Synfacts

Issue 06 · June 2024

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Synform
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SYNFORM ISSUE 2024/06
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Synthesis of Natural Products
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0561
Total Synthesis of (±)-Rubriflordilactone A
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0562
Total Synthesis of (±)-Pallamolide A

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0563
Total Synthesis of Salarins A and C

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0564
Synthesis of (–)-Aspersteroid A

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0565
Synthesis of (–)-Higginsianin A

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0566
Total Synthesis of (–)-Spirophylline C and (+)-Spirophylline D

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0567
Total Synthesis of Ajmaline
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Synthesis of Heterocycles
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0569
Efficient Chloroacetoxylation of Pyrrolidines and Piperidines
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0570
Cross-Dehydrogenative Couplings to Access C4-Disubstituted Dihydroquinazolines

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0571
Efficient Suzuki–Miyaura Coupling of Glutarimide Derivatives

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0572
C–H Functionalization of Heteroaromatics with α-C–H Bond of THF Rings

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0573
Enantioselective Synthesis of Dihydropyrans via Fe(III)-Catalyzed Hetero-Diels–Alder Reaction

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0574
Synthesis of Spiro Heterocycles through a Three-Component Reaction

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0575
Brønsted Acid-Mediated Intramolecular Cyclization of 1,3-Azadienes Derived from Imines

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0576
Efficient, One-Pot Synthesis of 5,6-Dihydro[2,1-a]isoquinolines

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0577
Solvent-Free Mechanochemical Elaboration of Pyrazine Derivatives

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0578
Chelation-Assisted Oxidative 1,3-Aryl Migration α-Aryl Allylic Alcohols via Csp²−Csp³ σ-Bond Activation

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0579
One-Pot Synthesis of Structurally Diverse Sulfurized/ Selenated 4-Aminopyrimidines

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0580
Nitrogen to Carbon Swap in Pyridine Systems

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Synthesis of Materials and Unnatural Products
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0581
Regioselectivity in Mechanochemistry
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0582
Double-Decker Macrocycles

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0583
Reversible Sulfur Exchange via S_NAr

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0584
Water-Degradable Copolymers

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0585
Facile π‑Extension of Triphenylenes

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0586
Double [7]Helicenes with Chiroptical Amplification

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0587
α,ω-Functionalized Polydienes from Organoaluminum

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0588
2,6-Naphthyridine Synthesis and its Conjugated Polymers

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0589
Self-Assembly and Self-Templated Growth of Graphdiynes

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0590
Room Temperature Suzuki–Miyaura Polymerizations

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0591
Four-Component Assembling of Covalent Organic Frameworks

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0592
B,N-Embedded Helicenes

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Metals in Synthesis
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0593
Enantioselective Synthesis of Organoborons Enabled by Cyclopropene Ring Opening
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0594
Nickel-Catalyzed Enantioselective 1,2-Carboboration of Alkenes to Access β-Chiral Alkylboronates

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0595
Making Allylamines by 1,4-Carboamination of 1,3-Dienes under Dual Cobalt and Acridine Catalysis
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0596
Copper-Catalyzed Synthesis of Phenols and Anilines

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0597
Copper Catalyzed C–H Functionalization

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0598
Visible-Light-Mediated Amination Using Iron Catalysis

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0599
Light-Enabled Isomerization of Borylated 1,3-Dienes

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0600
Photocatalyzed O- to S- Rearrangement of Cyclopropanols

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0601
Copper-Catalyzed Electrophilic Hydroxylamination of Arylboronic Acids with a Hypervalent Iodine Reagent

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0602
Synthesis of Si-Stereogenic Silanols via Pd-Catalyzed C–H Alkenylation

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0603
Allylic Amine Synthesis Enabled by Rare-Earth-Catalyzed Annulations

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0604
Dynamic Kinetic Resolution of Racemic 2-Substituted Indoles by Pd-Catalyzed Asymmetric Hydrogenation

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0605
A Metal-Catalyzed Functional Group Exchange Approach to Carbon-Labeled Carboxylic Acids

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0606
Copper-Catalyzed Asymmetric Aminative Difunctionalization of Alkenes with Azodicarboxylates

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0607
Stereoselective Synthesis of Chiral Cyclohexylamine Derivatives via Photocatalyzed [4+2] Cycloaddition

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0608
Copper-Catalyzed Enantioconvergent Propargylic Amination to Access Chiral α-Tertiary Amines

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0609
Stereoselective Synthesis of C-Aryl Glycosides via Palladium-Catalyzed Heck Coupling

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0610
Palladium-Catalyzed Asymmetric Intramolecular Addition of Vinyl Halides to Carbonyl Groups

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0611
Asymmetric Reductive Carbocyclization of 1,6-Enynes Under Nickel Catalysis

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0612
Synthesis of Dihydrofurans by Palladium-Catalyzed [3+2] Cycloaddition

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0613
Enantioselective Copper-Catalyzed C–S Coupling via SH2

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0614
Directed Regio- and Enantioselective Hydrofluorination of Alkenes Under Nickel Hydride Catalysis

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0615
Selective C–H Oxidation Enabled by Manganese Catalysis

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0616
Rapid Access to Novel Antimalarials by a Cross-Electrophile Coupling Oxidation Sequence

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0617
Rhodium-Catalyzed C–H Carbonylation of Benzamides Using a CO Surrogate

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0618
Aryl–Aryl Bond Formation via a Rhodium-Catalyzed Split Cross-Coupling Strategy

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Polymer-Supported Synthesis
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0619
Iron-Catalyzed Aerobic Oxidation of Allylic C–H Bonds

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0620
Cu@C₂N-Catalyzed Transformations of Alkynes: Hydration and Glaser–Hay Coupling

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0621
Enantioselective Michael Addition Using Ni(OAc)₂−Chiral Covalent Organic Cage Complexes
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0622
Ruthenium-Sulfide: A Sulfur-Resistant Catalyst for Selective Hydrogenation of S-Containing Quinolines

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0623
Oxidative Amidation of Aldehydes with an N-Doped Carbon-Supported Ni Catalyst

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0624
Cycloaddition of Epoxides and CO₂ by Cobalt Porphyrin-Based Hypercrosslinked Ionic Polymers

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0625
Platinum–Molybdenum Nanoparticles-Catalyzed Reductive Amination of Carboxylic Acids

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0626
Photo-Induced Hydrophosphinylation Using Single-Atom Copper, Supported on Carbon Nitride

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0627
Development of a Biomass-Derived Carbon Aerogel-Supported Cu(OTf)₂ Catalyst

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0628
Co-MOF-Catalyzed Dehydrogenative Borylation of Alkenes

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0629
Photo-Induced Aldol Condensation of Furfurals with Surface-Modified CdS Quantum Dots

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0630
A COF-Based Metallaphotocatalyst for C–P Bond Forming Cross-Coupling

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Organo- and Biocatalysis
z0631
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0631
Cooperative Photoredox and Chiral Brønsted Acid Catalysis Permits Asymmetric [2π+2σ] Cycloaddition
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0632
Efficient Asymmetric Syntheses of Chiral Imines with Multi-Stereocenters

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0633
Light-Governed Chemoselectivity in Organocatalytic C(sp²)–X Couplings

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0634
Cinchona Phosphinate-Catalyzed Desymmetrization of Sulfonimidamides

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0635
Silylium Ions Catalyze the Regioselective and Diastereoselective Thiosilylation of C–C Multiple Bonds

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0636
Pivalate Salt-Catalyzed, Bis(silyl)acetamide-Mediated Silylation of Terminal Alkynes

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0637
Harnessing N-Heterocyclic Carbene Catalytic Activity into Stereoselective Synthesis of Chiral Cyclophanes

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0638
Photoenzymatic Hydroalkylation of Olefins toward Chiral α‑Chloroamides

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0639
Organophotocatalytic Construction of Sulfonamides from Dibenzothiophenium Salts

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0640
Potassium-ACDC of the Wittig Reaction

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Innovative Drug Discovery and Development
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0641
A Non-Classical Linker for the Synthesis of a PROTAC

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0642
[¹⁸F]4-Fluoro-4-deoxyfructose for Tracing of Fructose Metabolism

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0643
Reproducibility Study of Surfactants Across Different Reaction Types

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0644
SuFEx-Clickable Probe Against HIV-1 Capsid Protein

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0645
Two-Step, One-Pot Annulation of Heteroarenes

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0646
[3+2] Cycloaddition Approach to Difluoromethyl Isoxazoline Derivatives

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0647
Large-Scale Asymmetric Synthesis of Spirocyclic Building Blocks for Drug Development

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0648
Chemoenzymatic Synthesis Enables Decagram- and Gram-Scale Preparation of Prostaglandins

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0649
(Chloromethyl)triisopropoxysilane Enables Highly Regioselective N1-Methylation of Pyrazoles

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0650
Transition Metal-Free Synthesis of Hydrazides from Amides and Amines

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0651
Structurally Simplified Natural Product Analogs Retain Bioactivity

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0652
ABBP Uncovers a New Covalent ERCC Degrader from Spirocyclic Azetidines

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0653
Synthesis and Biological Evaluation of a Voltage-Gated Sodium Channel Inhibitor

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0654
Intermolecular Chalcogen Bonding between Galectin-3 and an Orally Bioavailable Antagonist

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Peptide Chemistry
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0655
Synthesis of Peptides Inversely via the Utility of Transient Protected Amino Acids
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0656
5- and 6-Membered Heteroaromatics-Embedded Amino Acids Synthesis via Electrochemical Means

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0657
Visible-Light-Catalyzed Chemo-Selective β-C(sp³)–H Perfluoroarylation of Serine-Containing Peptides

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0658
Synthesis of Amino Acid Based Chiral Cyclic Carbonates

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0659
Near-IR-Induced Site-Selective Fluoroalkylation of Tryptophan and Tryptophan-Containing Peptides

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0660
Selective S- and N-Acylation of Glutathione Using N-Acyl Imidazole

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0661
gem-Difluorinated Cyclopropanes for α-Fluoro-allylation of Enantioselective Amino Acid Esters

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0662
Improved Synthesis of Sensitive Peptides via Fmoc Deprotection Approach

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0663
A Highly Diastereoselective Tandem Oxyhomologation–Coupling Method to Synthesize Amides and Peptides

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0664
Visible-Light-Mediated β-Amino Acid Synthesis from α-Amino Acids

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0665
gem-Difluoroallylation of Glycine and Glycine Residue in Peptides Using Organophotoredox Catalysis

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0666
Chemoselective Photocatalytic Desulfonylation of Tryptophan Based Peptides

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0667
CBMIT-Mediated Synthesis of Amino Esters and Peptides
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Flow Chemistry
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0669
Norrish-Type Photocyclization of Aryl Triazines in Flow

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0670
Continuous-Flow Process Enables Safe, Practical Access to Pharmaceutically Important 1,2,3-Triazole

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