Synthesis

Issue 03 · February 2007

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327
Feist, Holger; Langer, Peter: One-Pot Synthesis of Functionalized Carbacycles by Formal [3+3] Cyclizations of 1,3-Bis(silyl enol ethers) with 1,3-Dielectrophiles

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348
Strerath, Michael; Meng, Martin; Kubik, Stefan: Facile One-Step Synthesis of Mono-2-(p-Tolylsulfonyl)-β-cyclodextrin under Aqueous Conditions

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351
Murata, Miki; Oda, Takeshi; Watanabe, Shinji; Masuda, Yuzuru: 4,4,6-Trimethyl-1,3,2-dioxaborinane: A Practical Reagent for Palladium-Catalyzed Borylation of Aryl Halides

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355
Silva, Luiz F.; Quintiliano, Samir A. P.; Craveiro, Marcus V.; Vieira, Fabiana Y. M.; Ferraz, Helena M. C.: Rearrangement of Homoallylic Alcohols with Thallium(III): Diastereoselective Synthesis of Indans Bearing a β-Hydroxy Ketone Moiety

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363
Antoniow, Sylwia; Witt, Dariusz: A Novel and Efficient Synthesis of Unsymmetrical Disulfides

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367
Popowycz, Florence; Bernard, Philippe; Raboisson, Pierre; Joseph, Benoît: Synthesis of 8-Substituted Pyrazolo[1,5-a]-1,3,5-triazine Derivatives by Palladium-Catalyzed Cross-Coupling Reactions

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375
Kouznetsov, Vladimir V.; Cruz, Uriel Mora; Zubkov, Fedor I.; Nikitina, Eugenia V.: An Efficient Synthesis of Isoindolo[2,1-a]quinoline Derivatives via Imino Diels-Alder and Intramolecular Diels-Alder Reactions with Furan

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385
Sabitha, Gowravaram; Sudhakar, K.; Yadav, J. S.: A Simple and Efficient Total Synthesis of a Styryllactone, 7-epi-Goniodiol

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389
Özçubukçu, Salih; Schmitt, Ellen; Leifert, Annika; Bolm, Carsten: A General and Efficient Synthesis of Nitrogen-Substituted Ferrocenes

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393
Cui, Xin; Qin, Tian; Wang, Jia-Rui; Liu, Lei; Guo, Qing-Xiang: Pd(N,N-Dimethyl β-alaninate)₂ as a High-Turnover-Number, Phosphine-Free Catalyst for the Suzuki Reaction

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400
Liang, Yun; Xie, Ye-Xiang; Li, Jin-Heng: Cy₂NH·HX-Promoted Cyclizations of o-(Alk-1-ynyl)benzoates and (Z)-Alk-2-en-4-ynoate with Copper Halides to Synthesize Isocoumarins and α-Pyrone

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407
Jin, Peiyuan; Liu, Kai; Ji, Sanhao; Ju, Yong; Zhao, Yufen: Synthesis of Novel Steroidal Bioconjugates with AZT and Phosphorus

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412
Ma, Heng Chang; Jiang, Xuan Zhen: Synthesis of Iminoquinones from Anilines Using IBX in DMSO

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417
Ryabukhin, Sergey V.; Plaskon, Andrey S.; Ostapchuk, Eugeniy N.; Volochnyuk, Dmitriy M.; Tolmachev, Andrey A.: N-Substituted Ureas and Thioureas in Biginelli Reaction Promoted by Chlorotrimethylsilane: Convenient Synthesis of N1-Alkyl-, N1-Aryl-, and N1,N3-Dialkyl-3,4-Dihydropyrimidin-2(1H)-(thi)ones

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428
Anabha, E. R.; Nirmala, K. N.; Thomas, Abraham; Asokan, C. V.: Synthesis of 3-Aroylnicotinonitriles from Aroylketene Dithioacetals

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433
Stas, Sara; Abbaspour Tehrani, Kourosch: Novel Boronic Acid Mannich Reactions of α,α-Dichloro- and α,α,ω-Trichloroaldehydes with Arylboronic Acids

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442
Ahmar, Mohammed; Knoke, Mario; de Meijere, Armin; Cazes, Bernard: Pauson-Khand Carbonylative Cocyclizations of Acetylenes with Cyclopropylallenes

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447
Trofimov, B. A.; Sobenina, L. N.; Stepanova, Z. V.; Ushakov, I. A.; Petrova, O. V.; Tarasova, O. A.; Volkova, K. A.; Mikhaleva, A. I.: Regioselective Cross-Coupling of 1-Vinylpyrroles with Acylbromoacetylenes on Al₂O₃: Synthesis of 2-(2-Acylethynyl)-1-vinylpyrroles

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452
Vasil’tsov, Alexander M.; Ivanov, Andrey V.; Ushakov, Igor’ A.; Mikhaleva, Al’bina I.; Trofimov, Boris A.: Selective Thiylation of 1-Vinylpyrrole-2-carbaldehydes: Synthesis of the Novel Pyrrole Synthons 2-[Bis(ethylsulfanyl)methyl]-1-vinylpyrroles and 1-(2-Ethylthioethyl)pyrrole-2-carbaldehydes

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457
Baag, Md Merajuddin; Sahoo, Manoj Kumar; Puranik, Vedavati G.; Argade, Narshinha P.: Reactions of o-Aminothiophenol and o-Aminophenyl Disulfide with Itaconic Anhydride and (-)-Dimenthyl Itaconate: Access to Enantiomerically Pure 1,5-Benzothiazepines and Benzothiazolyl-2-methylacrylic Acid

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feature article
464
Wessig, Pablo; Müller, Gunnar; Pick, Charlotte; Matthes, Annika: The Photo-Dehydro-Diels-Alder (PDDA) Reaction - A Powerful Method for the Preparation of Biaryls

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practical synthetic procedures
478
Zhou, Guoqiang; Yost, Julianne M.; Coltart, Don M.: A Direct Aldol Addition of Simple Thioesters Employing Soft Enolization

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book review
483
Hiersemann, Martin: Modern Aldol Reactions FREE ACCESS

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484
Waldvogel, Siegfried R.: The Organic Chemistry of Sugars FREE ACCESS

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