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Synlett 1999; 1999(5): 553-554
DOI: 10.1055/s-1999-2673
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A Novel One-pot Method for Reductive Conversion of Azides to Acyl Amines with Acetic Anhydride and Trimethyl Chlorosilane

Apurba Barua* , Ghanashyam Bez, Nabin C. Barua
  • *Natural Products Chemistry Division, Regional Research Laboratory, Jorhat-785006, Assam, India; Fax +91-(03 76)32 11 58
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Publication Date:
31 December 1999 (online)

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A combination of acetic anhydride and chloro-trimethylsilane has been shown to effect the conversion of a variety of azides to the corresponding acetylated amines in excellent yields without affecting other functional groups such as ether, ester, halide etc.

azide - acyl amines - trimethyl chlorosilane - acetic anhydride

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