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Synlett 1994; 1994(3): 217-218
DOI: 10.1055/s-1994-22801
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Electrochemical Generation of C-N-C 1,3-Dipole Leading to Pyrrolidine Skeleton

Sigeru TORII* , Hiroshi OKUMOTO, Akiko GENBA
  • *Department of Applied Chemistry, Faculty of Engineering, Okayama University, Tsushima-Naka, Okayama 700, JAPAN
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Publication Date:
22 March 2002 (online)

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Electrochemical oxidation of N,N-bis(TMSmethyl)benzyl amine in a DMF/AcONa/(C)-(C) system using an undivided cell at room temperature generated a C-N-C 1,3-dipole, which underwent cycloaddition with electron deficient olefins to give pyrrolidine derivatives.

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