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Synlett 1995; 1995(9): 987-988
DOI: 10.1055/s-1995-5145
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Generation and Carbonyl Addition of Dibromofluoromethyllithium

Manabu Kuroboshi* , Nobuko Yamada, Yoko Takebe, Tamejiro Hiyama
  • *Department of Applied Chemistry, Faculty of Engineering, Okayama University, Tsushima-naka 3-1-1, Okayama, Okayama 700, JAPAN (mkurohos@cc.okayama-u.ac.jp)
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Publication Date:
31 December 2000 (online)

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When CFBr3 was treated with n-BuLi at -130 °C, thermally labile LiCFBr2 was generated which reacted smoothly with a coexisting electrophile RR’CO to give an adduct RR’C(OH)CFBr2 in good yield.

carbenoid - halofluoromethane - carbonyl addition - halohydrin - fluorinated alcohol

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