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Synlett 1995; 1995(4): 323-324
DOI: 10.1055/s-1995-4958
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Preparation of Oxepanes by Iodoetherification

Yves Brunel, Gérard Rousseau*
  • *Laboratoire des Carbocycles, URA CNRS 478, Institut de Chimie Moléculaire d’Orsay, Bât. 420, 91405 Orsay Cedex, France
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Publication History

Publication Date:
31 December 2000 (online)

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Reaction of 6-hepten-1-ols with bis(sym-collidine) iodine (I) hexafluorophosphate in methylene chloride leads in high yields to the formation of oxepanes.

Iodoetherification - oxepane - oxocane - oxirane

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