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Synthesis 1989; 1989(5): 400-402
DOI: 10.1055/s-1989-27267
DOI: 10.1055/s-1989-27267
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2-Azoniaallene Salts From the Reaction of Chlorocarbenium Salts with N-Silylimines
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Publication History
Publication Date:
17 September 2002 (online)
Chlorocarbenium hexachloroantimonates 1 react with N-silylimines 5 affording the 2-azoniaallene hexachloroantimonates 4 under mild conditions. The N-silylimine 5a reacts with phosgene to give a dicationic salt 7 with an interesting new structure.