Synthesis of C-Disaccharides by a Samarium Diiodide Induced Intramolecular Coupling Reaction of Tethered Sugars

Alain Chénedé; Elisabeth Perrin; El Djouhar Rekaï; Pierre Sinaÿ

doi:10.1055/s-1994-22872

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Synlett 1994; 1994(6): 420-422
DOI: 10.1055/s-1994-22872

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Synthesis of C-Disaccharides by a Samarium Diiodide Induced Intramolecular Coupling Reaction of Tethered Sugars

Alain Chénedé^* , Elisabeth Perrin, El Djouhar Rekaï, Pierre Sinaÿ

^*Ecole Normale Supérieure, Département de Chimie, URA 1686, 24 Rue Lhomond, F-75231 Paris Cedex 05, France

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Publication Date:
18 September 2002 (online)

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C-disaccharides 7 and 14 were expeditiously synthesized by Sml₂ promoted radical coupling of glucosyl phenyl sulfones 4 and 13 onto the temporarily tethered exomethylene sugar 5.

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