Synfacts

Ausgabe 09 · September 2014

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Ausgabe
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A114
SYNFORM ISSUE 2014/09 FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
z893
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0893
Synthesis of the Antifungal Agent ASP9726 FREIER ZUGRIFF

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0894
Synthesis of γ-Secretase Modulator SPI-1865

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0895
Total Synthesis of Sespenine FREIER ZUGRIFF

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0896
Synthesis of Taiwaniadducts B, C, and D

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0897
Synthesis of a Saxagliptin Fragment

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0898
Synthesis of (±)-Penifulvin A

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0899
Total Synthesis of Sculponeatin N

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0900
Synthesis of Both Enantiomers of Mequitazine

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0901
Synthesis of ALK Inhibitor PF-06463922

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0902
Total Synthesis of (–)-Nitidasin

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0903
Total Synthesis of Coccinellid Alkaloids

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0904
Syntheses of (+)-Psoracorylifol B and (+)-Psoracorylifol C

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Synthesis of Heterocycles
z905
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0905
Synthesis of Bioactive Nucleoside Analogues

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0906
2,3-Dihydro-1H-indazoles by Rhodium Catalysis

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0907
C–H Fluorination and Nucleophilic Aromatic Substitution of Nitrogen Heterocycles

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0908
2H‑Indazoles by Condensation−Cadogan Reductive Cyclization

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0909
Pd/C-Catalyzed Synthesis of 2-Substituted Benzothiazoles

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0910
Diastereoselective Preparation of Enantioenriched Polycyclic Oxoquinolines

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0911
Intramolecular Aryl–Aryl Coupling of 2-Substituted N-Phenylbenzamides

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0912
Synthesis of 1,3-Oxathiolan-2-ylidenes from α-Enolic Dithioesters and Epoxides

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0913
Synthesis of Oxepines by Cycloisomerization of 1,7-Oxadienes

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0914
Biomimetic Synthesis of Symmetrical Tetrasubstituted Pyrroles

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0915
Three-Component Synthesis of Fully Substituted Triazoles

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0916
Synthesis of Pyrroles by Photocatalyzed Cycloaddition of Alkynes to Azirines

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0917
C(sp²)–C(sp³) Bonds by Intramolecular Reductive Cross-Coupling

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0918
Fused Heterocycles via C–H Activation and Cyclization of Indoles and Pyrroles

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Synthesis of Materials and Unnatural Products
z919
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0919
SET Sets the Stage: Photochemical Synthesis of Aminomethylfullerenes

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0920
Activate Twice, Then Annulate

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0921
Get Your Biotin Kicks on Route 6+6

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0922
Stabilization of Hexacenes by Dioxolane Functionalization

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0923
Heterobenzene Club Welcomes First Aluminum Member

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0924
Highly Fluorinated Luminescent Subporphyrins

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0925
Light the Way: Phenanthro[9,10-c]thiophenes by Photocyclization

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0926
[2+2+2] to Twist: Synthesis of [9]- and [11]Helicene-Like Molecules FREIER ZUGRIFF

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0927
Reduce, Rearrange, Reoxidize: Thermal Route to a Ladder Diborole

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0928
Better Building of Benzo[b]phosphole Derivatives

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0929
Intramolecular Acylation of Biarylcarboxylic Acids to Fluorenones

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0930
We All Scream for Selenophenes

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z931
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0931
Diastereo- and Enantioselective Iridium-Catalyzed Annulation of Salicylimines FREIER ZUGRIFF

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0932
Intramolecular Heck Reaction of Secondary Benzylic Ethers

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0933
Dearomative Cycloadditions Catalyzed by Palladium FREIER ZUGRIFF

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0934
Iridium-Catalyzed Hydrogenation of Pyrrolo[1,2-a]pyrazinium Salts

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0935
Asymmetric Hydrogenation of Quinolin-3-amines

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0936
Enantioselective Synthesis of 2-Arylchromenes via Palladium Catalysis

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0937
Allylic Substitution of Enolates Derived from α,β-Unsaturated Ketones

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0938
Cyclopropanation of Allenes Catalyzed by Ruthenium

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0939
Enantioselective Copper-Catalyzed 1,4-Addition and Enolate Trapping

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0940
Titanium-Promoted Asymmetric Cyclo-propanation of N-Alkenyl Thioamides

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0941
Isoindolines via Enantioselective C−H Insertion of Diazo Compounds

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0942
Enantioselective β-Lactam Synthesis via Pd-Catalyzed C(sp³)–H Alkylation

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0943
Enantioselective Rhodium-Catalyzed Primary C–H Bonds

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0944
Hetero-Diels–Alder Reaction of Danishefsky’s Diene with Keto Esters

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0945
Direct syn-Selective Asymmetric Mannich-Type Reaction

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0946
Copper-Catalyzed Asymmetric 1,4-Additions to α,β-Unsaturated Lactones

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0947
Allylic Sulfonamides via a Palladium-Catalyzed Rearrangement of Allylic Carbonates

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0948
Selective Synthesis of Secondary Alkyl Fluorides

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0949
Asymmetric Hydrogenation of Disubstituted Furans

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0950
Enantioselective Rh-Catalyzed Additions to Cyclic N-Sulfamidate Ketimines

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0951
Enantioselective Copper-Catalyzed Decarboxylative Propargylic Alkylation

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0952
Diastereoselective Gold-Catalyzed Cycloisomerization of Enediynes

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0953
Carboetherification–Intermolecular Heck-Type Coupling

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0954
Asymmetric Friedel–Crafts Alkylation Catalyzed by Copper

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0955
Enantioselective Alkylative Ring Opening Catalyzed by Rhodium

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0956
Enantioselective Aminolactonization by Means of Copper Catalysis

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0957
Scandium-Catalyzed Enantioselective Epoxidation of 2-Arylidene-1,3-diketones

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0958
Polyenes via Palladium- and Chromium-Catalyzed Allylic C–H Olefination

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0959
Synthesis of Chiral Cyclic Allylic Amines via Rhodium-Catalyzed Hydrogenation

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Metal-Mediated Synthesis
z961
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0961
Copper-Catalyzed Trifluoromethylthiolation

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0962
Copper-Mediated Three-Component Reaction

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0963
Stereospecific Coupling of Aromatics with Secondary and Tertiary Boronates FREIER ZUGRIFF

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0964
Arylboration by Cooperative Pd/Cu Catalysis

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0965
Gold-Catalyzed Cross-Coupling of Aryl Boronic Acids

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0966
Cobalt-Catalyzed Migratory Arylzincation

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0967
trans-Diborylation of Propargylic Alcohols

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0968
Cyclotrimerization of Alkynes Mediated by n-BuLi–Ti(Oi-Pr)₄

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0969
Synthesis of Allenyl Boronates by Pd/Cu Catalysis

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0970
Amide-Directed C–NMe₂ Bond Activation and C–C Coupling Reactions

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0971
Lead-Mediated Arylation Using Aryl Azides for the Synthesis of 3H-Indoles

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0972
SmI₂-Induced Umpolung of Glycals

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0973
Nickel-Catalyzed Regioselective 1,4-Addition of Organoboronic Acid to Dienones

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0974
Zinc-Mediated C–H Activation of THF

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0975
Tandem Divergent Catalysis using Nitriles

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Organo- and Biocatalysis
z977
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0977
Catalytic Enantioselective [2+2] Intermolecular Photocycloaddition FREIER ZUGRIFF

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0978
Desymmetrization of Cyclohexadienones via Dienamine Catalysis

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0979
Metal-Free Arylation via a [3,3]-Sigmatropic Rearrangement

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0980
Stereoselective 1,2-Dibromination of Olefins Catalyzed by Ph₃PO

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0981
Lewis Base Catalyzed Enantioselective Sulfenoamination of Olefins

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0982
(+)-trans-Dyhydrolycoricidine via an Organocatalytic Michael–Aldol Sequence

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0983
Diastereodivergent Synthesis of Tetrasubstituted Cyclohexanes

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0984
Cooperative N-Heterocyclic Carbene–Chiral Phosphate Organocatalysis

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0985
Highly Enantioselective Route to Chromenes

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0986
Organocatalytic Asymmetric Hydrolysis of Epoxides

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0987
Preparation of (S)-CHBE by Bioreduction–Optimization and Scale-up

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0988
Esterase-Catalyzed Desymmetrization of a meso-Diester

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Polymer-Supported Synthesis
z989
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0989
An Immobilized Cobalt Complex for Alkyne-Tagged Peptide Enrichment FREIER ZUGRIFF

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0990
Cyanation of Aryl Halides with K₄[Fe(CN)₆] Using ZnO-Pd Nanoparticles

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0991
Core–Shell Palladium Nanocatalysts for the Oxidation of Alcohols

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0992
Palladium-Catalyzed Hydrogenation Using a Continuous Flow System

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0993
Cycloaddition of CO₂ to Epoxides Using Polymer-Supported NHC–Zn

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0995
Immobilized Rhodium Catalysts for Asymmetric Hydroformylation of Alkenes

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0996
Synthesis of Benzoxazoles and Benzimidazoles Using Au/TiO₂

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0997
Amide Condensation with MCF-Supported Boronic Acids

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0998
N-Methylation of Secondary Amines with CO₂ and H₂ Using Pt-MoO_x/TiO₂

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0999
Preparation of Indoles and Indolines via Pd/C-Mediated Cross-Couplings

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1000
Synthesis of 5-Substituted 1H-Tetrazoles Using Ln(OTf)₃–SiO₂

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1001
Oxidative Dimerization of Thioamides Using Phosphovanadomolybdic Acid

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1002
C3-Formylation of Indoles Using CAN-SiO₂

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