Synthesis

Issue 01 · January 2006

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editorial
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review
1
Bonauer, Christoph; Walenzyk, Thomas; König, Burkhard:
α,β-Dehydroamino Acids

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short paper
21
Prakash, Om; Kumar, Ajay; Sadana, Anil K.; Singh, Shiv P.:
A Novel Synthesis of New 3-Aryl-7-methylpyrano[4,3-b]pyran-4H,5H-diones Using Hypervalent Iodine(III) Reagents

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paper
24
Pietruszka, Jörg; Schöne, Niklas:
New Enantiomerically Pure Allylboronic Esters in Allyl Additions: Synthesis and NMR Investigation of Intermediates

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31
Koketsu, Mamoru; Kogami, Masakazu; Ando, Hiromune; Ishihara, Hideharu:
Preparation of 5-Acyl-2-amino-1,3-selenazoles by the Reaction of Selenazadienes with α-Haloketone

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37
Zhou, Aihua; Pittman Jr, Charles U.:
Generation of Cyclic Ketene-N,X-Acetals (X = O, S) from 2-Alkyl-1,3-oxazolines and 2-Alkyl-1,3-thiazolines. Reactions with Acid Chlorides, 1,3-Diacid Chlorides and N-(Chlorocarbonyl) Isocyanate

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49
Tonsiengsom, Fay; Miyake, Fumiko Y.; Yakushijin, Kenichi; Horne, David A.:
Reduction of 2,5-Bis(3′-indolyl)pyrazines to 2,5-Bis(3′-indolyl)piperazines: Synthesis of Bisindolylpiperazine Marine Alkaloids Dragmacidin A, B, and C

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55
Sharma, G. V. M.; Reddy, K. Laxmi; Lakshmi, P. Sree; Krishna, Palakodety Radha:
‘In situ’ Generated ‘HCl’ - An Efficient Catalyst for Solvent-Free Hantzsch Reaction at Room Temperature: Synthesis of New Dihydropyridine Glycoconjugates

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59
AL-Saleh, Balkis; Makhseed, Saad; Hassaneen, Huwaida M. E.; Elnagdi, Mohamed Hilmy:
Studies with Functionally Substituted Enamines: The Reactivity of Enaminals and Enamino Esters toward Naphthoquinone, Hydrazonoyl Halides, Aminoazoles and Hippuric Acid

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63
Singh, Vijay; Batra, Sanjay:
Convenient Synthesis of Substituted α-Methylene-δ-valerolactones in Aqueous Medium Using Baylis-Hillman Chemistry

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73
García, Marcos D.; Caamaño, Olga; Fernández, Franco; Abeijon, Paula; Blanco, José Manuel:
Synthesis of New 1′(N)-Homocarbanucleosides Based on 1-Methylcyclopenta[c]pyrazole Scaffold

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81
Couthon-Gourvès, Hélène; Simon, Gaëlle; Haelters, Jean-Pierre; Corbel, Bernard:
Synthesis of Novel Diethyl Indolylphosphonates and Tetraethyl Indolyl-1,1-bisphosphonates by Michael Addition

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89
Schmuck, Carsten; Rupprecht, Daniel; Urban, Christian; Walden, Nicholas:
Synthesis of Orthogonally Protected Pyrrole Tricarboxylic Acid Derivatives: Versatile Building Blocks for Pyrrole-Containing Compounds

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97
Sorokin, Vladimir Igorevich; Ozeryanskii, Valery Anatolievich; Borodkin, Gennady Sergeevich:
A New Route to Polykis(dialkylamino)benzenes and -naphthalenes Based on Protodefluorination of Electron-Rich Fluoroaromatics: Anion Radicals of Arenes as a Simple and Effective Alternative to ‘Classical’ LAH-Based Systems

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103
Brulé, Cédric; Bouillon, Jean-Philippe; Nicolaï, Eric; Portella, Charles:
Synthesis of Original Trifluoromethylated 6-Aryl-pyridazines Fused with Thiazolidine or 1,2,4-Triazole

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107
Nair, Vijay; Dhanya, R.; Vidya, N.; Devipriya, S.:
Lewis Acid Catalyzed Addition of Allylsilane to o-Quinonediimides: Formal Diels-Alder Reaction versus Allylation

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111
Shenglof, Margarita; Molander, Gary A.; Blum, Jochanan:
Cross-Coupling of Aryl Halides and Triflates with Group 13-Metal Alkylating Reagents by Palladium-Molybdenum and Palladium-Tungsten Mixed-Metal Catalysts

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115
Tiwari, Dharmendra Kumar; Gumaste, Vikas K.; Deshmukh, Abdul Rakeeb A. S.:
Azetidin-2,3-dione Synthon for Stereoselective Synthesis of cis- and trans-C-3-Alkyl/Aryl Azetidin-2-ones

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123
Song, Qing-bao; Lin, Ru-xiang; Teng, Ming-yu; Zhang, Jie; Ma, Chun-an:
An Improved Suzuki-Miyaura Cross-Coupling Reaction for the Synthesis of Fluorine-Substituted 3-Biaryl-1-ferrocenyl-2-propen-1-one

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128
Nadano, Ryo; Ichikawa, Junji:
1-(Trifluoromethyl)vinylation via Oxirane or Oxetane Ring-Opening: A Facile Synthesis of 4- or 5-Hydroxy-Functionalized 2-Trifluoromethyl-1-alkenes

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133
Cai, Lisheng; Brouwer, Chad; Sinclair, Kathryn; Cuevas, Jessica; Pike, Victor W.:
Titanium(IV) Chloride Promoted Syntheses of New Imidazo[1,2-a]pyridine Derivatives under Microwave Conditions

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146
Coe, Benjamin J.; Curati, Naomi R. M.; Fitzgerald, Emma C.:
Unusually Facile Syntheses of Diquat (6,7-Dihydrodipyrido[1,2-a:2′,1′-c]pyrazinediium) and Related Cations

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151
Anabha, Engoor R.; Asokan, Chittoorthekkathil V.:
A Convenient Preparation of 2-Aroyl-3,3-bis(alkylsulfanyl)acrylaldehydes and Their Application in the Synthesis of 5-Aroyl-2-oxo-1,2-dihydro-2-pyridinecarbonitriles

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156
Ivanova, Natalia V.; Sviridov, Sergey I.; Shorshnev, Sergey V.; Stepanov, Aleksander E.:
A Convenient Synthesis of 4,5-Disubstituted 1,2,4-Triazoles Functionalized in Position 3

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161
Heidecke, Christoph D.; Lindhorst, Thisbe K.:
Regioselective Phthalimidopropyl-Modification of Carbohydrates in One Step

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feature article
166
Commeiras, Laurent; Bourdron, Julien; Douillard, Soazig; Barbier, Pascale; Vanthuyne, Nicolas; Peyrot, Vincent; Parrain, Jean-Luc:
Total Synthesis of Terpenoids Isolated from Caulerpale Algae and Their Inhibition of Tubulin Assembly

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practical synthetic procedures
182
Gingras, Marc; Chabre, Yoann M.; Raimundo, J.-M.:
Tetrabutylammonium Difluorotriphenylstannate [Bu₄N][Ph₃SnF₂]: Delivering Carbon or Fluorine Ligands via Hypercoordination

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book review
186
Menéndez, J. Carlos:
Microwave Assisted Organic Synthesis
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