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Synlett 1995; 1995(10): 1017-1020
DOI: 10.1055/s-1995-5164
DOI: 10.1055/s-1995-5164
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Solid Phase Synthesis of Bicyclo[2.2.2]octane Derivatives via Tandem Michael Addition Reactions and Subsequent Reductive Amination
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Publication History
Publication Date:
31 December 2000 (online)
Tandem Michael addition reactions of polymer bound acrylates with cyclohexenones and subsequent reductive amination was achieved, which after cleavage from the support under reductive, acidolytic or aminolytic conditions afforded a wide variety of bicyclo[2.2.2]octanes. The process may find application in combinatorial library synthesis.
Solid Phase Synthesis - Tandem Michael Addition - Reductive Amination