Synfacts
Issue 07 · July 2019
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A97
SYNFORM
ISSUE 2019/07
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Synthesis of Natural Products and Potential Drugs
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Total Synthesis of (+)-Flavisiamine F
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Synthesis of an HCV NS5B RNA Polymerase Inhibitor
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Synthesis of AZD7594
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Synthesis of GSK8175
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Synthesis of Cephalotaxus Alkaloids
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Synthesis of a HCV NS5B Nucleoside Polymerase Inhibitor
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0706
Synthesis of a BACE 1 Inhibitor
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0707
Synthesis of (–)-Himalensine A
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0708
Synthesis of Dasabuvir
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0709
Synthesis of (+)-Biotin
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0710
Synthesis of BMS-919373
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0711
Synthesis of Tesirine
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0712
Synthesis of (±)-Phalarine
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0713
Synthesis of ABBV-168
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0714
Synthesis of Speradine C
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0715
Synthesis of AMG 232
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0716
Synthesis of Veliparib
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0717
Synthesis of GDC-0908
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0718
Synthesis of Venetoclax
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0719
Synthesis of BMS-911543
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0720
Syntheses of (+)-Pseudopteroxazole and (+)-Ileabethoxazole
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Synthesis of Heterocycles
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0721
Bithiophenes as a New Class of Organic Photoredox Catalysts
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0722
Programable Synthesis of Polyspirocyclic Heterocycles
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0723
Combined Electrochemical and Photochemical Syntheses of Pyrrolidines and Oxazolines
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0724
Synthesis of 1,3,4-Thiadiazines from Fluorinated Nitrile Imines and Thiols
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0725
Synthesis of Pyrazoles by a Silver-Mediated [3+2]-Cycloaddition Reaction
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0726
Rhodium(III)-Catalyzed Synthesis of (2
H
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0727
Synthesis of Fused Indoline–Cyclobutanone Derivatives
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0728
Decarboxylative Fluorination of Pyridin-2-ylacetates
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0729
Synthesis of 5,5-Disubstituted Hydantoins
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0730
Copper-Catalyzed Synthesis of Substituted Indoles and Benzoindoles
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0731
Base-Catalyzed Annulation for the Synthesis of Pterocarpene Analogues
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0732
Azepines by Palladium-Catalyzed C–H Activation and Isocyanide Insertion
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0733
Silver-Catalyzed Synthesis of 4-Trifluoromethyl-1,2,3-triazolines
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0734
Manganese-Catalyzed Selective C–H Alkylation of Imidazopyridines
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0735
Thiomorpholine Synthesis by a Copper-Catalyzed Three-Component Reaction
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Synthesis of Materials and Unnatural Products
z0737
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0737
Devising Rules of Thumb for a Bis(tetrathiofulvalene) Molecular Switch
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0738
Accio
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0739
Ladder to Conjugation
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0740
Can’t Buy These Earrings at Tiffany’s
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0741
Pyrazolyl Heptazine, You Make It Easy!
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0742
Sustainable Polymers Just Got a Little Bit Sweeter
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0743
A Short Route to BN-Heteroarenes
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0744
BN-Embedded PAHs Functionalized in Crossed Directions
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0745
Stitching to Make Substituted Fluorenes
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0746
DCPP-Based Bowl-Shaped Hydrocarbons
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0747
A Linear Nonacene Analogue
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0748
Towards 3D Semiconducting Nanostructures
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Metals in Synthesis
z0749
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0749
Palladium-Catalyzed Generation of C1 Ammonium Enolates
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0750
Iron-Catalyzed Thiolation of Azetidines
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0751
Di- and Tri-substituted Alkenyl Nitriles
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0752
Copper-Catalyzed Enantioselective Cyanofluoroalkylation of Alkenes Induced by Visible Light
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0753
Enantioselective Copper-Catalyzed Diels–Alder Cycloaddition
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0754
Photoredox-Catalyzed Trifluoromethylation
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0755
Photoredox-Catalyzed Hydroamidation of Olefins
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0756
Asymmetric Light-Mediated Radical Cyanation
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0757
Tele-Nucleophilic Substitution
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0758
P
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0759
Preparation of Branched/Linear Ketones via a Regiodivergent Rhodium-Catalyzed Reductive Coupling
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0760
Regio- and Enantioselective Indole Allylation
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0761
Synthesis of Ketones, Alcohols, and Amines by Anionic Chemistry
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0762
Mechanism-Based Optimization of the Palladium-Catalyzed Amination of Aryl Triflates
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0763
Enantioselective Allylic Alkylation of β,α-Unsaturated α-Amino Nitriles
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0764
Copper-Catalyzed Allylation of Imines via Umpolung
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0765
Functionalization of C–H Bonds of Aliphatic Alcohols
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0766
Light-Mediated Ruthenium-Catalyzed Olefin Metathesis
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0767
Rhodium(III)-Catalyzed Cyclopropanation of Allylic Alcohols
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0768
Enantioselective Rhodium-Catalyzed Synthesis of C–N Axially Chiral
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0769
Dual-Catalyzed Dihydrofunctionalization of Terminal Alyknes
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0770
Iridium-Catalyzed Enantioselective C(sp
3
)–H Amidation
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0771
Axially Chiral Biaryl Compounds via Cu-Catalyzed Acyloxylations of Cyclic Diaryliodonium Salts
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0772
ortho
-Thiolation via the Catellani Reaction
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0773
Asymmetric Synthesis of Alkyl Fluorides
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0774
Rhodium-Catalyzed Transfer Hydroformylation of Alkynes
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0775
The Birch Reduction
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0776
Palladium-Catalyzed
syn
-Hydrocarboxylation of Alkynes Utilizing Hydroxy Groups
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0777
Enantioselective Rhodium-Catalyzed Benzylic C(sp
3
)–H Amination
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Polymer-Supported Synthesis
z0779
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0779
Co-Synthesis of Glycolic Acids, Formamides, and Formates on Copper/Alumina
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0780
α-Alkylation of β-Diketones with Alkenes or Alcohols on Graphene Oxide
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0781
Synthesis of 1,2,4-Triazoles on Mesoporous Silica-Supported Copper(I) Bromide
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0782
Cadmium Sulfide Photocatalyzed Nickel-Mediated C–O and C–N Coupling of Aryl Bromides
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0783
Cobalt-Catalyzed C–H Sulfonylation of Tetrahydroquinoxalines
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0784
Cobalt-Catalyzed Reductive Coupling of Nitroarenes with Alcohols
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0785
Dehydrogenative Silylation of Terminal Alkynes on AuPd Nanoalloys
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0786
Self-Assembled Polymeric Pyridine–Copper Catalyst for Huisgen Cycloaddition
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0787
Synthesis of Triarylpyridines on an Iron–Organic Framework
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0788
Hydroarylation of Alkynes and Alkenes Catalyzed by Alumina-Sulfuric Acid
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0789
γ-Lactam Synthesis by Reductive Amination of Ethyl Levulinate on AuPd Nanoparticles
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0790
Pd/C-Catalyzed Reductive N-Methylation of Quinolines
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Organo- and Biocatalysis
z0791
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0791
Phosphine/Iodide-Based Photoredox-Catalyzed Decarboxylative Alkylations
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0792
Chiral Brønsted Acid-Catalyzed Direct Reductive Amination with Silanes
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0793
Phthalidyl Ester Prodrugs by Catalytic Asymmetric Acetalization of Carboxylic Acids
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0794
Synthesis of Tricyclic Scaffolds through Photochemical and Prins–Ritter Reactions
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0795
Machine Learning-Assisted Directed Evolution of Proteins
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0796
An Enzyme-Catalyzed Inverse-Electron-Demand Diels–Alder Reaction
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0797
Regioselective Vinylogous Aldol Condensation of α,β-Unsaturated Aldehydes
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0798
Toward Chiral 1,4-Enynes: Asymmetric Alkenylation of Propargyl Alcohols
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0799
Catalytic Asymmetric Alkylations via Phase-Transfer Catalysis
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0800
Organocatalytic Baeyer–Villiger Oxidation for the Synthesis of Prostaglandins
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0801
Cyclization of 2-Methylene-2
H
-indols with
ortho
-Quinone Methides Generated In Situ
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Chemistry in Medicine and Biology
z0803
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0803
An in Vivo Mass Cytometry Probe for Protein Translation
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0804
Sulfonium Sugars with Antidiabetic Activities
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0805
Synthesis of the Smallest Cyclodextrins
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0806
Sphingosine-1-phosphate Photopharmacology
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0807
Optical Control of Cardiac Function
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0808
C–H Activation and Decarboxylative Cross-Coupling of Carboxylic Acids
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0809
Targeting Myc through Stabilization of the Max Homodimer
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0810
Activity-Based Profiling of Bile Salt Hydrolases
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0811
The First Method to Sequence DNA
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0812
A Route to Complex N
-
Arylated Alkylamines via Photocatalytic C–H Amination
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0813
Optimizing Triarylborane Fluorophores for Biological Applications
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0814
Bioinspired Histidine Bioconjugation
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Peptide Chemistry
z0815
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0815
Synthesis of Disubstituted Peptidoisoxazoles
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0816
Organcatalysis for the Synthesis of α,α-Difluoro-β-Amino Amides
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0817
Photoredox-Catalyzed Decarboxylative Alkynylation of Peptides
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0818
Cooperative Catalysis for Enantioselective α-Allylic Alkylation
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0819
Peptide C(sp
2
)–O Cross-Coupling by Nickel/Photoredox Dual Catalysis
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0820
Photocatalyzed Efficient Synthesis of
C
-Glycoamino Acids
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0821
Efficient Peptide Coupling for the Total Synthesis of Echinocandins
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0822
Zn/Cu(OTf)
2
-Mediated 1,4-Addition of Alkyl/Aryl Halides to Dehydroalanine
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0823
β-Aryl-β-pyrazolyl α-Amino Acid Synthesis by Copper Catalysis
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0824
Copper-Catalyzed 1,4-Reduction of
N
-Aryl β-Enamino Esters
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0825
Total Synthesis of the Cyclic Tetrapeptide Pseudoxylallemycin A
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0826
Construction of Peptide Linkages by Using Sulfuryl Fluoride
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Flow Chemistry
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0827
A Rapid Flow Synthesis of Linezolid
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0828
Scandium-Catalyzed Electrochemical Intramolecular Cross-Coupling
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0829
Continuous-Flow Diastereoselective Synthesis of Substituted Tetrahydrofurans
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0830
Ynones and Pyrazoles in Continuous Flow
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0831
Thermolytic Deprotection of
N
-Boc Groups
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0832
Continuous-Flow Production of 5-(Hydroxymethyl)furfural
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