Synfacts

Ausgabe 05 · Mai 2021

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A66
SYNFORM ISSUE 2021/05 FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
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0477
Synthesis of (–)-Merrilactone A, (+)-Merrilactone B, and (–)-Anislactones A and B FREIER ZUGRIFF

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0478
Synthesis of GDC-0326

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0479
Synthesis of Delgocitinib FREIER ZUGRIFF

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0480
Total Syntheses of (–)-Daphenylline and (–)-Himalensine A

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0481
Synthesis of a Key Subunit of HIV-1 Protease Inhibitor Darunavir

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0482
Total Synthesis of (±) Cephanolides A, C, and D

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0483
Total Synthesis of (+)-Limaol

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0484
Synthesis of Atabecestat

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0485
Synthesis of a Key Subunit of HIV-1 Protease Inhibitor Darunavir

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0486
Total Synthesis of (+)-Stephadiamine

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0487
Synthesis of (+)-2-O-Deacetyl Plebedipenes A and C

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0488
Total Synthesis of (±)-Luciduline FREIER ZUGRIFF

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Synthesis of Heterocycles
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0489
Synthesis of Indolyl Cyclobutanones by Brønsted Acid Catalysis

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0490
Synthesis of 2-Fluoro-1-benzofurans from β,β-Difluoro-o-hydroxystyrenes by 5-endo-trig Cyclization

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0491
Explore Three-Dimensional Chemical Space with Triazolobenzodiazepines

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0492
Rhodium(III)-Catalyzed Synthesis of Thiobenzofurans

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0493
Atroposelective Synthesis of 2-Arylquinazolinones

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0494
Nickel-Catalyzed Electrochemical Cross-Coupling of Alcohols and Aryl Halides

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0495
Environmentally Friendly Achmatowicz Rearrangement

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0496
Synthesis of 2,4,6-Trisubstituted Pyridines from Methyl Ketones and Alkynones

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0497
Synthesis of Five-Membered Cyclic Sulfonamide (γ-Sultam) 4,4-Spirocycles

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0498
Synthesis of Bi(1,2,3-triazoles) by a Three-Component Reaction

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PDF (84 kb)
0499
One-Pot Synthesis of 2-Azaaryl Tetrahydroquinolines by a Base-Promoted Reaction

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0500
Synthesis of Heterocycles from Potassium Trifluoro(pyrimidin-4-yl)borate Salts FREIER ZUGRIFF

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Synthesis of Materials and Unnatural Products
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0501
Orthogonal Functional Group Interconversion

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0502
Preparation of Conjugated Azopolymer through Nitrene Dimerization

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0503
A New and Efficient Synthetic Route for Preparation of N-Arylphenothiazines

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0504
Synthesis of Tetratriazoliumethylene via Cationic Tetranuclear Mesoionic Carbene (MIC)-Ag(I) Complex

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0505
Arylene−Imidazolium Based Homopolymers and Copolymers for Anion Exchange Membranes

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0506
Expanding the DPP Family

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0507
Hydrogen Transfer Crosses the Rubicene

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0508
Marriage of Two Structures: Synthesis of an Azadioxa-planar Triphenylborane

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0509
Synthesis of Symmetric Conjugated Ladder-Type Polymers with Nitrogen Bridges

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0510
Radical Formation of Fused Quinoidal Dithiophene Helicenes

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0511
Supersized Indoles by Gold-Catalyzed [8+2]-Cycloadditions

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0512
Switchable Synthesis and Applications of 3-Thiosubstituted Pyrroles and Pyrrolines

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Metals in Synthesis
z0513
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0513
Negishi Cross-Couplings in Water and Deep Eutectic Solvents FREIER ZUGRIFF

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0514
Cobalt-Catalyzed Z-Selective Double Bond Transposition

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0515
Iridium-Catalyzed Z-Retentive Asymmetric Allylic Substitution Reactions FREIER ZUGRIFF

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0516
Nickel-Catalyzed Thioester Synthesis from Thiocarbonates

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0517
Palladium-Catalyzed Preparation of Anilines from Cyclohexanones

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0518
Dual Rh- and Sm-Catalyzed Enantioselective [4+3] Cycloaddition for the Construction of 1,3-Dioxepines

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0519
A Mild and Efficient Protocol for the Oxidation of Hydrazones to Diazo Compounds via Copper Catalysis

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0520
Carbonylative C–F Bond Functionalization of gem-Difluoroalkenes with Palladium and Copper Catalysis

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0521
Synthesis of β-Hydroxynitriles via Enantioselective Nickel-Catalyzed C–C Bond Formation

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0522
Palladium(II)-Catalyzed Enantioselective Desymmetrization Generating Carbazolones

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0523
Coupling of Alkynes with Cyclopropyl Ketones in a Samarium-Catalyzed Radical Relay

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0524
Ruthenium-Catalyzed Alkylation of Phosphines

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0525
Tungsten-Catalyzed SOMOphilic Alkynylations

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0526
Copper-Catalyzed Enantioselective α-Arylation of Silylenol Ethers Using Diaryliodonium Salts

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0527
Tandem Phosphine- and Pd-Catalyzed Michael–Heck Reaction for the Synthesis of Polyalkyl Furans

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PDF (88 kb)
0528
Enabling the Use of Alkyl Chlorides in Formal Mizoroki–Heck Couplings via Photoinduced Palladium Catalysis

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0529
Nickel-Catalyzed Intermolecular Cross-Electrophile Dialkylation of Alkynes

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0530
Gold-Catalyzed Asymmetric Addition of Unactivated Propargylic C–H Bonds to Aldehydes

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0531
Palladium/Copper Cooperative Catalysis for C–H Arylation of Five-Membered Heterocycles

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0532
C–C Bond Activation in Borylation of Cyclopropanes

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0533
Hydroaminoalkylation of Alkenes

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0534
Hydrosilane and Cesium Fluoride Triggered Aryne Formation and Subsequent Acylalkylation

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0535
ortho-C–H Oxygenation of Weakly Coordinating Amides and Ketones by Rhoda-Electrocatalysis

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0536
Hydrogenation via Ascorbic Acid and Cobalt-Photoredox Dual Catalysis

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PDF (75 kb)
0537
Carbon Nitride–Nickel Heterogeneous Photocatalyst for C–O Bond Formation

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0538
Photocatalyzed Deuteration of Carboxylic Acids

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0539
Asymmetric Arylation of α-Chlorosulfones

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PDF (90 kb)
0540
Nickel(0)-Catalyzed Bis-Silylation of Alkynes/Alkenes

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0541
The Fukuyama Cross-Coupling Reaction FREIER ZUGRIFF

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Polymer-Supported Synthesis
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0543
Benzylic C–H Borylation on Ceria-Supported Nickel Hydroxides FREIER ZUGRIFF

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0544
A Magnetic Cu–Phenylurazole Composite for Hydration of Nitriles and Reduction of -NCO, -NCS, and -NC Groups

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0545
A Titania-Supported Dual Single-Atom Catalyst for Chemoselective Hydrogenation

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0546
N-Arylation of 2-Aminopyridines with Arylboronic Acids Catalyzed by Cu on Phosphorus g-C₃N₄

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0547
Polymer-Supported Brønsted Acid Catalysts for Direct Esterification

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0548
Asymmetric Conjugate Addition to Nitrostyrenes Catalyzed by Ni on a Diamine–Sulfonate Copolymer

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0549
Synthesis of N-Benzyl Amides by C–H Arylation Catalyzed by Carbon Nitride and Nickel

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0550
C–N Coupling Reaction with a Quinoxaline-Based Porous Organic Polymer-Supported Copper Catalyst

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0551
Hydrosilylation of Alkenes and Alkynes Catalyzed by Platinum Supported on Carbon Nanotubes

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0552
Suzuki–Miyaura Coupling on Palladium–Tellurium Nanoparticles

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PDF (99 kb)
0553
Meerwein–Ponndorf–Verley Reduction of Aldehydes and Ketones on a Zirconium Organoborate

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0554
Photocatalytic Oxidative Amidation of Alcohols on Cu–N–TiO₂ under Visible-Light Irradiation

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PDF (87 kb)
0555
Hydrogenation of Alkenes in Water by Using Pd-PW₁₁/ZrO₂

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PDF (66 kb)
0556
Polymer-Supported Photocatalysts Bearing Phenothiazine and Tris(2,2′-bipyridyl)ruthenium

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Organo- and Biocatalysis
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0557
Intermolecular Abiological Hetero-Diels–Alder Reaction Catalyzed by an Artificial Metalloenzyme

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PDF (91 kb)
0558
Photoexcited Anthraquinone Permits C–H Pyridylation of Simple Nonactivated Hydrocarbons

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0559
Chiral Phosphoric Acid Catalysts Can Control the Stereoselectivity of Nucleoside Phosphitylations

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0560
Catalytic Asymmetric Fischer Indolization by Desymmetrization of Cyclopentane-1,3-diones

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PDF (86 kb)
0561
Enzymatic Zinc Hydrides Expand New-to-Nature Toolbox

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PDF (81 kb)
0562
Novel P-Stereogenic Organocatalysts Permit Desymmetrizing Enantioselective Reduction

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0563
Imine Reductase-Catalyzed Reductive Amination of α-Keto Esters Yields N-Substituted α-Amino Esters

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0564
Making Primary Amine Synthesis Simple: Photocatalytic Olefin Hydroamination

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0565
Catalytic Asymmetric Aminomethylation of Bis-Silyl Ketene Acetals to β²-Amino Acids

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0566
Organocatalytic Selective Depolymerization of Mixed Plastics

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Chemistry in Medicine and Biology
z0567
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0567
Targeted Tumor Therapy via Extracellular Calcification

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PDF (89 kb)
0568
EC5026, an Analgesic Without the Addictive Potential of Opioids

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PDF (71 kb)
0569
Synthesis of cis-Aminopiperidine by Asymmetric Hydrogenation

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PDF (90 kb)
0570
BET Bromodomain Inhibitors Promote Wound Healing

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PDF (108 kb)
0571
Toward Catalytic Antibiotics

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PDF (184 kb)
0572
A New Approach for the Synthesis of Covalent Inhibitor Libraries FREIER ZUGRIFF

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0573
Discovery of LYS006, an Inhibitor of Leukotriene A₄ Hydrolase for the Treatment of Inflammatory Diseases

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0574
Targeting Mutant BRAF with PROTACs

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PDF (77 kb)
0575
Enantioselective Diacetoxylation of Terminal Alkenes

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PDF (70 kb)
0576
E7766, a Novel Interferon Genes (STING) Agonist

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PDF (78 kb)
0577
The First Total Synthesis of Cocaine FREIER ZUGRIFF

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PDF (134 kb)
0578
Synthesis of (±)-Uvaridacol L: An Antiausterity Agent

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Peptide Chemistry
z0579
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0579
Catalytic Intramolecular C–H Alkylation for the Synthesis of Peptide Macrocycles FREIER ZUGRIFF

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PDF (127 kb)
0580
Phase-Transfer-Catalyzed Synthesis of 4-Cyanotryptophan

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PDF (76 kb)
0581
Palladium-Catalyzed Intramolecular Peptide Macrocyclization

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PDF (98 kb)
0582
Synthesis of α-Sulfanyl-β-Amino Acids by a Mannich-Type Reaction

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PDF (98 kb)
0583
[3+2] Photocycloaddition of a Cyclopropylurea with α-Substituted Acrylates

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PDF (100 kb)
0584
Visible-Light Photoredox-Catalyzed Redox-Neutral Carbocarboxylation of Activated Alkenes

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PDF (92 kb)
0585
Organophotoredox and Hydrogen Atom Transfer Catalysis for the Synthesis of β-Silyl α-Amino Acids

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PDF (93 kb)
0586
Palladium/Copper Catalysis to Access α-Amino Esters

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PDF (95 kb)
0587
Thiopyridone-Derived Reagents for Peptide Coupling Reactions FREIER ZUGRIFF

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PDF (118 kb)
Flow Chemistry
z0589
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PDF (212 kb)
0589
Catalytic Si–H Functionalization in Flow

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PDF (81 kb)
0590
UV-Mediated Synthesis of 1,3,4-Oxadiazoles in Flow

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PDF (83 kb)
0591
Improved Flow Synthesis of Remdesivir

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PDF (80 kb)
0592
Zirconium Oxide Catalyzed Amidation Reactions Using Unactivated Esters in Flow

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PDF (76 kb)
0593
Generation and Use of Pyrylium Tetrafluoroborates in Polymerization under Continuous-Flow Conditions

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PDF (80 kb)
0594
Synthesis of Primary Amides by Site-Selective Hydrolysis

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PDF (74 kb)
0595
Photocatalytic Hydrocarboxylation in Flow for β-Lactone Synthesis

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PDF (102 kb)
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