Synthesis

Publication Date: 25 February 2020

paper

Gucchait, Arin; Ghosh, Sritin; Misra, Anup Kumar: Synthesis of Novel Glycosyl Carbamo(dithioperoxo)thioate Derivatives

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paper

Rahman, Md. Mahbubur; Li, Guangchen; Szostak, Michal: Thioesterification and Selenoesterification of Amides via Selective N–C Cleavage at Room Temperature: N–C(O) to S/Se–C(O) Interconversion

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paper

Wang, Zijuan; Chen, Wenteng; Luo, Haofan; He, Chang; Zhang, Guolin; Yu, Yongping: Cascade Reactions to Substituted 1H-Pyrrole-3-carbonitriles via Ligand-Free Palladium(II)-Catalyzed C(sp)–C(sp²) Coupling

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Publication Date: 24 February 2020

paper

Cheng, Dongping; Yan, Xianhang; Shen, Jing; Pu, Yueqi; Xu, Xiaoliang; Yan, Jizhong: Synthesis of 2,4-Diarylquinoline Derivatives via Chloranil-Promoted Oxidative Annulation and One-Pot Reaction

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paper

Mollo, María C.; Bisceglia, Juan A.; Kilimciler, Natalia B.; Mancinelli, Michele; Orelli, Liliana R.: Microwave-Assisted Synthesis of 2-Substituted 2-Thiazolines and 5,6-Dihydro-4H-1,3-thiazines

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paper

Zhu, Zheng-He; Ren, Ming-Zhe; Cao, Bao-Qian; Quan, Zheng-Jun; Wang, Xi-Cun: Metal- and Oxidant-Free Electrochemical Oxidative Desulfurization C–O Coupling of Thiourea-Type Compounds with Alcohols

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psp

Mulks, Florian F.; Heckershoff, Robin; Zimmer, Marc; Hashmi, A. Stephen K.: Practical Preparation of Cyclopropenone 1,3-Propanediol Ketal

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Publication Date: 20 February 2020

paper

Stockdale, Trevor F.; Leitch, Michael A.; O’Neil, Gregory W.: Chelation and Stereodirecting Group Effects on Regio- and Diastereoselective Samarium(II)-Water Allylic Benzoate Reductions

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paper

Tüllmann, Carl Phillip; Steiner, Sebastian; Knochel, Paul: Preparation and Reactions of (1H-Tetrazol-5-yl)zinc Pivalates

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Publication Date: 19 February 2020

feature

Ong, Derek Yiren; Chiba, Shunsuke: Controlled Reduction of Nitriles by Sodium Hydride and Zinc Chloride

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paper

Fiore, Vito A.; Keim, Michael; Werz, Roland; Maas, Gerhard: Electrophilic ipso-Halocyclization of N-Phenyl-N-triflylpropiolamides Leading to 8-Halo-1-azaspiro[4.5]deca-3,6,9-trien-2-ones

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short review

Ping, Yuanyuan; Kong, Wangqing: Ni-Catalyzed Reductive Difunctionalization of Alkenes

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Publication Date: 17 February 2020

paper

Chao, María N.; Szajnman, Sergio H.; Cattaneo, Mauricio; Gonzalez, Jonathan Sanchez; Bonesi, Sergio M.; Rodriguez, Juan B.: Synthetic and Mechanistic Studies on 2,3-Dihydrobenzo[b][1,4]-oxaselenines Formation from Selenocyanates

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paper

Kiran, Kuppalli R.; Swaroop, Toreshettahally R.; Rajeev, Narasimhamurthy; Anil, Seegehalli M.; Rangappa, Kanchugarakoppal S.; Sadashiva, Maralinganadoddi P.: Cyclization of Active Methylene Isocyanides with α-Oxodithioesters Induced by Base: An Expedient Synthesis of 4-Methylthio/Ethoxycarbonyl-5-acylthiazoles

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review

Zambroń, Bartosz K.: Internal Chelation within Functionalized Organoindium Reagents: Prospects for Regio- and Stereocontrol in the Allylation, Propargylation and Allenylation of Carbonyl Compounds

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Publication Date: 13 February 2020

paper

Arbuzova, Svetlana N.; Gusarova, Nina K.; Kazantseva, Tatyana I.; Verkhoturova, Svetlana I.; Zinchenko, Sergey V.; Kolyvanov, Nikita A.; Trofimov, Boris A.: Catalyst- and Solvent-Free Synthesis of α-Amino Polyfluoroalkylphosphonates from Bis(fluoroalkyl) Phosphonates and Aldimines

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paper

Dang, Minh-Huy Dinh; Nguyen, Linh Ho Thuy; Tran, Phuong Hoang: Sulfur/DABCO Promoted Reductive Coupling/Annulation Cascade Reaction between o-Hydroxy/Amino Nitrobenzenes and Benzaldehydes

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Publication Date: 12 February 2020

paper

Devi, Ngangbam Renubala; Shit, Sudip; Behera, Bipin Kumar; Saikia, Anil K.: Synthesis of 4-Vinyl-1,2,3,4-tetrahydroisoquinoline from N-Tethered Benzyl-Alkenol Catalyzed by Indium(III) Chloride: Formal Synthesis of (±)-Isocyclocelabenzine

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paper

Huang, Tiao; Liu, Li; Wang, Qinghe; Wu, Mingshu; Kong, Dulin: 1,3-Dipolar Cycloaddition of 3-Amino Oxindole-Based Azomethine Ylides and O-Vinylphosphonylated Salicylaldehydes for Diastereoselective Synthesis of Oxindole Spiro-P,N-polycyclic Heterocycles

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paper

Wang, Shuai; Kraus, George A.: The Dianion of Dehydroacetic Acid: A Direct Synthesis of Pogopyrone A

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Publication Date: 10 February 2020

feature

Li, Dong; Lv, Shujun; Qu, Jingping; Zhou, Yuhan: Oxidation of 4-Aryl-1,1,1-trifluorobut-2-en-2-yl Trifluoro­methanesulfonates by 4-Picoline-N-Oxide: A Novel Approach to β-Trifluoromethyl-α,β-enones

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paper

Liu, Jin; Jin, Shaofen; Zhou, Yingxing; Ni, Dongmei; Liu, Tingting; Cui, Bingcun; Hu, Gang; Yu, Xin; Huang, Guosheng: Palladium-Catalyzed ortho-Monoacylation of Arenes with Aldehydes­ via 1,2,4-Benzotriazine-Directed C–H Bond Activation

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paper

Qiu, Changfu; Yu, Heshui; Qiu, Chuanjiang; Li, Fangyi; Suo, Tongchuan; Wang, Chunhua; Bie, Songtao; Li, Zheng: Metal-Free Halogenation of N-Substituted Enaminoesters and Enaminones: A Facile Access to Functionalized α,α-Dihaloimines

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paper

Xue, Feng; Liu, Qibin; Zhu, Yong; Huang, Yifei; Ge, Jimeng; Wan, Boshun: Highly Enantioselective Rh-Catalyzed Arylation of N,N-Dimethylsulfamoyl-Protected Aldimines and Cyclic N-Sulfonylimines with Chiral Phenyl Backbone Sulfoxide-Olefin Ligands

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short review

Kuang, Guanghua; Liu, Guangyuan; Zhang, Xingxing; Lu, Naihao; Peng, Yiyuan; Xiao, Qiang; Zhou, Yirong: Directing-Group-Assisted Transition-Metal-Catalyzed Direct C–H Oxidative Annulation of Arenes with Alkynes for Facile Construction of Various Oxygen Heterocycles

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Publication Date: 06 February 2020

paper

Chow, Shiao; Green, Adam I.; Arter, Christopher; Liver, Samuel; Leggott, Abbie; Trask, Luke; Karageorgis, George; Warriner, Stuart; Nelson, Adam: Efficient Approaches for the Synthesis of Diverse α-Diazo Amides

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paper

Yavari, Issa; Khaledian, Omid: Copper-Catalyzed Tandem Dehydrocyanation and [3+2] Cyclo­addition Reactions of Phenacylmalononitriles: Regioselective Synthesis of Functionalized 4-Benzoyl-5-cyanopyrazoles under Mild Conditions

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Publication Date: 05 February 2020

paper

Chang, Caizhu; Geng, Jialin; Liu, Yinxin; Du, Yuguo; Liu, Jun; Dong, Zhi-Bing: Stereoselective Total Synthesis of Arundinolides A and B

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paper

Jin, Hongwei; Liu, Daohong; Zhou, Bingwei; Liu, Yunkui: One-Pot Copper-Catalyzed Three-Component Reaction of Sulfonyl Azides, Alkynes, and Allylamines To Access 2,3-Dihydro-1H-imi­dazo[1,2-a]indoles

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review

DaBell, Peter; Thomas, Stephen P.: Iron Catalysis in Target Synthesis

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short review

Zhu, Yannan; Huang, You: Organocatalyzed [3+3] Annulations for the Construction of Heterocycles

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Publication Date: 04 February 2020

paper

Han, Zhao; Lin, Xufeng: Synthesis of Chiral Tertiary Amine–Thioureas Based on Spirobi­indane and Application in Catalytic Asymmetric Michael Addition Reaction

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Publication Date: 03 February 2020

feature

Zhan, Fuxu; Zhang, Wei; Zhao, Huaiqing: Copper/Silver Cocatalyzed Regioselective C5–H Functionalization of 8-Aminoquinoline Amides with 1,3-Dicarbonyl Compounds

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paper

Vasilenko, Dmitry A.; Sadovnikov, Kirill S.; Sedenkova, Kseniya N.; Kurova, Anastasiya V.; Grishin, Yuri K.; Kuznetsova, Tamara S.; Rybakov, Victor B.; Volkova, Yulia A.; Averina, Elena B.: Synthesis of 4-Nitroisoxazoles via NO/NO₂-Mediated Heterocyclization of Aryl-Substituted α,β-Unsaturated Ketones

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Publication Date: 30 January 2020

feature

Gao, Qianwen; Liu, Ze-Shui; Hua, Yu; Zhou, Siwei; Cheng, Hong-Gang; Zhou, Qianghui: Alkyl Tosylates as Alkylating Reagents in the Catellani Reaction

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paper

Luo, Yang; Gao, Fei; Liu, Hong; Zhang, Fuyi; Zhao, Yufen: Facile Synthesis of Novel Benzoylthiophene C-Nucleoside Analogues via Coupling of Sugar Alkynes, Aroyl Chlorides, and 1,4-Dithiane-2,5-diol

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Publication Date: 29 January 2020

paper

Li, Yang; Guo, Hao; Fan, Renhua: Iodobenzene-Catalyzed Oxidative Cyclization for the Synthesis of Highly Functionalized Cyclopropanes

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paper

Rajbongshi, Kamal K.; Ambala, Srinivas; Govender, Thavendran; Kruger, Hendrik G.; Arvidsson, Per I.; Naicker, Tricia: Microwave-Accelerated N-Acylation of Sulfoximines with Aldehydes under Catalyst-Free Conditions

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Publication Date: 28 January 2020

paper

Dahlmann, Uwe; Vollhardt, K. Peter C.: Oligoether-Substituted Derivatives of Carbon-Rich 1,4,7,10,13,16-Hexaethynyltribenzo[a,e,i]cyclododeca-5,11,17-triyne (C₃₆H₁₂) and 1,4,9,12-Tetrakis(ethynyl)dibenzo[a,g]cyclododeca-5,7,13,15-tetrayne (C₂₈H₈): Potential Precursors to the Circular [6]Phenylene (‘Antikekulene’) Frame

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Publication Date: 27 January 2020

paper

Chang, Meng-Yang; Chen, Shin-Mei; Hsiao, Yu-Ting: One-Pot Access to 4-Aryl-2-arylacetoxynaphthalenes via Benz­annulation of Oxygenated Arylacetic Acids and Alkyl Aryl Ketones

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paper

Choi, Anthony; Castle, Jemma; Saruengkhanphasit, Rungroj; Coldham, Iain: Synthesis of Spirocyclic Amines by 1,3-Dipolar Cycloaddition of Azomethine Ylides and Azomethine Imines

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paper

Dar’in, Dmitry; Khoroshilova, Olesya; Kantin, Grigory; Krasavin, Mikhail: Realizing the Trifunctional Potential of Alkyl 4-Chloro-2-diazo-3-oxobutanoates: Convenient Assembly of 6,7-Dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]thiazine Core

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paper

Hussain, Mulla Althafh; Khan, Faiz Ahmed: Total Synthesis of (±)-Cassumunins A–C and Curcumin Analogues

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short review

Salom-Roig, Xavier; Bauder, Claude: Recent Applications in the Use of Sulfoxides as Chiral Auxiliaries for the Asymmetric Synthesis of Natural and Biologically Active Products

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Publication Date: 23 January 2020

paper

Naruto, Hiroki; Togo, Hideo: Preparation of 2-Arylquinolines from 2-Arylethyl Bromides and Aromatic Nitriles with Magnesium and N-Iodosuccinimide

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paper

Sereda, Grigoriy; Sarkar, Akash Mamon; Hussain, Anwar; Zefirov, Nikolai: Solvent-Free and Liquid-Phase Iodination of Thiophene Derivatives with Potassium Dichloroiodate Monohydrate

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Publication Date: 22 January 2020

paper

Su, Yingpeng; Liu, Xuan; Yu, Jie; Cao, Guiyan; Zhang, Rong; Zhao, Yanan; Huang, Danfeng; Wang, Ke-Hu; Huo, Congde; Hu, Yulai: Trichloroisocyanuric Acid Mediated Oxidative Dehydrogenation of Hydrazines­: A Practical Chemical Oxidation To Access Azo Compounds

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Publication Date: 21 January 2020

paper

Chikayuki, Yuya; Miyashige, Takakane; Yonekawa, Shiori; Kirita, Akiko; Matsuo, Natsuko; Teramoto, Hiroyoshi; Sasaki, Shigeru; Higashiyama, Kimio; Yamauchi, Takayasu: Transition-Metal-Free Synthesis of Pyridine Derivatives by Thermal Cyclization of N-Propargyl Enamines

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Publication Date: 15 January 2020

short review

Youn, So Won: Transition-Metal-Catalyzed Annulative Coupling Cascade for the Synthesis of 3-Methyleneisoindolin-1-ones

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Publication Date: 13 January 2020

paper

Linnemannstöns, Marvin; Neumann, Beate; Stammler, Hans-Georg; Mitzel, Norbert W.: Synthesis and Structural Diversity of Triaryl(phenylethyl)silanes

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Publication Date: 09 January 2020

paper

Liu, Yue; Zhang, Cheng; Liang, Xiaoxia; Zeng, Xianzhong; Lu, Rongmei; Fang, Zixuan; Wang, Shaoyu; Liu, Yanjun; Hu, Jinxing: Synthesis of 2-Imidazolines via Palladium-Catalyzed Cyclization Reaction of 2,3-Allenyl Amines and Aryl Iodides

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short review

Hsieh, Jen-Chieh; Su, Haw-Lih: Synthesis of N-Heterocycles via Transition-Metal-Catalyzed Tandem Addition/Cyclization of a Nitrile

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Publication Date: 08 January 2020

paper

Senoo, Takahiro; Inoue, Aiko; Mori, Keiji: Facile Synthesis of π-Conjugated Heteroaromatic Compounds via Weak-Base-Promoted Transition-Metal-Free C–N Coupling

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psp

Morra, Barbora; Morra, Nicholas A.; MacDonald, Daniel G.; Pagenkopf, Brian L.: Gram-Scale Synthesis of the Co(nmp)₂ Catalyst to Prepare trans-2,5-Disubstituted Tetrahydrofurans by the Aerobic Oxidative Cyclization of Pent-4-en-1-ols

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short review

Song, Si-Zhe; Dong, Youren; Ge, Guo-Ping; Li, Qiang; Wei, Wen-Ting: Recent Advances in Radical Nitration Using tert-Butyl Nitrite

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Publication Date: 03 January 2020

review

Reznikov, Alexander N.; Klimochkin, Yuri N.: Recent Developments in Highly Stereoselective Michael Addition Reactions Catalyzed by Metal Complexes

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Publication Date: 02 January 2020

paper

Gerasov, Andrii; Dolgonos, Grygoriy A.; Mandzhulo, Aleksandr Yu.; Ryabitsky, Alexey; Fetyukhin, Volodymyr; Lukin, Oleg; Shivanyuk, Alexander: Selective Synthesis of exo-Spiro[2′,2′-difluorocyclopropane-3′,2′-tropanes]

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paper

Luo, Zaigang; Han, Xinxin; Liu, Chenfu; Liu, Qiannan; Li, Rui; Liu, Peng; Xu, Xuemei: Catalyst-Free Synthesis of 1,4-Dihydroquinolines and Pyrrolo[1,2-a]quinolines via Intermolecular [4+2]/[3+2] Radical Cyclization of N-Methylanilines with Alkynoates

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Publication Date: 16 December 2019

paper

dos Santos, Deborah A.; da Silva, Allan R.; Ellena, Javier; da Silva, Cecilia C. P.; Paixão, Marcio W.; Corrêa, Arlene G.: Green One-Pot Asymmetric Synthesis of Peptidomimetics via Sequential Organocatalyzed Aziridination and Passerini Multicomponent Reaction

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paper

Zubenko, Anastasia D.; Shchukina, Anna A.; Fedorova, Olga A.: Synthetic Approaches to the Bifunctional Chelators for Radio­nuclides Based On Pyridine-Containing Azacrown Compounds

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Publication Date: 12 December 2019

paper

Bartolotta, Roberta; La Rosa, Concetta; Nava, Donatella: New Strategy of Synthesis of Peramivir Analogues as Potential Neuraminidase Inhibitors

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Publication Date: 10 December 2019

paper

Kohlhaas, Martha; Lutz, Fabian; Paransothy, Nirtharsan; Octa-Smolin, Frescilia; Wölper, Christoph; Niemeyer, Jochen: Synthesis of Bis-BINOL Derivatives: Linking via the 3-, 4-, or 5-Position by Generation of Suitable C₁-Symmetric Precursors

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Publication Date: 09 December 2019

paper

Lu, Hai-Long; Guo, Fu-Hu; Wang, Tong-Lin; Wang, Xi-Cun; Quan, Zheng-Jun: Palladium-Catalyzed/Copper-Mediated Desulfurization and Aryl­­ation of Quinoline-2-(1H)-thione for Rapid Access to Quinoline Derivatives

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Publication Date: 06 December 2019

paper

Skotnitzki, Juri; Kremsmair, Alexander; Kicin, Bilal; Saeb, Rakan; Ruf, Vincent; Knochel, Paul: Stereoselective anti-S_N2′-Substitutions of Secondary Alkylcopper-Zinc Reagents with Allylic Epoxides: Total Synthesis of (3S,6R,7S)-Zingiberenol

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Publication Date: 04 December 2019

paper

Dziuba, Kamil; Lubańska, Małgorzata; Pietrusiewicz, K. Michał: Enantiodivergent Synthesis of Both PAMPO Enantiomers Using l-Menthyl Chloroacetate and Stereomutation at P in Classical Quaternisation Reactions

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paper

Lee, Sumin; Jang, Young Jin; Phipps, Erik J. T.; Lei, Honghui; Rovis, Tomislav: Rhodium(III)-Catalyzed Three-Component 1,2-Diamination of Unactivated Terminal Alkenes

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Publication Date: 28 November 2019

paper

Chang, Meng-Yang; Chen, Kuan-Ting; Tsai, Yu-Lin; Chen, Han-Yu: One-Pot Access to 2-Aryl-3-(arylmethyl)chromones

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Publication Date: 26 November 2019

paper

Ban, Jaeyoung; Lim, Minkyung; Shabbir, Saira; Baek, Junghyun; Rhee, Hakjune: Site-Specific Synthesis of Carbazole Derivatives through Aryl Homocoupling and Amination

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paper

Ohsawa, Kosuke; Zhao, Hongbin; Tokunaga, Takuya; Thomas, Carys; Ganesan, A.; Masuda, Yuichi; Doi, Takayuki: Stereoselective Synthesis of Protected l-allo-Enduracididine and l-Enduracididine via Asymmetric Nitroaldol Reaction

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paper

Trubitsõn, Dmitri; Martõnova, Jevgenija; Erkman, Kristin; Metsala, Andrus; Saame, Jaan; Kõster, Kristjan; Järving, Ivar; Leito, Ivo; Kanger, Tõnis: Enantioselective N-Alkylation of Nitroindoles under Phase-Transfer Catalysis

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Publication Date: 14 November 2019

paper

Pruschinski, Lucas; Lücke, Ana-Luiza; Freese, Tyll; Kahnert, Sean-Ray; Mummel, Sebastian; Schmidt, Andreas: Suzuki–Miyaura Cross-Couplings under Acidic Conditions

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Publication Date: 07 November 2019

special topic

Shen, Zican; Li, Chen; Mercado, Brandon Q.; Ellman, Jonathan A.: Cobalt(III)-Catalyzed Diastereoselective Three-Component C–H Bond Addition to Butadiene and Activated Ketones

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Publication Date: 30 October 2019

special topic

Connon, Robert; Carroll, Laura; Guiry, Patrick J.: A Base-Promoted One-Pot Asymmetric Friedel–Crafts Alkylation/Michael Addition of 4-Substituted Indoles

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Publication Date: 29 October 2019

special topic

Yang, Yuzhong; Zhou, Liwei; Yang, Xiumei; Luo, Xiai; Deng, Guobo; Yang, Yuan; Liang, Yun: Synthesis of Phenanthrenes via Palladium-Catalyzed Three-Component Domino Reaction of Aryl Iodides, Internal Alkynes, and o-Bromobenzoic Acids

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Publication Date: 24 October 2019

paper

Sun, Manman; Li, Jinshan; Chen, Weida; Wu, Haijian; Yang, Jianguo; Wang, Zhiming: Palladium-Catalyzed [4+2] Annulation of Aryl and Alkenyl Carboxamides with 1,3-Dienes via C–H Functionalization: Synthesis of 3,4-Dihydroisoquinolones and 5,6-Dihydropyridinones

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Publication Date: 02 October 2019

paper

Henkel, Michael; Bach, Thorsten: Annulation of Indoles with 1,n-Dibromoalkanes by a Pd(II)-Catalyzed and Norbornene-Mediated Reaction Cascade

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