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Synthesis 2004(17): 2942-2942
DOI: 10.1055/s-2004-834886
DOI: 10.1055/s-2004-834886
ADDENDA
© Georg Thieme Verlag Stuttgart · New YorkThe First Synthesis of 1,1-Dinitrocyclopropane
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Publication History
Publication Date:
19 November 2004 (online)
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In the typical procedure given for the reaction of diazomethane with trinitromethane, the sentence ‘Then the mixture was concentrated to give 1.30 g of a yellow oil consisting of 1 and 2 in the ratio 7:3 (as shown by 1H NMR)’ should instead read ‘The described synthesis was run four times and the combined reaction mixtures were concentrated to give 1.30 g of a yellow oil consisting of 1 and 2 in the ratio of 7:3 (as shown by 1H NMR)’.
The authors apologize for this omission.