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Synlett 1999; 1999(6): 759-761
DOI: 10.1055/s-1999-2720
DOI: 10.1055/s-1999-2720
letter
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Synthesis and Lipase-Catalyzed Enantiotope Selective Acetylation of 2-Benzoyloxy-1,3-propanediol
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Publication History
Publication Date:
31 December 1999 (online)
Preparation and porcine pancreatic lipase (PPL)-catalyzed enantiotope selective acetylation of the prochiral 2-benzoyloxy-1,3-propanediol (1a) is described. The reaction with PPL and vinyl acetate gave monoacetate (2a) of 96% e.e.
2-O-benzoylglycerol - enantiotope selective - acetylation - lipase