Synfacts

Issue 10 · October 2016

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A143
SYNFORM ISSUE 2016/10 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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0999
Synthesis of (+)-Notoamides F, I, and R and (–)-Sclerotiamide FREE ACCESS

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1000
Syntheses and Structure Elucidation of Juglocombins A and B, and Juglorescein

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1001
Synthesis of Vismodegib through meta-Selective Nitration of Arenes FREE ACCESS

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1002
Synthesis of Exochomine

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1003
Synthesis of (+)-Psiguadial B

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1004
Synthesis of an α_Vβ₆ Antagonist

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1005
Synthesis of MK-8876

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1006
Synthesis of (–)-Oseltamivir

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1007
Highly Efficient Synthesis of (−)-Maoecrystal V

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1008
Synthesis of MK-8718

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1009
Synthesis of AS-3201 (Ranirestat)

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1010
C–H Arylation of Heterocyclic N-Oxides: Application to SB222200

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1011
Syntheses of (+)-Javaberine A, (+)-Javaberine B, and (–)-Latifolian A

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1012
Synthesis of Palbociclib

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1013
Syntheses of Hyperjapones A–E, and Hyperjaponols A and C

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Synthesis of Heterocycles
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1015
Photocatalytic Azolylation of (Het)arenes

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1016
C2-Alkylation of Pyridine N-Oxides with 1,1-Diborylalkanes

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1017
Photoredox-Catalyzed Aryl Aminations with Ligand-Free Nickel(II) Salts

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1018
Rhodium(III)-Catalyzed C–H Activation Route to 1H-Isoindoles

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1019
Cobalt-Catalyzed Cross-Coupling Route to Homoallylic Alcohols and Amines

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1020
Enantioselective Synthesis of Pyrrolidines by Aminotrifluoromethylation of Alkenes

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1021
Directed Decarboxylative Cross-Coupling Route to Piperidines and Pyrrolidines

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1022
Synthesis of Perfluorinated Isochromene Derivatives by Ring Expansion

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1023
Synthesis of 3-Aminofurans from 1,2,3-Triazoles and Propargylic Alcohols

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1024
Sulfonated β-Cyclodextrin-Catalyzed Synthesis of Imidazopyridinamines

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1025
Gold-Catalyzed Synthesis of 1,5-Benzodiazepines

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1026
Synthesis of Fused and Spiro Dihydrobenzofurans

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1027
Synthesis of Isoquinolones and Isocoumarins by a Suzuki–Miyaura Coupling

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Synthesis of Materials and Unnatural Products
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1029
Nitrogen Analogues of Polycyclic Aromatic Hydrocarbons FREE ACCESS

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1030
Transition-Metal-Free Sulfoximidation with Hypervalent Iodine(III)

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1031
Enantiospecific Reduction Leads to P-Stereogenic Synthons

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1032
Introducing an Apical Anchor Group

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1033
A Halogen Party

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1034
Hydrogen-Bond Anionic Polymerization with Alkoxide and Thiourea

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1035
Four-State Nanoswitch Controls Two-Step Sequential Catalysis

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1036
Synthetic Route to Thiophene-Based Double Helical Oligomers

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1037
Helical ortho-Arylene Foldamers

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1038
N-Arylation of Iminodibenzyls and Iminostilbenes

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1039
Nitrogen Heterocycles through Migratory Ring Expansion of Metalated Ureas

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1040
Biazulene Diimide as a New Building Block for Organic Materials

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z1041
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1041
Convenient Reagent for the Copper-Catalyzed Asymmetric Methyl 1,4-Addition Reaction FREE ACCESS

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1042
Catalytic Asymmetric Henry Reaction

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1043
Asymmetric Allylic Amination

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1044
A Palladium-Catalyzed Dearomatization for the Synthesis of Polycyclic Indoles

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1045
Asymmetric 1,4-Addition by Chiral Nanoparticle/Lewis Acid Catalysts

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1046
Synthesis of Enantioenriched Arylglycines via Dynamic Kinetic Resolution

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1047
Palladium-Catalyzed Asymmetric C–O Bond Cleavage of α-Acyloxy Ketones

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1048
Highly Asymmetric Hydrogenation of Cyclic Enamides by Iridium Catalysis

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1049
Palladium-Catalyzed Asymmetric Synthesis of α-Arylglycines

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1050
Stereoselective Annulation by Palladium/Phosphine–Thiourea Catalysis

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1051
Asymmetric Synthesis of Silylated Indanols by Nickel Catalysis

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1052
Iridium-Catalyzed Enantioselective Hydrogenation of Pyridinium Bromides

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1053
Copper-Catalyzed Asymmetric Conjugate Addition of α,β-Unsaturated Carbonyls

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1054
Rhodium-Catalyzed Asymmetric Addition to N-Sulfonylimines

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1055
Cobalt-Catalyzed Stereoselective Three-Component C–H Bond Addition

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1056
Enantioselective Heck Reaction Leading to S- and P-Stereogenic Heterocycles

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1057
Enantioselective Rhodium-Catalyzed Arylation of Aldehydes

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1058
Synthesis of Tetrahydro-γ-Carbolines by [3+3] Cycloaddition

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1059
Synthesis of Chiral Tertiary Alcohols by Asymmetric Cyanosilylation

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1060
Asymmetric Copper-Catalyzed Etherification of Propargylic Esters

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1061
Enantioselective Hydrogenation by a Supramolecular Chiral Catalyst

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1062
Diastereoselective Synthesis of Amino Acids with a Quaternary Stereocenter

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1063
Diastereoselective Copper-Catalyzed Cyanation and Diborylation of Allenes

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1064
Ruthenium-Catalyzed Asymmetric Intermolecular Cyclopropanation Reaction

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1065
Enantioselective Intermolecular Hydroalkoxylation of Allenes and Alkynes

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1066
C₂-Symmetric Bis-sulfinamide Ligands for the Asymmetric Rh-Catalyzed Conjugate Addition

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1067
Palladium-Catalyzed Dearomative Reaction of Furans Towards Spirooxindoles

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1068
Asymmetric Hydrogenation of Seven-Membered C=N-Containing Heterocycles

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Metal-Mediated Synthesis
z1069
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1069
Addition of Organotrifluoroborates to Arylated Cyclopropyl Ketones

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1070
Iron-Catalyzed Cycloisomerization/Cross-Coupling Cascade

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1071
Aromatic Hydroxylation and Amination through Deprotonative Cupration FREE ACCESS

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1072
Borylation of 2-Pyridones

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1073
Carbonylative Coupling of Grignard Reagents

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1074
Catalytic Difluoromethylation of Aryl Halogenides

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1075
Enantioselective Allyl–Allyl Coupling between Boronates and Phosphates

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1076
Ring Opening of 2-Alkylenecyclobutanones

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1077
Boron Conjugate Addition Reactions

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1078
Enantioselective Addition of Boronated Allylcopper Derivatives

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1079
Ligand Coupling Reactions of Chiral Sulfoxides

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1080
Coupling of Secondary and Tertiary Boronic Esters

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1081
Photoredox-Mediated C–H Alkylation of N-Heteroarenes

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1082
Preparation of Homoallylic Alcohols in Flow and Batch

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1083
Enantioselective Conjugate Alkynylation of β-Aryl-β-trifluoromethyl Enones

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Organo- and Biocatalysis
z1085
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1085
Catalytic Asymmetric Geminal Difluorination of β-Substituted Styrenes FREE ACCESS

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1086
Asymmetric Mannich Reaction of Aliphatic N-Boc Imines

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1087
Biocatalytic Asymmetric Synthesis of Bulky Amines

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1088
Indolinecarboxylate-Catalyzed Enantio-selective oxa-Pictet–Spengler Reaction

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1089
Chiral Pyridoxamine Catalyzed Transamination of α-Keto Acids

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1090
Ser-His is Not a Microprotease

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1091
Catalytic Cyanotritylation of Aldehydes

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1092
Imidophosphate-Catalyzed Enantioselective Oxa-Pictet−Spengler Reaction

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1093
Hydrogen-Bonding Catalysis with Tetraalkylammonium Salts

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1094
Vanadium Chloroperoxidase Catalyzed Aza-Achmatowicz Reaction

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Polymer-Supported Synthesis
z1095
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1095
Flow Reactions in a Palladium/Carbon-Packed Bed Reactor

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1096
Aqueous Oxidation of Sugars on Hydrotalcite-Supported Gold Nanoparticles

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1097
Asymmetric Michael and Aldol Reactions with a Supported Chiral Diamine FREE ACCESS

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1098
Palladium/γ-Alumina-Catalyzed Amidation of Esters with Formamides

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1099
Controlled Hydrogenation of Alkynes with Nickel Nanoparticles on an Ionic Liquid

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1100
Asymmetric Michael Reaction on a Polystyrene-Supported Organocatalyst

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1101
Cyanation of Enones on Polystyrene-Supported Ammonium Fluoride

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1102
Suzuki–Miyaura Coupling on Palladium/Mesoporous Silica Microspheres in Water

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1103
Synthesis of 3-(Aminoalkyl)indoles on Silver/Silver–Nickel Alloy Nanoparticles

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1104
Hβ Zeolite Catalyzed Tandem Alkyne Hydration/Aldol Condensation

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1105
Friedel–Crafts Acylation with a Polymer-Supported Indium(III) Catalyst

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1106
Suzuki–Miyaura Coupling with Palladium Nanoparticles on Activated Carbon

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1107
Photoreduction of Nitroarenes on Palladium/Silica

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1108
Magnetic Zirconia Nanoparticle Catalyzed Trimethylsilylation of Alcohols

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1109
Synthesis of 1,2,3-Triazoles on Cuttlebone-Supported Copper(II) Chloride

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1110
Pt Nanoparticle/Polystyrene Catalyzed Indole Synthesis by Aerobic Oxidation

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Erratum
1111
Organocatalytic Transformation of Epoxides into Thiiranes

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