalyzed Synthesis of Chiral Tetrahydroacridines

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0971
Brønsted Acid Catalyzed Transfer Hydrogenation of Imines and Alkenes

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0972
Chiral NHC-Catalyzed Benzoin Reaction Permits a Dynamic Kinetic Resolution

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0973
Enantioselective Intermolecular [2+2] Photocycloaddition

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0974
Conformational Control of Thiourea Catalysts for Improved Performance

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0975
Enantioenriched γ-Butenolides via Chiral Electrophilic Selenium Catalysis

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0976
Alkynylogous Mukaiyama Aldol Reaction

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Polymer-Supported Synthesis
z977
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0977
Photocatalytic Sonogashira Coupling on Polymeric Pyrazine–CuO Nanoparticles
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0978
Oxidation of α-Hydroxy Ketones by Dendrimer-Stabilized Gold Nanoclusters

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0979
Supported Gold Nanoparticles Catalyzed the α-Oxygenation of Amines to Amides

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0980
Hydrogenation of Nitro Compounds by Using a Porous Carbon–Cobalt Catalyst

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0981
Oxidative α-Cyanation of Tertiary Amines by a Gold Complex on Magnetic Nanoparticles

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0982
Sonogashira Coupling by Using a Mesoporous Carbon Nitride–Pd Catalyst

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0983
C–C Bond Formation by Using Magnetite-Supported Pd(II)–β-Cyclodextrin

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0984
Dehydrogenative Cyclization of ortho-Alkenylphenols by Using Pd/C

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0985
Copper-Catalyzed Oxidation of Benzaldehydes to Benzonitriles

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0986
Transamidation Catalyzed by Fe₃O₄ Nanoparticles

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0987
Controlled Hydrogenation of Nitrobenzenes to Anilines on RhIn/SiO₂

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0988
Aminocarbonylation of 1-Alkynes by Using Palladium/Carbon

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0989
Pd-Catalyzed N-Methylation of Amines with Paraformaldehyde and Calcium Hydride

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0990
Asymmetric Aldol Reaction Catalyzed by a Polystyrene-Supported Triazolylproline

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0991
Synthesis of 4(3H)-Quinazolinones by Using a CuCO₃–K₂CO₃ Nanocomposite

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0992
Synthesis of Phthalazine Derivatives with a Supported Organocatalyst

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0993
Silver Iodide Catalyzed Synthesis of Carbo-nates from Propargylic Alcohols and CO₂

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Erratum
995
Pyrrolizidines and Indolizidines by Photooxidation of Furylalkylamines

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996
Asymmetric Chromium-Catalyzed Dearomative 1,2-Addition

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997
Enantioselective Rhodium-Catalyzed C−H Insertion of Carbenes

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