Synfacts

Issue 07 · July 2014

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Synform
A88
SYNFORM ISSUE 2014/07
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PDF (748 kb)
Synthesis of Natural Products and Potential Drugs
z663
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PDF (421 kb)
0663
Enantioselective Total Synthesis of (+)-Nocardioazine A

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PDF (111 kb)
0664
Synthesis of PSI-6130, the Nucleoside Core of Sofosbuvir

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PDF (137 kb)
0665
Synthesis of an Estrogen Receptor Beta Agonist
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PDF (162 kb)
0666
Synthesis of (+)-Liphagal

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PDF (127 kb)
0667
Total Synthesis of (–)-Filiformin
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PDF (130 kb)
0668
Synthesis of MET Kinase Inhibitor LY2801653

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PDF (126 kb)
0669
Short Stereodivergent Synthesis of Three Aromadendrane Hydroazulenes

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PDF (125 kb)
0670
Synthesis of (–)-Walsucochin B

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PDF (109 kb)
0671
Synthesis of GK–GKRP Disruptor AMG-3969

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PDF (118 kb)
0672
Synthesis of Efinaconazole

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PDF (130 kb)
0673
Synthesis of Evacetrapib

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PDF (117 kb)
0674
Total Synthesis of (−)-Lepenine

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PDF (119 kb)
0675
Total Synthesis of Panaginsene

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PDF (110 kb)
0676
Synthesis of DPP-4 Inhibitor Omarigliptin

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PDF (118 kb)
Synthesis of Heterocycles
z677
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PDF (342 kb)
0677
Synthesis of Azepines by HSbF₆-Catalyzed Cycloaddition of Aziridines with Acetylenes

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PDF (107 kb)
0678
F₃C-Containing Phenanthridines by Palladium-Catalyzed Intramolecular Cyclization

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PDF (114 kb)
0679
Azoloquinazolines from ortho-Triazoloanilines Using an Isocyanide Linchpin

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PDF (111 kb)
0680
Asymmetric Arylative Cyclization of 5-Alkynones with Arylboronic Acids

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PDF (97 kb)
0681
Synthesis of β-Lactones via Intramolecular Rhodium-Catalyzed Cyclization

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PDF (126 kb)
0682
Synthesis of 4-Alkyl-2,3-difluorobut-2-enolides by Cyclization

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PDF (115 kb)
0683
Dihydro-oxazinones from Salicylamides

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PDF (106 kb)
0684
3-Methylene-1-pyrrolines from N-Propargylic β-Enaminones

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PDF (128 kb)
0685
Gold-Catalyzed Synthesis of Thiazoles via Methanesulfonyloxymethyl Ketones

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PDF (117 kb)
0686
Palladium-Controlled Regioseletive Arylative Cyclization of Alkynols to Cyclic Ethers

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PDF (107 kb)
0687
Hydroisoquinolines via Organocatalytic Diels–Alder/Nucleophilic Ring Closure

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PDF (107 kb)
0688
Heterocyclic-Fused Benzopyrans by Heck-Type Reaction

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PDF (106 kb)
0689
Synthesis of Trifluoromethyl-Containing Imidazoles

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PDF (116 kb)
0690
Transition-Metal-Free Synthesis of Indazoles and Azaindazoles

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PDF (106 kb)
0691
Triazolopyridines by Metal-Free Heteroannulation

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PDF (106 kb)
Synthesis of Materials and Unnatural Products
z693
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PDF (315 kb)
0693
Surprising Stability: New Diaryltetraynes

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PDF (97 kb)
0694
Novel Azaheptacenes from Two-Directional Cyclizations

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PDF (105 kb)
0695
Amorphous Modular Polyamides via Ugi Four-Component Reaction

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PDF (115 kb)
0696
A Copper-Catalyzed Dimerization Approach to Chrysene Derivatives

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PDF (104 kb)
0697
Carboranes, Meet Carbenes; Carbenes, Meet Carboranes

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PDF (109 kb)
0698
Direct Functionalization of Thiophene-Fused Borepins

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PDF (114 kb)
0699
Fluoranthenes and Acenes Synthesized from Diol–Diene Cycloaddition

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PDF (109 kb)
0700
Oligonaphthofurans: Molecular Fans

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PDF (122 kb)
0701
The Return of Tetravinylethylene

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PDF (104 kb)
0702
Nitrogen at the Center: Tristriazolotriazines from Tetrazoles

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PDF (102 kb)
0703
‘ROMPing Around’: Paracyclophane Monomers for Poly(para-phenylenevinylene)s

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PDF (110 kb)
0704
A Simplified Synthesis of Siloles

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z705
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PDF (656 kb)
0705
Gold(I)-Catalyzed Asymmetric Cycloadditions

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PDF (106 kb)
0706
Ligand-Controlled Palladium-Catalyzed E- and Enantioselective Allylic Alkylation

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PDF (125 kb)
0707
Chiral Triarylmethanes via an Enantiospecific Palladium-Catalyzed Cross-Coupling
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PDF (129 kb)
0708
Spirocyclization in Air Catalyzed by an Iron-Salen Complex

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PDF (108 kb)
0709
Asymmetric Ring Opening–Cross-Metathesis of Cyclobutene-diols

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PDF (110 kb)
0710
Indolines via Asymmetric Copper-Mediated Inverse-Electron-Demand Aza-DA Reaction

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PDF (129 kb)
0711
Borylation of Chiral Imines Catalyzed by Copper(II)

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PDF (131 kb)
0712
Nickel-Catalyzed Enantioselective Nitro-Mannich Reaction of Isatin Derivatives

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PDF (105 kb)
0713
Gold-Catalyzed Ring-Expanding Cycloisomerization of 1,5-Enynes

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PDF (120 kb)
0714
Asymmetric Allylic Amination of Allylic Esters Catalyzed by Palladium

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PDF (113 kb)
0715
Ruthenium–Porphyrin-Catalyzed trans-Selective Octalone Synthesis

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PDF (111 kb)
0716
Synthesis of Enantioenriched Amines via an Asymmetric Palladium-Catalyzed Arylation

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PDF (118 kb)
0717
Enantioselective Cobalt-Catalyzed Synthesis of [¹⁸F]Fluorohydrins for Use as PET Tracers

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PDF (108 kb)
0718
A Copper-Catalyzed Oxidative Povarov Reaction Towards Polycyclic Amines

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PDF (105 kb)
0719
Asymmetric Copper-Catalyzed Dynamic Kinetic Reactions of Aminocyclopropanes

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PDF (104 kb)
0720
Gold-Catalyzed Synthesis of Heteroaryl Atropisomers

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PDF (100 kb)
0721
Asymmetric Hydroamination Catalyzed by Zinc/Zirconium

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PDF (98 kb)
0722
Asymmetric Tandem Alkylation–π-Allylation of α-Imino Esters

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PDF (134 kb)
0723
Asymmetric Alkene Diamination Catalyzed by Copper

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PDF (108 kb)
0724
Copper-Catalyzed Asymmetric 1,6-Selective Borylation of Dienones and Dienoates

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PDF (121 kb)
0725
Asymmetric Reductive Allylations Catalyzed by Nickel(II)

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PDF (101 kb)
0726
Asymmetric Conjugate Cyanation Catalyzed by Magnesium

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PDF (118 kb)
0727
Enantioselective Michael Addition of Nitroalkenes Using a Cobalt Complex

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PDF (113 kb)
0728
Allylsilanes in Asymmetric Inverse-Electron-Demand Hetero-DA Reactions

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PDF (127 kb)
0729
Asymmetric Allylic Substitution Catalyzed by Pd−Thioether−Phosphite

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PDF (112 kb)
0730
Enantioselective Azahelicenes via Intramolecular Hydroarylation of Alkynes
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PDF (128 kb)
0731
Copper(II)-Catalyzed Silylation of Activated Alkynes

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PDF (137 kb)
0732
Asymmetric Ruthenium-Catalyzed Hydrogenation of Trifluoromethyl Ketimines

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PDF (115 kb)
0733
Copper-Catalyzed Intermolecular Three-Component Oxyarylation of Allenes

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PDF (106 kb)
Metal-Mediated Synthesis
z735
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PDF (348 kb)
0735
Iron-Catalyzed Direct Arylation Using a Triazole Directing Group

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PDF (100 kb)
0736
The Remarkable Role of Salt in the Cross-Coupling of Arylzincs

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PDF (95 kb)
0737
C–H Zincation of (Hetero)Arenes Followed by Copper-Catalyzed Amination
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PDF (123 kb)
0738
Stereocontrolled Synthesis of β-Hydroxy-α-Amino Acid Derivatives

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PDF (132 kb)
0739
Synthesis of Enantioenriched α-Bromo-α-Fluoro-β-Lactams

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PDF (128 kb)
0740
The Versatility of Ynimines

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PDF (98 kb)
0741
Trifluoromethylthiolation of Diazoesters

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PDF (109 kb)
0742
α-Amino Acid Synthesis from CO₂ and N-Acyl-N,O-acetals

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PDF (124 kb)
0743
Selective Addition of Organometallics to 3-Geminal Bis(silyl) N-Acyl Pyridinium

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PDF (102 kb)
0744
A Novel Oxacycle Synthesis

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PDF (99 kb)
0745
BF₃-Mediated Synthesis of Amides

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PDF (101 kb)
0746
Palladium-Catalyzed Hydrofluorination of Alkenylarenes

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PDF (105 kb)
0747
Iron-Catalyzed Friedel–Crafts-Type Alkylation of Secondary Alcohols

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PDF (97 kb)
0748
Titanium(III)-Catalyzed Acyloin-Type Cross-Coupling

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PDF (124 kb)
0749
Trifluoromethylthiolation of Benzofuranes and Benzothiophenes

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PDF (99 kb)
Organo- and Biocatalysis
z751
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PDF (335 kb)
0751
Oxidative α-Amination of β-Ketocarbonyls Catalyzed by a Primary Amine

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PDF (134 kb)
0752
A Direct β-Alkylation of Aldehydes via Photoredox Organocatalysis

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PDF (127 kb)
0753
Catalytic Asymmetric Synthesis of 8-Oxabicyclooctanes

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PDF (106 kb)
0754
Organocatalytic Asymmetric Trifluoromethylthiolation of Oxindoles

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PDF (108 kb)
0755
Photoredox Organocatalytic Anti-Markovnikov Hydroamination of Alkenes

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PDF (118 kb)
0756
Catalytic Enantioselective [2+2] Photocycloaddition of Alkenylcoumarins

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PDF (116 kb)
0757
Enantioselective Friedel–Crafts Reaction of Furylacetones

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PDF (114 kb)
0758
Brønsted Acid Catalyzed Oxidative Addition of Ketone Radicals to Olefins

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PDF (134 kb)
0759
Tetrahydroisoquinolines via Asymmetric Aminocatalytic [3+2] Cycloaddition

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PDF (122 kb)
0760
Asymmetric Catalysis on the Nanoscale

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PDF (121 kb)
0761
Organocatalytic Synthesis of Atropisomers

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PDF (102 kb)
0762
Formal [5+3] Cycloaddition via Cascade Dienamine–Dienamine Catalysis

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PDF (119 kb)
Polymer-Supported Synthesis
z763
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PDF (377 kb)
0763
Pyranopyrazole Synthesis with Iron Oxide Nanoparticles

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PDF (112 kb)
0764
Synthesis of Chiral Phthalides Using a Silica-Supported Rhodium Catalyst

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PDF (105 kb)
0765
Oxidation of Secondary Alcohols with UiO-66-Cr MOF Catalyst
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PDF (130 kb)
0766
C–N, C–O, and C–C Bond-Forming Reactions with NiFe₂O₄ Nanoparticles

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PDF (104 kb)
0767
S-Arylation of Thiophenols with Aryl Halides Using Pd_np-nSTDP

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PDF (107 kb)
0768
α-Alkylation of Ketones with Trialkylamines Using Palladium on Carbon

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PDF (123 kb)
0769
1,4-Hydrogenation of α,β-Unsaturated Carbonyls with [Au]-TPDI-Rh

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PDF (128 kb)
0770
Asymmetric Addition and Hydrogenation Using BINAP-MOF

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PDF (120 kb)
0771
Amidation of Aryl Halides with Isocyanides Catalyzed by PS-Pd-NHC

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PDF (123 kb)
0772
Transfer Hydrogenation of Nitroarenes with N₂H₄·H₂O Using SS-Rh Nanoparticles

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PDF (105 kb)
0773
Synthesis of Substituted Benzoxazoles Using CuFe₂O₄ Nanoparticles

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PDF (102 kb)
0774
Mukaiyama Aldol Reaction Using Ion-Exchanged Montmorillonite Clay

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PDF (99 kb)
0775
Unsymmetrical Diyne Synthesis via Solid-Phase Glaser–Hay Coupling

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PDF (104 kb)
0776
Heck and Sonogashira Reactions Using PVC-Supported Palladium Nanoparticles

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PDF (102 kb)
0777
Synthesis of Alkynyl Chalcogenides Catalyzed by Magnetite Nanoparticles

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PDF (97 kb)
Erratum
0778
Direct Borylation of Arenes Catalyzed by Ir(I)-bpy-PMO

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PDF (108 kb)

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