Synfacts

Issue 09 · September 2023

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A149
SYNFORM ISSUE 2023/09 FREE ACCESS

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Synthesis of Natural Products
z0849
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0849
Total Synthesis of (–)-Mitragynine Pseudoindoxyl

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0850
Synthesis of (–)-Caulamidine A

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0851
Synthesis of (+)-Malettinin C and (+)-Malettinin E FREE ACCESS

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0852
Total Synthesis of (–)-Retigeranic Acid A

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0853
Synthesis of (+)-Hinckdentine A

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0854
Synthesis of (+)-Asteriscanolide FREE ACCESS

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Synthesis of Heterocycles
z0855
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0855
Rh-Catalyzed Asymmetric Carbometallation to Access 3-Substituted Piperidines

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0856
Synthesis of Hybrid Scaffolds Featuring 4-Pyridine and 4-Piperidine Moieties

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0857
Cu-Mediated C(sp²)–H Elaboration of Benzylic Scaffolds

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0858
Copper-Catalyzed Synthesis of Axially Chiral Arylpyrroles via Atroposelective Cyclization of Diyne

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0859
One-Pot Synthesis of Pyrazolooxazines from 2,2-Dichlorovinylacetophenones

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0860
Efficient Exploration of Reaction Space to Optimize Sustainable Cu-Mediated Ullmann Couplings FREE ACCESS

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0861
Photocatalyzed Formate-Mediated Deoxygenation of Alcohols through Benzoate Ester Intermediates

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0862
Synthesis of Polysubstituted Furans via Electrocatalyzed Cyclization

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0863
Synthesis of Azabicyclic Systems through [3+2] Cycloaddition of Oxidopyridinium Ions

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0864
Versatile Synthesis of 4-Fluoropyrroles

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0865
Regioselective Synthesis of Isoxazoles from Ynones

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0866
Catalyst-Controlled [3+2] Cycloaddition for the Synthesis of endo- or exo-Substituted Pyrrolidines

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0867
Catalytic Asymmetric Synthesis of Morpholinones and Piperazinones via Domino Ring-Opening Cyclization

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Synthesis of Materials and Unnatural Products
z0869
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0869
Adamantane-Annulated Arenes

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0870
Synthesis of Boratatriptycene

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0871
Molecular Cage from Diradical Dimerization FREE ACCESS

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0872
A New Benzotrisazulene Synthesis

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0873
Arylquinoline from Three Components in One-Pot

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0874
One Stone, Two Birds: Versatile Grignard Reagent-Enabled Coupling for Advanced Arylamines and Biaryls

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0875
Aromatic C–C Bond Cleavage in a Curved π‑System of Aminocorannulene

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0876
A Helicene-Bridged Cyclophane

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0877
Synthesis of Tetraphenanthroporphyrins

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0878
A Self-Accelerated Polymerization

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0879
Tetraradical in Cyclic Paraphenylene

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0880
Facile 10- and 11-Membered Azalactam Synthesis

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Metals in Synthesis
z0881
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0881
Making Acid Chlorides from Olefins by Palladium-Catalyzed Regiodivergent Hydrochlorocarbonylation FREE ACCESS

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0882
Palladium-Catalyzed Synthesis of Polysubstituted Cyclopropanecarbonitriles

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0883
Rhodium Catalyzed Aryl C–H Functionalization with Nitroalkenes FREE ACCESS

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0884
Nickel-Catalyzed Alkenyl C(sp²)–H Functionalization via an Aryl-to-Vinyl 1,4-Nickel/Hydride Shift

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0885
Rh-Catalyzed Synthesis of Propargylic Sulfides via a [2,3]-Sigmatropic Rearrangement

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0886
Synthesis of Chiral meta-Arylated 2-Aryl Anilines via an Atroposelective Palladation Relay

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0887
Copper-Catalyzed Three-Component Carboesterification of Styrenes to Access Chiral γ-Butyrolactones

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0888
C(sp³)–H Functionalization Enabled by Hydrogen Atom Transfer with Tertiary Cyclopropyl Radicals

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0889
Palladium-Catalyzed Cross-Coupling of 2-Benzoylpyridine N-Oxides via C(sp²)–C(O) Bond Cleavage

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0890
Synergystic Catalysis Used Toward the Synthesis of Strychnan Alkaloids

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0891
Enantioselective Hydroamination of Cyclopropenes Catalyzed by Copper

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0892
Synthesis of β-N-Glycopyranosides via Palladium-Catalyzed Tsuji–Trost Amination

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0893
Synthesis of Imidazolidines by Copper-Catalyzed Formal (3+2) Cycloaddition of Aziridines and Diazetidines

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0894
Cyclization of Enynes by Iron-Catalyzed Hydrochlorination

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0895
Nickel-Catalyzed Synthesis of Hydrazides from O-Benzoylated Hydroxamates and Aryl/Aliphatic Amines

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0896
Nickel-Catalyzed Regioselective Allylic Alkylation of Unsymmetric Ketones at the Higher-Substituted α-Site

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0897
Palladium-Catalyzed Directed Regio- and Stereoselective 1,1-Diarylation of Alkenes

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0898
Dual Nickel/Photoredox-Catalyzed Regioselective β-Allylation of Silyl Enol Ethers

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0899
Regio- and Chemoselective Synthesis of Trisubstituted Allenes via a Pd-Catalyzed Three-Component Reaction

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0900
Chromium-Catalyzed Enantioselective Cyclopropanation of Terminal Olefins with gem-Dihaloalkanes

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0901
Aerobic α,β-Dehydrogenation of Lactams and Flavanones under Iron Catalysis

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0902
Rh-Catalyzed Regio- and Diastereoselective Synthesis of Difluorinated Cyclopentanes via a [3+2] Cycloaddition

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0903
Time-Dependent Synthesis of Spirocyclic Silacycles via Pd-Catalyzed Domino C–H Activation Reactions

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0904
Ru-Catalyzed Intermolecular [4+3] Cycloaddition of ortho-Quinone Methides with Carbonyl Ylides

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0905
The Overman Asymmetric Intramolecular Heck Reaction for the Synthesis of 3-Alkyl-3-Aryloxindoles FREE ACCESS

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0906
Asymmetric Alkylation of N‑Sulfonyl Ketimines

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0907
The Larock Indole Synthesis: Pd-Catalyzed Annulation of 2-Iodoaniline and Internal Alkyne Derivatives FREE ACCESS

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Polymer-Supported Synthesis
z0909
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0909
Electrochemical Allylation of Imines Promoted by Single-Atomic Zinc on Nitrogen-Doped Carbon FREE ACCESS

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0910
Selective Oxidation of Sulfides to Sulfoxides by a Nickel-Salphen Based Porous Organic Polymer Catalyst

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0911
Photocatalytic α-Alkynylation of Tertiary Amines by Copper-Doped Carbon Nitride

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0912
Photocatalytic Oxidative Hydroxylation of Arylboronic Acids to Phenols by a CdS-TiO₂ Nanohybrid

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0913
Photocatalytic Borylation, Silylation, Phosphorylation, and Thiolation Using a Metal–Organic Framework

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0914
Photocatalytic Olefination of Aldehydes with Benzyl Bromides Promoted by Quantum Dots

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0915
A Polyacrylonitrile Fiber-Supported Acid-Base Bifunctional Catalyst for the Henry Reaction

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0916
One-Pot Four-Component Synthesis of Substituted Imidazole Derivatives Using Magnetic Polyborate NPs

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0917
Photocatalytic C–N Bond Formation with Single Iron Atoms on Sulfur-Containing Carbon Nitride

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0918
Visible-Light-Induced Aerobic C=C Bond Cleavage of Vinylarenes Using CsPbBr₃

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Organo- and Biocatalysis
z0919
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0919
Photo-Organocatalyst Enables Reduction of C–F, C–Cl, and C–O Bonds

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0920
Asymmetric Dearomatization of N-Heteroarenes Catalyzed by a Multidentate Halogen-Bond Donor

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0921
Photocatalytic Radical Alkene Hydrogenation by Phosphine-Mediated Water Activation FREE ACCESS

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0922
NHC Catalysis Permits Regioselective C3–OH or C5–OH Acylation of Unprotected Nucleosides

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0923
Discovery of a General Catalyst for the Oxidative Desymmetrization of Structurally Diverse Diols

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0924
N-Triflyl Phosphoramide-Catalyzed Atroposelective C–C Cross-Coupling of 1-Azonaphthalenes

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0925
Chiral Phosphoric Acid-Catalyzed Asymmetric Synthesis of Remotely Chiral Naphthols and Naphthylamines

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0926
Transition-Metal-Free Synthesis of Bicyclo[2.1.1]hexan-2-ones – meta- and ortho-Benzene Bioisosteres

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0927
P(III)/P(V) Redox Catalysis Enables Isodesmic Deoxygenation of Phosphine Oxides

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Innovative Drug Discovery and Development
z0929
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0929
Discovery of Selective SYK Inhibitors by the Macrocyclization and Prodrug Approaches

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0930
pH-Switchable Phase-Transfer Agents for Impurity Purging from Biocatalytic Transformations

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0931
Bioinspired Total Synthesis and Bioactivity Evaluation of a Novel Sesquiterpene (–)-Adenophorone FREE ACCESS

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0932
Lewis Acid-Mediated Tagging of Bioactive Amides

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0933
Site-Specific Functionalization of RNA by a Ribozyme

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0934
Discovery of a Potent and Orally Bioavailable Keap1–Nrf2 PPI Inhibitor

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0935
The Influence of Variable Solvent Peroxide Levels on endo/exo-Selectivity

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0936
Modular Synthesis of Ligand-Directed Covalent Probes

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0937
Radio-Pharmaceutical Probe for ROS Self-Monitoring

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0938
New sp³-Rich Isosteres of the Phenyl Ring with Enhanced Physicochemical Properties

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0939
From Carboxylic Acid Derivatives to Ketones: Modular Ketone Synthesis via Catalytic Olefination

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0940
ortho-Substituted Cannabinoids Achieve Axial Chirality and Impact Receptors Affinity

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0941
SARS-CoV-2 Inhibitors from Synthetic Alotaketal C Analogs

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Peptide Chemistry
z0943
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0943
Peptide Elongation Using α-NCAs Both as Nucleophiles and Electrophiles FREE ACCESS

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0944
Cu-Catalyzed Late-Stage Functionalization of Glycine Derivatives and Glycine-Containing Peptides

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0945
Silver-Catalyzed Intermolecular [3+2] Cycloaddition for the Synthesis of Tetrazole-Fused Amino Acids

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0946
Pinnick Oxidation to Form 4-Substituted Proline

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0947
Amine Installation and Facilitated Peptide Elongation

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0948
Ir-Catalyzed Functionalization of Cysteine-Containing Peptides

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0949
Peptide Modification Using Ag-Catalyzed C–H Amination

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0950
Fluorous Sulfur-Containing Boronic Acid Catalyst for Amidation

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0951
Synthesis of Sterically Hindered Tripeptides Using a Modified Ugi Reaction FREE ACCESS

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0952
Cu-Catalyzed γ-Addition to Form Unnatural Amino Acid Bearing Allene Units

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Flow Chemistry
z0953
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0953
Rapid Access to Benzodiazepines Using Flow Chemistry

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0954
Transformation of Amides to Nitriles Catalyzed by CeO₂ in Continuous-Flow Synthesis

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