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Synthesis 1989; 1989(3): 204-205
DOI: 10.1055/s-1989-27198
DOI: 10.1055/s-1989-27198
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Synthese von Tricyclohexylphosphoniumbromiden aus einem luftstabilen Phosphinderivat
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Publication History
Publication Date:
17 September 2002 (online)
Synthesis of Tricyclohexylphosphonium Bromides from an Air-Stable Phosphine Derivative Reaction of tricyclohexylphosphine-carbon disulfide complex 5 with primary alkyl bromides 4 produces tricyclohexylphosphonium bromides 1 in good yields, making isolation of the phosphine 3 unnecessary. In two cases for 4g, h, rearranged products were obtained.