Synfacts

Issue 07 · July 2019

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A97
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Synthesis of (±)-Phalarine

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Bithiophenes as a New Class of Organic Photoredox Catalysts

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0725
Synthesis of Pyrazoles by a Silver-Mediated [3+2]-Cycloaddition Reaction

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0726
Rhodium(III)-Catalyzed Synthesis of (2H)-Indazoles from Azobenzenes

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0727
Synthesis of Fused Indoline–Cyclobutanone Derivatives

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0728
Decarboxylative Fluorination of Pyridin-2-ylacetates

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Synthesis of 5,5-Disubstituted Hydantoins

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Copper-Catalyzed Synthesis of Substituted Indoles and Benzoindoles

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0731
Base-Catalyzed Annulation for the Synthesis of Pterocarpene Analogues

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0732
Azepines by Palladium-Catalyzed C–H Activation and Isocyanide Insertion

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0733
Silver-Catalyzed Synthesis of 4-Trifluoromethyl-1,2,3-triazolines

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0734
Manganese-Catalyzed Selective C–H Alkylation of Imidazopyridines

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0735
Thiomorpholine Synthesis by a Copper-Catalyzed Three-Component Reaction

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Synthesis of Materials and Unnatural Products
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0737
Devising Rules of Thumb for a Bis(tetrathiofulvalene) Molecular Switch

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Accio peri-Acenoacenes

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0739
Ladder to Conjugation

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0740
Can’t Buy These Earrings at Tiffany’s

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0741
Pyrazolyl Heptazine, You Make It Easy!

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0742
Sustainable Polymers Just Got a Little Bit Sweeter

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0743
A Short Route to BN-Heteroarenes

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0744
BN-Embedded PAHs Functionalized in Crossed Directions

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0745
Stitching to Make Substituted Fluorenes

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0746
DCPP-Based Bowl-Shaped Hydrocarbons

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A Linear Nonacene Analogue

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0748
Towards 3D Semiconducting Nanostructures

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0749
Palladium-Catalyzed Generation of C1 Ammonium Enolates FREE ACCESS

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Iron-Catalyzed Thiolation of Azetidines

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0751
Di- and Tri-substituted Alkenyl Nitriles FREE ACCESS

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0752
Copper-Catalyzed Enantioselective Cyanofluoroalkylation of Alkenes Induced by Visible Light

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0753
Enantioselective Copper-Catalyzed Diels–Alder Cycloaddition FREE ACCESS

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0754
Photoredox-Catalyzed Trifluoromethylation

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Photoredox-Catalyzed Hydroamidation of Olefins

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0756
Asymmetric Light-Mediated Radical Cyanation

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Tele-Nucleophilic Substitution

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0758
P-Stereogenic Centers via Thulium(III)-Catalyzed Desymmetrization of Dialkynylphosphine Oxides

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Preparation of Branched/Linear Ketones via a Regiodivergent Rhodium-Catalyzed Reductive Coupling

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Regio- and Enantioselective Indole Allylation

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Synthesis of Ketones, Alcohols, and Amines by Anionic Chemistry

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0762
Mechanism-Based Optimization of the Palladium-Catalyzed Amination of Aryl Triflates

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Enantioselective Allylic Alkylation of β,α-Unsaturated α-Amino Nitriles

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Copper-Catalyzed Allylation of Imines via Umpolung

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0765
Functionalization of C–H Bonds of Aliphatic Alcohols

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Light-Mediated Ruthenium-Catalyzed Olefin Metathesis

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Rhodium(III)-Catalyzed Cyclopropanation of Allylic Alcohols

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Enantioselective Rhodium-Catalyzed Synthesis of C–N Axially Chiral N-Aryloxindoles

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Dual-Catalyzed Dihydrofunctionalization of Terminal Alyknes

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Iridium-Catalyzed Enantioselective C(sp³)–H Amidation

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Axially Chiral Biaryl Compounds via Cu-Catalyzed Acyloxylations of Cyclic Diaryliodonium Salts

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0772
ortho-Thiolation via the Catellani Reaction

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0773
Asymmetric Synthesis of Alkyl Fluorides

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0774
Rhodium-Catalyzed Transfer Hydroformylation of Alkynes

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0775
The Birch Reduction FREE ACCESS

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0776
Palladium-Catalyzed syn-Hydrocarboxylation of Alkynes Utilizing Hydroxy Groups

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0777
Enantioselective Rhodium-Catalyzed Benzylic C(sp³)–H Amination

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Polymer-Supported Synthesis
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0779
Co-Synthesis of Glycolic Acids, Formamides, and Formates on Copper/Alumina FREE ACCESS

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0780
α-Alkylation of β-Diketones with Alkenes or Alcohols on Graphene Oxide

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0781
Synthesis of 1,2,4-Triazoles on Mesoporous Silica-Supported Copper(I) Bromide

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0782
Cadmium Sulfide Photocatalyzed Nickel-Mediated C–O and C–N Coupling of Aryl Bromides

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0783
Cobalt-Catalyzed C–H Sulfonylation of Tetrahydroquinoxalines

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0784
Cobalt-Catalyzed Reductive Coupling of Nitroarenes with Alcohols

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0785
Dehydrogenative Silylation of Terminal Alkynes on AuPd Nanoalloys

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0786
Self-Assembled Polymeric Pyridine–Copper Catalyst for Huisgen Cycloaddition

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0787
Synthesis of Triarylpyridines on an Iron–Organic Framework

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0788
Hydroarylation of Alkynes and Alkenes Catalyzed by Alumina-Sulfuric Acid

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0789
γ-Lactam Synthesis by Reductive Amination of Ethyl Levulinate on AuPd Nanoparticles

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0790
Pd/C-Catalyzed Reductive N-Methylation of Quinolines

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Organo- and Biocatalysis
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0791
Phosphine/Iodide-Based Photoredox-Catalyzed Decarboxylative Alkylations

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0792
Chiral Brønsted Acid-Catalyzed Direct Reductive Amination with Silanes

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0793
Phthalidyl Ester Prodrugs by Catalytic Asymmetric Acetalization of Carboxylic Acids FREE ACCESS

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0794
Synthesis of Tricyclic Scaffolds through Photochemical and Prins–Ritter Reactions

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0795
Machine Learning-Assisted Directed Evolution of Proteins

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0796
An Enzyme-Catalyzed Inverse-Electron-Demand Diels–Alder Reaction

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0797
Regioselective Vinylogous Aldol Condensation of α,β-Unsaturated Aldehydes

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0798
Toward Chiral 1,4-Enynes: Asymmetric Alkenylation of Propargyl Alcohols

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0799
Catalytic Asymmetric Alkylations via Phase-Transfer Catalysis FREE ACCESS

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0800
Organocatalytic Baeyer–Villiger Oxidation for the Synthesis of Prostaglandins

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0801
Cyclization of 2-Methylene-2H-indols with ortho-Quinone Methides Generated In Situ

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Chemistry in Medicine and Biology
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An in Vivo Mass Cytometry Probe for Protein Translation FREE ACCESS

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0804
Sulfonium Sugars with Antidiabetic Activities

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0805
Synthesis of the Smallest Cyclodextrins

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0806
Sphingosine-1-phosphate Photopharmacology

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0807
Optical Control of Cardiac Function

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0808
C–H Activation and Decarboxylative Cross-Coupling of Carboxylic Acids

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0809
Targeting Myc through Stabilization of the Max Homodimer

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0810
Activity-Based Profiling of Bile Salt Hydrolases

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0811
The First Method to Sequence DNA FREE ACCESS

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0812
A Route to Complex N-Arylated Alkylamines via Photocatalytic C–H Amination

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0813
Optimizing Triarylborane Fluorophores for Biological Applications

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0814
Bioinspired Histidine Bioconjugation

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Peptide Chemistry
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0815
Synthesis of Disubstituted Peptidoisoxazoles

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0816
Organcatalysis for the Synthesis of α,α-Difluoro-β-Amino Amides

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0817
Photoredox-Catalyzed Decarboxylative Alkynylation of Peptides FREE ACCESS

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0818
Cooperative Catalysis for Enantioselective α-Allylic Alkylation

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0819
Peptide C(sp²)–O Cross-Coupling by Nickel/Photoredox Dual Catalysis

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0820
Photocatalyzed Efficient Synthesis of C-Glycoamino Acids

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0821
Efficient Peptide Coupling for the Total Synthesis of Echinocandins

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0822
Zn/Cu(OTf)₂-Mediated 1,4-Addition of Alkyl/Aryl Halides to Dehydroalanine

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0823
β-Aryl-β-pyrazolyl α-Amino Acid Synthesis by Copper Catalysis

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0824
Copper-Catalyzed 1,4-Reduction of N-Aryl β-Enamino Esters

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0825
Total Synthesis of the Cyclic Tetrapeptide Pseudoxylallemycin A

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0826
Construction of Peptide Linkages by Using Sulfuryl Fluoride

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Flow Chemistry
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0827
A Rapid Flow Synthesis of Linezolid

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0828
Scandium-Catalyzed Electrochemical Intramolecular Cross-Coupling

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0829
Continuous-Flow Diastereoselective Synthesis of Substituted Tetrahydrofurans

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0830
Ynones and Pyrazoles in Continuous Flow

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0831
Thermolytic Deprotection of N-Boc Groups

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0832
Continuous-Flow Production of 5-(Hydroxymethyl)furfural

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