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Synlett 1993; 1993(3): 193-194
DOI: 10.1055/s-1993-22397
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1-[(Hydroxy)(trifyloxy)iodo]-4-[(phenyl)(trifyloxy)iodo]benzene as a Reactive Organoiodine(III) Reagent: Isolation and Characterization

Tsugio Kitamura* , Ryuji Furuki, Kensuke Nagata, Lei Zheng, Hiroshi Taniguchi
  • *Department of Chemical Science and Technology, Faculty of Engineering, Kyushu University 36, Hakozaki, Fukuoka 812, Japan
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Publication History

Publication Date:
19 March 2002 (online)

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The title bisiodine(III) reagent was prepared and isolated as stable crystals from the reaction of iodosylbenzene (PhIO) with trifluoromethanesulfonic (triflic) acid (TfOH) or with triflic anhydride (Tf2O).