Synfacts

Issue 09 · September 2024

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Synform
A135
SYNFORM ISSUE 2024/09
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Synthesis of Natural Products
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0895
Total Synthesis of (+)-Dihydropleurotinic Acid
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0896
Synthesis of (+)-Enteropeptin A

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0897
Total Synthesis of Sealutomicin C

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0898
Total Synthesis of (+)-Alstrostine G

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0899
Total Synthesis of (+)-Lirionol

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0900
Total Synthesis of (–)-Cyclopamine

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0901
First Synthesis of (±)-Retigeranic Acid
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Synthesis of Heterocycles
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0903
Bench-Stable Azabicyclo[2.1.1] Piperazinium Salt as a Versatile Synthetic Intermediate

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0904
Enzyme-Catalyzed Access to Spiro-Oxazolidinones

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0905
Photocatalyzed Enantioselective Access to Oxetanes

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0906
Synthesis of 2,3-Dihydrofuro[3,2-c]quinolines via Acid-Mediated Condensation

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0907
Versatile, Photochemical Approach to 2-Azanorbornanes

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0908
Carboxylic-Acid-Directed Cyclization of N-Protected ω-Amino Acids

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0909
Light-Mediated Deoxygenative Hydroalkylation of Olefins

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0910
Hectogram Scale Synthesis of Key Prostaglandin Synthesis Intermediate

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0911
Regioselective Difluoromethylation of Pyridines through Oxazino-pyridine Intermediates

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0912
Synthesis of 2,3-Diaroylquinolines via Copper-Catalyzed [4+1+1] Annulation

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0913
Modular Copper-Mediated Synthesis of Imidazolidines and Imidazolidinones

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0914
Three-Component Photochemical Construction of Trisubstituted Oxazoles

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0915
General Methodology for the α-Alkylation of Cyclic Ketones

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0916
Same Substrates, Different Products: Regiodivergent Cycloaddition Pathways to 1,2,3- and 1,3,4-Triazoles

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Synthesis of Materials and Unnatural Products
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0917
Enantioselective Syntheses of π-Extended Carbohelicenes
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0918
Spiro-Conjugated Chiral Radical Cations

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0919
Nucleophilic Perfluoroalkylation Facilitated by 4-Pyridylthioether

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0920
Backbone-Editing with Polyesters and Polyurethanes

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0921
Triple Suzuki–Miyaura Arylation via Cyclic Iodonium Salts

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0922
Joining Carborane with Arenes

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0923
‘Click’ Polymerization of Acetal-thiol

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0924
Cyclic Polymers with Ultrahigh Molar Mass

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0925
‘Cage of Cages’

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0926
Kinetic Resolution Polymerization

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0927
Single-Atom Skeletal Editing: Turning N into C

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0928
Isolable Secondary Carbon Radical

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Metals in Synthesis
z0929
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0929
Nickel- and Photocatalytic Enantioselective Alkylation of α-Amino C(sp³)–H Bonds
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0930
Atroposelective Reductive Coupling of Two ortho-Substituted Aryl Halides under Nickel Catalysis

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0931
Synthesis of Oximes by Nickel-Catalyzed Coupling of Nitrates with Organohalides
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0932
Palladium-Catalyzed Cascade Reaction to Fused Isoindolinones

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0933
Chromium-Catalyzed Enantioselective Addition of α-Chlorinated Esters and Amides to Aldehydes

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0934
Nickel-Catalyzed Cine-Substitution of Enolates

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0935
Enantioselective Synthesis of Highly Decorated Pyrrolidines Through a Zinc-Catalyzed [3+2] Reaction

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0936
Synthesis of Chiral Allylic Alcohols by Enantioselective Alkenylation of Aldehydes Under Cobalt Catalysis

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0937
Dearomative 1,2-Hydroamination of Nonactivated Arenes via Copper–Hydride Catalysis

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0938
Synthesis of Anilines by Ruthenium/η⁵-Phenoxo-Catalyzed Condensation of Phenols and Amines

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0939
Asymmetric Arylation of Enone Diesters Enabled by Synergistic Copper Catalysis

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0940
Selective Palladium Visible Light Catalyzed Ether/Esterification of Allylic C–H Bonds

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0941
Gold-Catalyzed Electrophilic Cyclopropenylation of Terminal Alkynes and Vinyl Boronic Acids

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0942
Nickel-Catalyzed α-anti-Hydroarylation of Arylpropiolic Acids and Arylboronic Acids

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0943
Asymmetric Aminooxygenation of 1,3-Dienes Enabled by Copper Catalysis

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0944
Copper-Catalyzed Borylative Cyclization of Unactivated Vinylcyclopropanes

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0945
Palladium-Catalyzed Chain-Walking of Alkynyl Alcohols to α,β-Unsaturated Carbonyls

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0946
Asymmetric β-Arylation of Aliphatic Alcohols by Merging Relay Catalysis and Dynamic Kinetic Resolution

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0947
Palladium-Catalyzed Spirocyclopropanation of gem-Difluoroalkenes

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0948
Enantioselective Rhodium-Catalyzed N²-Allylation of Indazoles with Dienyl Allylic Alcohols

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0949
Iridium-Catalyzed Allylation of Bis(alkenyl)boronates to Access Enantioenriched Tertiary Allylic Boronic Esters

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0950
Separation by Isomerization: Kinetic Resolution of N-Allylic Pyrazoles under Photoexcited Copper Catalysis

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0951
Semipinacol Rearrangement of Allylic Alcohols under Dual Photoredox and Cobalt Catalysis

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0952
Decarboxylative C(sp³)–O Coupling Enabled by an Iron Ligand-to-Metal Charge Transfer

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0953
Nickel/Photoredox-Catalyzed C(sp³)–H Alkenylation

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0954
Dearomative Carbonylative trans-1,2-Difunctionali-zation of Arenes via Chromium–Arene Complexes

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0955
Synthesis of anti-1,3-Diols: The Evans–Tishchenko Reaction
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Polymer-Supported Synthesis
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0957
Pd Nanoclusters Supported on N-Doped Carbon Spheres for Hydrogenation of Phenols and Benzoic Acids

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0958
Hydrogenation of Arenes at Room Temperature under 1 atm of Hydrogen Gas by Rh-Pd/C or Rh-Pt

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0959
Selective Hydrogenation of Aldehydes and Ketones under Syngas Using Au NPs Supported on CeO₂
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0960
Solvent-Free Aerobic Oxidation of C(sp³)–H by a Carbon- and PdO-Doped Nb₂O₅ Photocatalyst

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0961
Hydrogenation of Dinitroarenes Catalyzed by Pt Clusters on a Graphene Shell with a Diamond Core

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0962
Photocatalytic Thio/Selenocyanation of Indoles Using Lead-Free Cs₂AgBiBr₆ Double Perovskite MCs

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0963
Nickel-Catalyzed C(sp²)–S Cross-Coupling with mpg-CN under Blue LED Irradiation

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0964
Dehydrogenative Silacyclization with a Porous Polymer-Supported Iridium Catalyst

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0965
Catalytic Transfer Hydrogenation of Carbonyls by SILP-Supported Manganese Nanoparticles

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0966
Enantioselective [2+2] Cross-Photocycloaddition Using a Homochiral Metal–Organic Cage Reactor

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0967
Photocatalytic Oxidative Bromination of Arenes by Al₂O₃-Supported Perylenetetracarboxylic Dianhydride

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Organo- and Biocatalysis
z0969
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0969
Photocalatytic C–H Alkylation Enabled by a Zwitterionic Acridinium Amidate Catalyst
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0970
Asymmetric Synthesis of Seven-Membered N-Heterocycles and Carbocycles

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0971
Alcohol-Directed Functionalization of Remote C–H Bonds

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0972
Organocatalytic Asymmetric Epoxidation of Alkenyl Aza-Heteroarenes

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0973
Consecutive Photoinduced Electron Transfer Enables Asymmetric [3+2] Cycloadditions

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0974
Confined Acid Catalyzes the Enantioselective Hydroamination of Non-Activated Olefins

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0975
Solid-State Preorganization Enables Highly-Selective [2+2] Cycloaddition towards Truxillates

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0976
Organophotocatalytic Method for Synthesis of α-Amino Bicycloalkanes – Pharmaceutically Relevant Molecules

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0977
Synergistic Catalytic Asymmetric Decarboxylation of β-Keto Acids with Acyclic α-Arylenamides

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0978
Photoorganocatalytic Reduction of Esters to Alcohols

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Innovative Drug Discovery and Development
z0979
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0979
Synthesis and Medicinal Chemistry of Veragranine Alkaloids
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0980
Functionalization of Oxetanes with C/N/O/S Nucleophiles – Convenient Access to Carbonyl Isosteres

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0981
High-Throughput Access to Libraries of N-Acylsulfamide Derivatives, a Bioisostere of Carboxylic Acids
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0982
Amination of Arenes Using Blue Light and Lewis Acids

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0983
Vinylpyridine Based Covalent EGFR Inhibitors

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0984
Photochemical Conversion of Pyridines into Diazepines, Pyrazolines and Pyrazoles

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0985
Divergent Synthesis of 2- and 3-Azabicyclo[3.1.1]heptenes as Bioisosteres of Pyridines

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0986
Development of the Photoresponsive Drug via Caging Triarylimidazoles

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0987
An Eight-Step Total Syntheses of Clausenawallines A and E are Enabled by High-Throughput Experimentation

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0988
HRO761: a First-in-Class Non-Covalent WRN Inhibitor with Synthetic Lethality in MSI Cancers

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0989
A Modified Arbuzov–Michaelis Reaction for Chemoselective Alkylations

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0990
New Method for the Highly Enantioselective Synthesis of cis-Hydrobenzofurans and cis-Hydroindoles

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0991
Synthesis of a Selective Co-factor to Investigate Methyltransferase Activity

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0992
Subcellular Uncaging of H₂S and Drug with NIR Light

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0993
Diverse Synthesis of C‑Glycosides by Stereoselective Ni-Catalyzed Carboboration of Glycals

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0994
Expanding Chemical Space One Carbocycle at a Time

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Peptide Chemistry
z0995
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0995
N-Methylated Peptide Synthesis Using Flow Chemistry
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0996
α,α-Disubstituted Unnatural Amino Acid Synthesis Using Photochemical Carboxylation

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0997
Chiral Phenanthroline-Potassium-Catalyzed Synthesis of Axially Chiral Biaryl δ-Amino Acid Derivatives

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0998
Utilizing Cyclen Installation as an Efficient Strategy for Macrocyclization and Multifunctionality of Peptides

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0999
Synthesis of Proline Derivatives via [1,2]-Stevens Rearrangement of Azetidinium Salts

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1000
Synthesis of Unprotected α-Tertiary Amino Acids Using Synergistic Photoenzymatic Catalysis

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1001
Macrocyclic Thiazol(in)e Peptide Synthesis from Peptide Nitriles Using a Biocompatible Strategy

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1002
Electrochemical Modification of Tryptophan and Tryptophan-Containing Peptides

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1003
Tertiary Amine Catalyzed Late-Stage Tryptophan Allylation of Peptides

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1004
Synthesis of Functionalized Diketopiperazines

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1005
Photocatalyzed Synthesis of Unnatural α-Amino Acids

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1006
Asymmetric Synthesis of α,α-Disubstituted α-Amino Acid Esters via Tsuji–Trost Allylation

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1007
O-Hydroxybenzenesulfonyl Chloride Mediated Peptide Synthesis
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Flow Chemistry
z1009
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1009
Photocatalyst-, Oxidant-, Additive-Free Nitrosylation Using Continuous Flow/Photochemical Conditions

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