Synfacts

Ausgabe 03 · März 2020

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A31
SYNFORM ISSUE 2020/03

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Synthesis of Natural Products and Potential Drugs
z0245
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PDF (571 kb)
0245
Total Synthesis of Swinhoeisterol A, Dankasterones A and B, and Periconiastone A
FREIER ZUGRIFF

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PDF (124 kb)
0246
Total Syntheses of (+)-Lyconadins D and E

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PDF (86 kb)
0247
Synthesis of a Macrocyclic Mcl-1 Inhibitor
FREIER ZUGRIFF

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PDF (143 kb)
0248
Synthesis of d₉-Ivacaftor Using o-Quinone Methide Chemistry

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PDF (89 kb)
0249
Synthesis of Sonidegib Using Palladium Catalysis in Water

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PDF (79 kb)
0250
Synthesis of (–)-Oridonin

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PDF (100 kb)
0251
Synthesis of Taniborbactam

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PDF (100 kb)
0252
Synthesis of β-Lactamase Inhibitor Relebactam

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PDF (100 kb)
0253
Synthesis of (–)-Curvulamine

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PDF (79 kb)
0254
Synthesis of a Baloxavir Marboxil Fragment

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PDF (92 kb)
0255
Total Synthesis of (–)-PF-1018

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PDF (91 kb)
0256
Synthesis of O-GlcNAcase Inhibitor MK-8719

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PDF (74 kb)
0257
Synthesis of ERK1/2 Inhibitor AZD0364

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PDF (79 kb)
0258
Synthesis of AMG 510

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PDF (87 kb)
0259
Synthesis of Axelopran

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PDF (101 kb)
0260
Synthesis of (+)-Tronocarpine

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PDF (83 kb)
0261
Synthesis of (±)-Tetrodotoxin
FREIER ZUGRIFF

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PDF (138 kb)
Synthesis of Heterocycles
z0263
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PDF (301 kb)
0263
One-Step Synthesis of 4-Fluoropyrimidines

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PDF (93 kb)
0264
Synthesis of Benzofuroindolines through Biocatalytic Oxidative Phenol–Indole [3+2] Reactions

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PDF (79 kb)
0265
Palladium-Catalyzed Ring Expansion for the Synthesis of 12-Membered Heterocycles

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PDF (78 kb)
0266
Synthesis of Butenolides from Functionalized Cyclopropenones

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PDF (84 kb)
0267
Electrochemical Synthesis of trans-2,3-Disubstituted Aziridines

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PDF (93 kb)
0268
Regioselective Synthesis of CF₂H-Containing Pyrazoles

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PDF (83 kb)
0269
Enantioenriched Dihydroquinolines by NHC Catalysis

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PDF (93 kb)
0270
Diastereoselective Cyclization of Oxime-Tethered Cyclopropanes to Pyrrolooxazines

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PDF (85 kb)
0271
Light-Mediated Dehydrogenative Povarov Reaction of Indoles and Benzofurans

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PDF (81 kb)
0272
Stereoselective and Regioselective Functionalization of Piperidines through C–H Activation

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PDF (86 kb)
0273
The N-Oxide Moiety as a Traceless Directing Group for Pyridine 2-C(O)–C Bond Activation

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PDF (86 kb)
0274
Asymmetric Palladium-Catalyzed Synthesis of Fluoropiperidines

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PDF (89 kb)
0275
Modified Pomeranz–Fritsch Reaction for the Synthesis of 1,2-Dihydroisoquinolines

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PDF (84 kb)
Synthesis of Materials and Unnatural Products
z0277
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PDF (355 kb)
0277
Dendralenes and Radialenes and Butadienes, Oh My!

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PDF (76 kb)
0278
Two ‘L’s are a Win for Fluorescent Helical Foldamers

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PDF (97 kb)
0279
Close to N-Doped Zigzag Carbon Nanobelts

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PDF (78 kb)
0280
A Palladium-Catalyzed Tandem Reaction to Construct bis-BN-Naphthalene-Fused Oxepins

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PDF (88 kb)
0281
Synthesis of Fold-Line-Shaped BN-Embedded Polycyclic Aromatic Hydrocarbons

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PDF (72 kb)
0282
Helical Nanographenes: Now with Azulene

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PDF (82 kb)
0283
Stereospecific PAH Synthesis with a Twist

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PDF (91 kb)
0284
Covalently Linked Dimers with Intramolecular Stacking

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PDF (92 kb)
0285
Gold-Digging Polythioamides via Sulfur, Acid and Amine Polymerization

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PDF (102 kb)
0286
Little PolyANIs

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PDF (86 kb)
0287
Supramolecular Pi

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PDF (84 kb)
0288
Oxygen/Sulfur Exchange in Epoxides to Make Poly(thioethers)

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Metals in Synthesis
z0289
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0289
Palladium-Catalyzed Dicarbonylation of 1,3-Dienes for the Synthesis of Adipic Acid Esters
FREIER ZUGRIFF

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PDF (121 kb)
0290
Dual-Catalyzed 1,2-Difunctionalization of Vinyl Boronates

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PDF (74 kb)
0291
Synthesis of C-Alkyl Glycoamino Acids via Palladium-Catalyzed C(sp³)–H Glycosylation
FREIER ZUGRIFF

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PDF (141 kb)
0292
Nickel-Catalyzed Hydroalkylation of Olefins

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PDF (90 kb)
0293
Iron-Electrocatalyzed C–H Arylations

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PDF (74 kb)
0294
Synthesis of Acylsilanes via Carbonylative Silylation of Alkyl Halides Using Copper Catalysis

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PDF (71 kb)
0295
Reduction of Amides and Esters with Borane Dimethyl Sulfide Complex

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PDF (70 kb)
0296
Hydroamination of Olefins

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PDF (78 kb)
0297
Hydroamination of Cyclobutenes and Cyclopropenes

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PDF (71 kb)
0298
Highly Selective Rhodium-Catalyzed Tandem Spirocyclization/Reduction of 3‑Allenylindoles

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PDF (79 kb)
0299
Enantioselective Rhodium-Catalyzed C–H Borylation of N-Alkylamines and Amides

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PDF (85 kb)
0300
Dual Photoredox/Nickel-Catalyzed Preparation of Aryl Aminooxetanes

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PDF (82 kb)
0301
Nickel/Photoredox Dual Catalysis Mediated Dicarbofunctionalization of Olefines

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PDF (73 kb)
0302
Iron-Catalyzed Allylic and Propargylic C–H Functionalization for the Formation of C–C Bonds

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PDF (78 kb)
0303
Enantioselective C(sp³)–H Amidation under Rhodium Catalysis

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PDF (76 kb)
0304
Conjunctive Cross-Coupling of Vinyl Boronic Esters

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PDF (82 kb)
0305
[4+2] Cycloaddition of Dienes with Vinylcarbenes

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PDF (80 kb)
0306
A New para-Selective Difluoroalkylation

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PDF (81 kb)
0307
Regioselective Aziridine Opening

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PDF (68 kb)
0308
Nickel-Catalyzed Synthesis of Homoallylic Alcohols under Photoredox Conditions

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PDF (79 kb)
0309
Thiiranes and Thiethane Oxyalkynylation through a Copper-Catalyzed Ring Opening

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PDF (80 kb)
0310
Enantioselective Pd-Catalyzed Desymmetrization of Cyclohexanones: γ‑All-Carbon Quaternary Centers

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PDF (95 kb)
0311
Palladium-Catalyzed Dearomative [2+2+1] Spiroannulation through Alkyne-Directed C–H Activation

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PDF (79 kb)
0312
Enantioselective Rhodium-Catalyzed Dearomatization of Pyridinium Salts

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PDF (73 kb)
0313
Photoredox- and Cobalt-Catalyzed Intermolecular Reductive Ene-Yne Coupling

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PDF (74 kb)
0314
The Stille Carbonylative Cross-Coupling Reaction
FREIER ZUGRIFF

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PDF (123 kb)
0315
Directed Metalation Using TMP₂AgCNLi₂

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PDF (81 kb)
0316
Difluoromethylation of Benzylic C–H Bonds via Copper Catalysis

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PDF (79 kb)
Polymer-Supported Synthesis
z0317
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PDF (339 kb)
0317
Shape-Selective Hydrogenation of Nitroarenes by Using Zeolite-Encaged Single-Atom Rhodium Catalysts
FREIER ZUGRIFF

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PDF (125 kb)
0318
Synthesis of Chromenopyrimidines on Cobalt Oxide–Nickel Oxide–Sulfonated Graphene Quantum Dots

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PDF (74 kb)
0319
Oxygenation of Olefins with N-Doped Carbon-Incarcerated Cobalt Nanoparticles

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PDF (85 kb)
0320
Dehydrogenation and Hydrogen-Borrowing Reactions with a P-Doped Polymer-Supported Iridium Catalyst

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PDF (79 kb)
0321
Photodehydrogenation of N-Heterocycles on Nickel(II)-Grafted Titanium Dioxide

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PDF (81 kb)
0322
Palladium Nanoparticle Catalyzed Suzuki–Miyaura Cross-Coupling under Ultrasonic Irradiation

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PDF (78 kb)
0323
Micellar Cross-Coupling of Aryl Halides with N-Tosylhydrazones Catalyzed by Palladium Nanoparticles

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PDF (82 kb)
0324
Synthesis of Chromeno[b]pyridines under Ultrasonic Irradiation using TiO₂ NPs on Carbon Nanotubes

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PDF (82 kb)
0325
Photoinduced Aerobic C–C Coupling of Xanthenes on Sulfated Carbon Dots

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PDF (79 kb)
0326
Continuous-Flow Asymmetric Transfer Hydrogenation of Acetophenones with Propan-2-ol

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PDF (80 kb)
0327
Silica-Supported Manganese(II) Catalyst for Carbonyl Hydrosilylation, Hydroboration, and Transesterification

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PDF (82 kb)
0328
One-Pot Synthesis of Propargylamines on a Zinc Chloride Loaded Titania Catalyst

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PDF (71 kb)
0329
Cycloaddition of Carbon Dioxide to Epoxides on a Hollow Zn–Co Based Zeolitic Imidazole Framework

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PDF (76 kb)
Organo- and Biocatalysis
z0331
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PDF (318 kb)
0331
Foldamer-Catalyzed Macrocyclizations
FREIER ZUGRIFF

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PDF (124 kb)
0332
Lewis-Basic Peptide-Catalyzed Coupling of Naphthols and Quinones to Non-C₂-Symmetric Biaryls

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PDF (98 kb)
0333
Efficient Enzymatic Cascade for the Biosynthesis of Islatravir

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PDF (70 kb)
0334
Decarboxylative C(sp³)–X (X = O, NBoc, S) Bond Formation through Photoredox Catalysis

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PDF (93 kb)
0335
Methyl Triptycen-1-yl Sulfide Catalyzed Electrophilic Aromatic Halogenation with N-Halosuccinimides

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PDF (90 kb)
0336
NHC Catalysis Enables a Practical and General Organocatalytic Approach to C1-Deuterated Aldehydes

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PDF (82 kb)
0337
Asymmetric Counteranion-Directed Catalysis Meets Supramolecular Chemistry

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PDF (83 kb)
0338
Chiral Acyl Azolium Permits Dynamic Kinetic Resolution of Hydroxyphthalides

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PDF (93 kb)
0339
Biocatalytic Cascade Reduction of Cyclic Enimines

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PDF (101 kb)
0340
Nitrenium Salts as Hydrogen-Transfer Catalysts

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PDF (71 kb)
Chemistry in Medicine and Biology
z0341
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PDF (496 kb)
0341
A Repurposed Chemotherapy Drug as C1 Synthon
FREIER ZUGRIFF

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PDF (121 kb)
0342
Permeable and Fluorogenic Nanoscopy Probes

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PDF (111 kb)
0343
A Highly Selective Inhibitor of TBK1/IKKε

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PDF (91 kb)
0344
Cell-Type-Specific Voltage Imaging Using Covalently Tethered Fluorophores

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PDF (200 kb)
0345
A Versatile Cellular Target Engagement Probe for MPC2

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PDF (77 kb)
0346
Natural PDE4 Inhibitor Toddacoumalone

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PDF (83 kb)
0347
Bioinspired Nucleobase Caging

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PDF (85 kb)
0348
Investigating TRPA1 Modulation with Noncovalent Piperidine Carboxamide Based Binders

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PDF (83 kb)
0349
Staudinger Reduction-Activated Lysine for the Control of Protein Subcellular Localization and SUMOylation

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PDF (76 kb)
0350
Total Synthesis of a Gene
FREIER ZUGRIFF

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PDF (140 kb)
Peptide Chemistry
z0351
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PDF (395 kb)
0351
Cyclic Peptides Synthesis with the Assistance of a Removable Activating Group
FREIER ZUGRIFF

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PDF (126 kb)
0352
Synthesis of syn-α,β-Diamino Esters through an Asymmetric Mannich Reaction

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PDF (92 kb)
0353
Chiral Ammonium Salt Phase-Transfer-Catalyzed Synthesis of Quaternary β^2,2-Amino Acids

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PDF (100 kb)
0354
Hydroperoxide-Mediated Decarboxylative Acylation of Amines with α-Keto Acids

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PDF (87 kb)
0355
Metal-Free Photochemical Synthesis of α-Amino Acid Derivatives

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PDF (79 kb)
0356
Synthesis of α-Amino Acid Derivatives from Amines

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PDF (83 kb)
0357
Synthesis of C-Terminal Glycopeptides

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PDF (81 kb)
0358
Heterogeneous Catalysis for Amide Bond Formation

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PDF (70 kb)
0359
Photocatalytic Amide-Bond Formation

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PDF (67 kb)
0360
Enantioselective Synthesis of α-Aryl-β-amino Acids from N-Boc Imines and Homophthalic Anhydrides

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PDF (105 kb)
0361
Rhodium-Catalyzed Synthesis of α-Amino Acid Derivatives

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PDF (86 kb)
0362
Synthesis of α-Amino Acids by One-Pot Oxidation and Transamination of 1,2-Diols

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PDF (87 kb)
0363
Chlorofusin Cyclic Peptide Synthesis
FREIER ZUGRIFF

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PDF (117 kb)
Flow Chemistry
z0365
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PDF (149 kb)
0365
Heterogeneous Catalysis in Continuous Flow

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PDF (81 kb)
0366
Organocatalyzed Rauhut–Currier and [3+2] Annulation Domino Reaction under Flow Conditions

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PDF (76 kb)
0367
Functionalized Aryl Azides through Aryllithium Generation in Flow

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PDF (79 kb)
0368
Continuous Palladium-Catalyzed Carbonylative Cyclization Using Iron Pentacarbonyl as a CO Source

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PDF (77 kb)
Addendum
0370
Enzyme-Catalyzed Site-Selective C–H Amidation

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PDF (62 kb)

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