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Synthesis 1996; 1996(11): 1345-1349
DOI: 10.1055/s-1996-4390
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Synthesis of Racemic Ethanolamine Plasmalogen

Hans Rudolf Pfaendler* , Volker Weimar
  • *Institute of Organic Chemistry, University of Munich, Karlstrasse 23, D-80333 Munich, Germany, Fax +49(89)5902483; E-mail hrp@org.chemie.uni-muenchen.de
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Publikationsdatum:
31. Dezember 2000 (online)

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Racemic C12-ethanolamine plasmalogen 5b was prepared in high yield. The amino group was generated by selective reaction of azide 4b with polymeric triphenylphosphine followed by mild hydrolysis of the intermediate phosphine imine. A novel universal phosphorylation reagent 2-azidoethyl dichlorophosphate (7) was used.

plasmalogen - synthesis - ethanolamine-phospholipids - 2-azidoethyl dichlorophosphate - polymeric triphenylphosphine