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Synlett 1991; 1991(3): 165-167
DOI: 10.1055/s-1991-20664
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Synthesis of Annulated Furanoses via Stereoselective Radical Cyclization of Haloalkenes Derived from Diacetone Glucose

José Marco-Contelles* , Angeles Martínez-Grau, Manuel Bernabé, Nazario Martín, Carlos Seoane
  • *Instituto de Química Orgánica, CSIC, Juan de la Cierva 3, E-28006 Madrid, Spain
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Publikationsdatum:
07. März 2002 (online)

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The synthesis of some cyclohexane-, cycloheptane- and tetrahydropyran-annulated furanoses via tributyltin hydride - 2,2′-azobisisobutyronitrile promoted radical cyclization of C3-branched-chain sugars 2-7, prepared from diacetone glucose (1,2:5,6-di-O-isopropylidene-α-D-glucofuranose), is described.