Download PDF
Synthesis 2000; 2000(1): 67-68
DOI: 10.1055/s-2000-6239
short paper
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved. This journal, including all individual contributions and illustrations published therein, is legally protected by copyright for the duration of the copyright period. Any use, exploitation or commercialization outside the narrow limits set by copyright legislation, without the publisher's consent, is illegal and liable to criminal prosecution. This applies in particular to photostat reproduction, copying, cyclostyling, mimeographing or duplication of any kind, translating, preparation of microfilms, and electronic data processing and storage.

Efficient Method for Selective Cleavage of Acetals and Ketals Using Peroxymonosulfate on Alumina under Solvent-Free Conditions

D. Subhas Bose* , B. Jayalakshmi, A. Venkat Narsaiah
  • *Organic Chemistry Division III, Fine Chemicals Laboratory, Indian Institute of Chemical Technology, Hyderabad 500 007, India; Fax +91 (40) 7 17 33 87; E-mail: root@csiict.ren.nic.in
Further Information

Publication History

Publication Date:
31 December 2000 (online)

  PDF Download  Permissions and Reprints All articles of this category

In an environmentally benign solvent-free system, acetals and ketals are rapidly cleaved with peroxymonosulfate-alumina under microwave irradiation in high yields.

peroxymonosulfate - acetals - alumina - ketals - solid support - hydrolysis - protecting groups - microwaves - solvent-free conditions

      >