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Synthesis 1994; 1994(6): 624-628
DOI: 10.1055/s-1994-25536
DOI: 10.1055/s-1994-25536
paper
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved.
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data processing and storage.Deoxygenation of Aliphatic Alcohols via Reduction of New Thioxocarbamate Derivatives
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Publikationsverlauf
Publikationsdatum:
17. September 2002 (online)

N-Acylthioxocarbamates, obtained by the reaction of alcohols with acyl isothiocyanates, were reduced by tributylstannane or triphenylsilane under radical conditions to give deoxygenated products of the corresponding alcohols in good yields. An application to regioselective deuteration using tributyldeuteriostannane is also examined.