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Synlett 2001; 2001(5): 0597-0600
DOI: 10.1055/s-2001-13353
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Tandem Glycol Cleavage-Intramolecular [4 + 2] Cycloadditions Mediated by Dess-Martin periodinane

José Ignacio Candela Lena* , José Ignacio Martín Hernando, Maria del Rosario Rico Ferreira, Ertan Altinel, Siméon Arseniyadis
  • *Institut de Chimie des Substances Naturelles, CNRS, F-91198 Gif-sur-Yvette, France; Fax: 33-1-69 07 72 47; E-mail: Simeon.Arseniyadis@icsn.cnrs-gif.fr
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Publication Date:
31 December 2001 (online)

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The product distribution on oxidation of vicinal unsaturated diols using Dess-Martin periodinane (DMP) under various conditions is investigated. The process depends upon 1,2-diol-stereochemistry and constitutes a useful method for glycol fission offering molecular complexity.

oxidative cleavage - tandem reactions - Dess-Martin periodinane

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