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Synlett 2001; 2001(9): 1479-1481
DOI: 10.1055/s-2001-16779
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Diastereoselective Titanocene-Catalyzed Oxidative Cyclization of Bishomoallylic Alcohols

Alessandra Lattanzi* , Giorgio Della Sala, Maurizio Russo, Arrigo Scettri
  • *Dipartimento di Chimica, Università di Salerno 84081 Baronissi (Salerno), Italy; Fax + 39(0)89-96 52 96; E-mail: lattanzi@unisa.it
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Publication History

Publication Date:
28 August 2001 (online)

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Bishomoallylic alcohols are converted in good yields and diastereoselectivity into tetrahydrofuranols and tetrahydropyranols by Cp2TiCl2/t-butyl hydroperoxide/activated 4 Å molecular sieves system.

epoxidation - cyclization - metallocenes - tetrahydrofuranols - tetrahydropyranols

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