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Synlett 1991; 1991(3): 165-167
DOI: 10.1055/s-1991-20664
DOI: 10.1055/s-1991-20664
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Synthesis of Annulated Furanoses via Stereoselective Radical Cyclization of Haloalkenes Derived from Diacetone Glucose
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Publication Date:
07 March 2002 (online)
The synthesis of some cyclohexane-, cycloheptane- and tetrahydropyran-annulated furanoses via tributyltin hydride - 2,2′-azobisisobutyronitrile promoted radical cyclization of C3-branched-chain sugars 2-7, prepared from diacetone glucose (1,2:5,6-di-O-isopropylidene-α-D-glucofuranose), is described.