Synlett

Issue 07 · July 1999

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1009
Ballini, Roberto:
Recent Progress on the Ring Cleavage of Cyclic 2-Nitro Ketones by External Nucleophiles

PDF (150 kb)
1019
Poli, Rinaldo:
Different Approaches to Mid-Valent, Paramagnetic Half-Sandwich Complexes of the Heavier Group 6 Metals

PDF (153 kb)
letter
1029
Rahim, Md Abdur; Fujiwara, Tooru; Takeda, Takeshi:
Titanocene(II)-Promoted Intramolecular Olefination of Thiol Esters: A New Route to Substituted 2,3-Dihydrothiophenes

PDF (60 kb)
1033
Markó, István E.; Ates, Ali:
Novel Annelation Methodology for the Rapid and Efficient Construction of Bicyclo [4.n.0] Alkanols and Alkenones

PDF (88 kb)
1037
Fujiwara, Kenshu; Saka, Kimiko; Takaoka, Daisuke; Murai, Akio:
A Simple Convergent Method for the Construction of Fused Tri- and Tetracyclic Ethers

PDF (94 kb)
1041
Gaertzen, Oliver; Misske, Andrea M.; Wolbers, Peter; Hoffmann, H. M. R.:
Synthesis of Enantiopure C-Glycosides and Pseudo C-Glycosides. Lewis Acid Mediated Cleavage of [3.3.1] Oxabicyclic Lactones

PDF (67 kb)
1045
Akiyama, Takahiko; Takaya, Jun; Kagoshima, Hirotaka:
HBF₄ Catalyzed Mannich-Type Reaction in Aqueous Media

PDF (41 kb)
1049
Punniyamurthy, T.; Irie, Ryo; Katsuki, Tsutomu; Akita, Munetaka; Moro-oka, Yoshihiko:
Why Do (R,R)- and (R,S)-(Salen)manganese(III) Complexes Show Different Substrate-Specificity? The Role of an Apical Aqua Ligand

PDF (52 kb)
1053
Raiman, Marina V.; Il'ina, Natalia A.; Kulinkovich, Oleg G.:
A Convenient Method for the Preparation of N-Substituted 1-Acetonylaminocyclopropanes from Acetoacetic Ester Ethylene Acetal

PDF (25 kb)
1055
Park, Chan Pil; Sung, Jin Wuk; Oh, Dong Young:
Stereoselective Synthesis of 1,1-Bimetalloalkenes of Tin and Selenium, Tin and Tellurium

PDF (36 kb)
1057
Dambrin, Valéry; Villiéras, Monique; Amri, Hassen; Lebreton, Jacques; Villiéras, Jean:
Copper (I) Mediated Conjugate Addition of Grignard Reagents to 2-Oxoethylcyclohexenols. A Versatile, Efficient and Diastereoselective Route to anti, Z 6-Alkyl-2-trialkylsilyloxy-1-(2-trimethylsilyloxypropylid-1-ene)-cyclohexanes

PDF (37 kb)
1059
Loh, Teck-Peng; Wei, Lin-Li; Feng, Li-Chun:
Direct Aldol Reactions of Glycoxylic Acid Monohydrate with Ketones

PDF (31 kb)
1061
Raza, Abbas:
Novel Solid State Reduction of Organic Functional Groups on Solid Support (Merrifield's Resin)

PDF (32 kb)
1063
Chandrasekhar, S.; Mohanty, Pradyumna K.; Ramachander, T.:
One Pot Deprotective Oxidation of O-Allyl Ethers Using 70% tert-Butyl Hydroperoxide and Catalytic CrO₃

PDF (28 kb)
1065
Wang, Lei; Zhou, Longhu; Zhang, Yongmin:
Reduction of Aromatic Nitro Compounds Using Samarium Metal in the Presence of a Catalytic Amount of Iodine under Aqueous Media

PDF (20 kb)
1067
Olah, George A.; Mathew, Thomas; Farnia, Morteza; Prakash, G. K. Surya:
Nafion-H Catalysed Intramolecular Friedel-Crafts Acylation: Formation of Cyclic Ketones and Related Heterocycles

PDF (43 kb)
1069
timac, Anton; Leban, Ivan; Kobe, Joe:
An Efficient Stereospecific Method for the Synthesis of 8-Aza-3-deazaguanine Nucleosides from Glycosyl Azides

PDF (83 kb)
1074
Fukase, Koichi; Nakai, Yoshihiko; Egusa, Kenji; Porco Jr, John A.; Kusumoto, Shoichi:
A Novel Oxidatively Removable Linker and Its Application to α-Selective Solid-Phase Oligosaccharide Snythesis on a Macroporous Polystyrene Support

PDF (177 kb)
1079
Lütjens, Henning; Scammells, Peter J.:
Synthesis of 2-Substituted 3-Acylbenzo[b]furans via the Palladium Catalysed Carbonylative Cyclisation of ortho-Hydroxytolans

PDF (43 kb)
1082
Piers, Edward; Romero, Miguel A.; Walker, Shawn D.:
Sequential Anionic 1,3 Ester Shifts and Intramolecular Stille Couplings: A New Protocol for the Concise Assembly of Functionalized Polycyclic Dienes

PDF (55 kb)
1085
Joczyk, Andrzej; Konarska, Anna:
Generation and Reactions of Ammonium Ylides in Basic Two-Phase Systems: Convenient Synthesis of Cyclopropanes, Oxiranes and Alkenes Substituted with Electron-Withdrawing Groups

PDF (63 kb)
1088
Brun, Eva M.; Gil, Salvador; Mestres, Ramón; Parra, Margarita:
Dienediolates of α,β-Unsaturated Carboxylic Acids in Synthesis: A New Synthetic Method to 2-Pyridones

PDF (50 kb)
1091
Piotrowski, David W.:
A Concise Route to Novel 1-Aryl and 1-Pyridyl-2-Azabicyclo[2.1.1]hexanes

PDF (48 kb)
1094
Agami, Claude; Comesse, Sebastien; Kadouri-Puchot, Catherine; Lusinchi, Marie:
Efficient 1,3-Asymmetric Inductions during Nucleophilic Additions to Imine and Iminium Ion Derivatives

PDF (40 kb)
1097
Mohanakrishnan, Arasambattu K.; Cushman, Mark:
Pd(0)-Mediated Cross Coupling of 2-Iodoestradiol with Organozinc Bromides: A General Route to the Synthesis of 2-Alkynyl, 2-Alkenyl and 2-Alkylestradiol Analogs

PDF (39 kb)
1100
Wuckelt, Jörg; Döring, Manfred; Beckert, Rainer; Langer, Peter:
Efficient Synthesis of Quinazolin-4-ones and Axially Chiral 2,2′-Bisquinazolin-4-ones by Reaction of Anthranilic Acid Derived Nucleophiles with Oxalic Acid-Bis(imidoyl)chlorides

PDF (44 kb)
1103
Endo, Atsushi; Kann, Toshiyuki; Fukuyama, Tohru:
Synthetic Study on Ecteinascidin 743 Starting from d-Glucose

PDF (61 kb)
1106
Barberis, Claude; Voyer, Normand:
Synthesis of Both Enantiomers of Phenylglycine Using (-)-Sparteine

PDF (34 kb)
1109
Luo, Meiming; Iwabuchi, Yoshiharu; Hatakeyama, Susumi:
Regioselective Buta-1,3-dienylation of Aldehydes via Transmetallation of 2-Tributylstannylbuta-1,3-diene

PDF (58 kb)
1112
Reddy, B. S. Praveen; Damayanthi, Yalamati; Lown, J. William:
Design and Efficient Synthesis of Novel DNA Interstrand Cross-Linking Agents: C2-Linked Pyrrolo[2,1-c][1,4]benzodiazepine Dimers

PDF (44 kb)
1115
Bourque, Élyse; Grenon, Michel; Laliberté, Sébastien; Deslongchamps, Pierre:
Macrocyclic Studies of EZ and ZZ 12-membered Aza Macrocycles; Novel Molecular Rearrangement Observed

PDF (51 kb)
1118
Haddad, Mansour; Botuha, Candice; Larchevêque, Marc:
Total Synthesis of the Multidrug-Resistance Reversing Agent Hapalosin

PDF (43 kb)
1121
Berteina, Sabine; De Mesmaeker, Alain; Wendeborn, Sebastian:
Functionalization via Radical Cyclization of Cyclohexenediol Derivatives Bound to Polystyrene

PDF (75 kb)
1124
Abbas, Sahar; Hayes, Christopher J.:
A Novel Palladium-Catalysed Coupling Strategy for the Rapid Synthesis of Nucleic Acid Analogues Bearing Modified Backbones

PDF (59 kb)
1127
Diedrichs, Nicole; Westermann, Bernhard:
Synthesis of Enantiomerically Pure Bicyclic Lactams

PDF (48 kb)
1130
Mikami, Koichi; Matsumoto, Shoji; Okubo, Yasutaka; Okubo, Yasutaka; Suenobu, Tomoyoshi; Fukuzumi, Shunichi:
Single Electron Transfer Diels-Alder Reaction of Fullerene with Danishefsky's Diene

PDF (65 kb)
1133
Crew, Andrew P. A.; Lyons, Amanda J.; Camp, Nicholas P.:
Synthesis of a Stable Mimic for the Ring Closed Form of Gallein, Featuring a Novel One Pot Boron Tribromide Mediated Intramolecular Cyclisation Process

PDF (46 kb)
1136
Löhr, Birgit; Orlich, Simone; Kunz, Horst:
Modified Trityl Ester Protecting Groups in Peptide Synthesis

PDF (48 kb)
1139
Löhr, Birgit; Orlich, Simone; Kunz, Horst:
A Strategy Towards the Stereoselective Synthesis of 5-Hydroxylysine

PDF (43 kb)
1142
Krief, Alain; Remacle, Bruno; Dumont, Willy:
On the Carbocyclization of ω-Styrenylbenzyllithiums

PDF (42 kb)
1145
Havelková, Martina; Hocek, Michal; esnek, Michal; Dvoák, Dalimil:
The Suzuki-Miyaura Cross-Coupling Reactions of 6-Halopurines with Boronic Acids Leading to 6-Aryl- and 6-Alkenylpurines

PDF (64 kb)
1148
Bertrand, Michèle P.; Feray, Laurence; Nouguier, Robert; Perfetti, P.:
Diethylzinc Mediated Radical Additions to Glyoxylate Imines

PDF (46 kb)
1151
Smith, Martin D.; Long, Danile D.; Martín, Angeles; Campbell, Neil; Blériot, Yves; Fleet, George W. J.:
Tetrahydrofuran α-Azido Esters: Precursors of Anomeric α-Amino Acid Monomers via Radical Bromination

PDF (51 kb)
1154
Itoh, Takashi; Nagata, Kazuhiro; Miyazaki, Michiko; Ohsawa, Akio:
A Novel Synthesis of Chiral Tetrahydroisoquinolines Employing Silyl Enol Ethers in the Presence of Chiral Acyl Chlorides

PDF (68 kb)
1157
Takeda, Tsuyoshi; Irie, Ryo; Shinoda, Yo; Katsuki, Tsutomu:
Ru-Salen Catalyzed Asymmetric Epoxidation: Photoactivation of Catalytic Activity

PDF (69 kb)
1160
Mihara, Jun; Hamada, Tetsuya; Takeda, Tsuyoshi; Irie, Ryo; Katsuki, Tsutomu:
Photo-controlled Lewis Acidity: Chiral (ON)Ru-Salen Catalyzed Hetero Diels-Alder Reaction and Kinetic Resolution of Racemic Epoxides

PDF (70 kb)
1163
Uchida, Tatsuya; Irie, Ryo; Katsuki, Tsutomu:
Chiral (ON)Ru-Salen Catalyzed Cyclopropanation: High Cis- and Enantioselectivity

PDF (61 kb)
1166
Takeda, Tsuyoshi; Irie, Ryo; Katsuki, Tsutomu:
X-Ray Diffraction Analysis of Chiral (R,S)-(ON)Ru-Salen Complex: Unusual Unsymmetric Conformation

PDF (39 kb)
new tools in synthesis
1169
Griesbeck, Axel G.; Kramer, Wolfgang; Oelgemöller, Michael:
Synthetic Applications of Photoinduced Electron Transfer Decarboxylation Reactions
FREE ACCESS

PDF (422 kb)
synlett spotlight
1179
Fernández-Megía, Eduardo:
Zirconocene Hydrochloride "Schwartz Reagent"
FREE ACCESS

PDF (55 kb)

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