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Synthesis 1990; 1990(2): 104-106
DOI: 10.1055/s-1990-26799
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Improved Direct Preparation of O-Trimethylsilyl Monothioacetals from Thiols and Carbonyl Compounds

Mark B. Sassman* , G. K. Surya Prakash, George A. Olah
  • *Donald P. and Katherine B. Loker Hydrocarbon Reasearch Institut and Department of Chemistry, University of Southern California, Los Angeles, CA 90089-1661, USA
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Publication History

Publication Date:
17 September 2002 (online)

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Preparation of 1-alkylthio- or 1-phenylthio-1-trimethylsiloxyalkanes and-cycloalkanes directly from carbonyl compounds and thiols, is achieved using 1-trimethylsilylimidazole and trimethylsilyl triflate as a catalyst.

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