Synfacts

Issue 11 · November 2015

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SYNFORM ISSUE 2015/11 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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1121
Boron-Catalyzed N-Alkylation of Amines Using Carboxylic Acids FREE ACCESS

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1122
Total Synthesis of Fijiolide A

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1123
Total Synthesis of Epicolactone FREE ACCESS

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1124
Synthesis of Cinacalcet by Asymmetric Hydroamination

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1125
Synthesis of a Squaramide-Based CXCR2 Receptor Antagonist

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1126
Synthesis of a Tetracyclic Indolenine that Represses β-Lactam Resistance

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1127
Synthesis of Verruculogen and Fumitremorgin A

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1128
Syntheses of (−)-Leucoridines A and C

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1129
Synthesis of (+)-Rubriflordilactone A

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1130
Synthesis of Hyperforin

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1131
Total Synthesis of Multifidosides A–C

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1132
Synthesis of BACE1 Inhibitors

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Synthesis of Heterocycles
z1133
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1133
Synthesis of Spiroxindoles by Enantioselective [3+2] Annulation

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1134
Efficient Synthesis of 5-Nitro-7-azaindole on a Kilogram Scale

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1135
Substituted 7-Azaindoles by Directed Ortho Metalation/Nucleophilic Aromatic Substitution

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1136
Synthesis of Polyfunctionalized 1,4,2-Oxathiazoles by Oxidative Cyclization

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1137
Dihydroisocoumarin Synthesis by C–H ortho-Alkylation of Benzoic Acids

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1138
Copper-Catalyzed Asymmetric Synthesis of Thiazolidine-2-imines

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1139
Synthesis of Oxazoles from 2H-Azirines and Aldehydes by Photoredox Catalysis

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1140
Synthesis of Indoles by Reductive Cyclization of ortho-Nitrostyrenes

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1141
Ylidenemalononitrile Enamines in the Synthesis of Pyridines and Pyrones

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1142
Synthesis of Azetidin-3-ones from Allenes by Oxidative Amination

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1143
Synthesis of α-Hetaryl Nitriles by Asymmetric Reductive Cross-Coupling

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1144
Synthesis of Borazaroquinolines and Borazaroisoquinolines

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1145
Synthesis of Tetrasubstituted Furans by the Morita–Baylis–Hillman Reaction

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1146
Substrate-Controlled C-2 Amination of Dichloropyrimidines with Tertiary Amines

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1147
Asymmetric Synthesis of Heterocycle-Fused Butyrolactones

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Synthesis of Materials and Unnatural Products
z1149
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1149
Give Me Five

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1150
Fused Boracyclic Donor–Acceptor Materials

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1151
Regioselective Double Acylation

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1152
Quinoidal Bithiophenes Fluoresce in NIR

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1153
A Smart Glue

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1154
Buchwald’s Bullet

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1155
Third Aryne’s the Charm

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1156
New Oligomers by Radical Couplings for Delicious SWCNT Wraps

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1157
Picky Zinc Porphyrazines: They Only Shine for Acids

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1158
Formal SiH₄ Chemistry Using Stable and Easy-to-Handle Surrogates

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1159
Oxidation makes Dinaphtothiophenes Voracious for Electrons

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1160
C,N Organoborons: New Dyes for Fluorescence Microscopy

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z1161
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1161
Palladium-Catalyzed Asymmetric Hydroesterification of Alkenylphenols

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1162
Utility of a Fluoroiodomethylzinc Carbenoid in Fluorocyclopropanation

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1163
Copper-Catalyzed Asymmetric 1,4-Addition of Alkylzirconocenes to Enones

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1164
Copper-Catalyzed Asymmetric Synthesis of Spirobilactams

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1165
Enantioselective Formation of All-Carbon Quaternary Stereocenters

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1166
Enantioselective Nitrosocarbonyl Hetero-ene Reaction with Silyl Enol Ethers

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1167
Copper-Catalyzed Enantioselective Synthesis of Carbo- and Heterocycles

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1168
Iron-Catalyzed [2+2] Cycloadditions of Unactivated Alkenes

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1169
Palladium-Catalyzed Asymmetric Carboamination of Alkenes FREE ACCESS

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1170
Enantioselective Michael Addition to 2-Enoyl-pyridine N-Oxides

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1171
Enantioselective Imine Reduction Catalyzed by Chiral Oxorhenium Complexes

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1172
Catalytic Asymmetric Synthesis of Tetrahydrocarbazoles

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1173
Rhodium-Catalyzed Asymmetric 1,4-Addition to Conjugated Imino Esters

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1174
Asymmetric Synthesis of Furo[3,4-b]indoles by Catalytic [3+2] Cycloaddition

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1175
Enantio- and Diastereoselective Synthesis of γ-Amino Alcohols

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1176
Asymmetric Synthesis of γ-Lactams by Hydroxoiridium/Chiral Diene Catalysis

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1177
Asymmetric Iron(III)-Catalyzed Sulfa-Michael Addition of Thiols to Dienones

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1178
Ligand-Controlled Regiodivergent Alkylboration of Alkenes with a Copper Catalyst

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1179
Magnesium(II)-Catalyzed Asymmetric (4+1)-Annulation Reaction

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1180
Enantioselective Borylation and Enantio-specific Cross-Coupling to Triarylmethanes

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1181
Lewis Acid-Catalyzed [3+2] Asymmetric Annulation of Indoles with Aziridines

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1182
Copper-Catalyzed Diastereoselective Synthesis of Hexahydropyrrolopyrroles

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1183
Palladium(II)-Catalyzed Asymmetric Allylic Alkylation of Prochiral Enolates

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1184
Kinetic Resolution of Vinyl Sulfoxides by Rhodium Catalysis

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1185
Heck–Matsuda Desymmetrization of meso cis-4-Cyclopentene-1,3-diol

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1186
Scandium-Catalyzed Diastereoselective [3+3] Cyclization

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1187
Iron-Catalyzed Asymmetric Hydrophosphonylation of Aldehydes

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1188
Redox Deracemization of Tetrahydroiso-quinolines

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1189
Asymmetric Synthesis of Benzoxasiloles by Nickel Catalysis

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Metal-Mediated Synthesis
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1191
Cobalt-Catalyzed Cyanation

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1192
Oxidative Cross-Coupling of Boron Enolates

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1193
Regioselective Aromatic C–H Borylation FREE ACCESS

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1194
Coupling of Aryl Fluorosulfonates with Aryl Boronic Acids

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1195
Copper-Catalyzed Oxidative Cross-Coupling of Tetrahydroisoquinolines

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1196
Asymmetric 1,4-Addition of Arylboronic Acids to Cycloalkenes

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1197
Stereospecific Coupling of Boronic Esters with Lithiated N-Heterocycles

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1198
Pd-PEPPSI-IHept^Cl-Catalyzed Cross-Coupling of Alkyl Zinc Reagents

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1199
Dehydrogenative Borylation of Terminal Alkynes

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1200
Cross-Coupling of Anisoles with a Nickel Catalyst

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1201
Copper-Catalyzed Cyanation of Arylboronic Acids using Acetonitrile

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1202
Palladium-Catalyzed Synthesis of Aryl Ketones from Amides

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1203
Ligand-Controlled Stereoretentive Suzuki–Miyaura Cross-Coupling

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1204
Silver-Mediated Direct O-Trifluoromethylation

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1205
Aminoboration of Unfunctionalized Olefins

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Organo- and Biocatalysis
z1207
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1207
Enzymatic cis-Dihydroxylation of Alkenes

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1208
Rigid Cationic Multidentate Halogen Bond Donor Catalysts

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1209
Switchable Organocatalytic Annulation Reactions

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1210
1,4-Iodofunctionalizations of Conjugated Dienes

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1211
Catalytic Heteroarene C-Alkylation with Alcohol-Derived Radicals

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1212
Phosphoric Acid-Catalyzed Asymmetric Nitroso-Diels–Alder Reaction

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1213
Synthesis of a Chiral β-Hydroxy-α-amino Acid by Using d-Threonine Aldolase

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Polymer-Supported Synthesis
z1215
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1215
Aerobic Cross-Dehydrogenative Coupling with Nanoporous Gold FREE ACCESS

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1216
Double Carbonylation of Aryl Iodides with Amines Using Palladium Nanoparticles

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1217
Titania-Encapsulated Palladium Catalyst for Hydrodechlorination of Chlorophenols

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1218
Synthesis of Benzimidazoles Catalyzed by an Ionic Liquid on Zinc Oxide Nanoparticles

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1219
Suzuki–Miyaura Coupling Catalyzed by a Polymer-Bound Palladium–Phosphine Complex

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1220
Oxidation of Hydrosilanes by Using Gold/Hydroxyapatite

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1221
Continuous-Flow Kinetic Resolution by Lipase-Catalyzed N-Acetylation

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1222
Hydrogenation of Nitroarenes by Using Co(0)-Co₃O₄/N-Doped Carbon Nanotubes

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1223
Amidation of Carboxylic Acids Catalyzed by Polystyrene-Supported Triphenylphosphine

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1224
Chitosan-Catalyzed Petasis Borono-Mannich Reaction

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1225
Asymmetric Reduction of Imines Catalyzed by a Supported Organocatalyst

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1226
One-Pot Synthesis of 2-Amino-4H-chromene-3-carbonitrile Derivatives

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1227
Solid-Phase Synthesis of Quinolines by Using an Alkoxyamine Linker

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1228
Hydrogenation with a Palladium/Ionic Liquid Catalyst on a Metal–Organic Framework

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1229
Monodisperse Platinum Nanoparticles on Active Carbon for the Synthesis of 1H-Tetrazoles

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1230
Solvent-Free Synthesis of Imidazoles by Using a Supported Heteropolyacid

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