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Synthesis 1987; 1987(5): 508-509
DOI: 10.1055/s-1987-33426
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A Convenient Method for the Synthesis of 1-Adamantyldichlorophosphine

Maryse Gouygou* , Guita Etemad-Moghadam, Max Koenig
  • *Laboratoire de Synthèse, Structure et Réactivité de Molécules Phosphorées U.A. 454, Université Paul Sabatier, 118, Route de Narbonne, F-31062 Toulouse, France
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Publication Date:
18 September 2002 (online)

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1-Adamantyldichlorophosphine is obtained in good yield by reduction of 1-adamantyldichlorophosphine sulfide with triphenylphosphine in toluene. It can be quantitatively reduced to 1-adamantylphosphine with lithium alanate in ether.

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