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Synthesis 1987; 1987(9): 841-843
DOI: 10.1055/s-1987-28097
DOI: 10.1055/s-1987-28097
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Synthese von α-Halogen-ω-alkylthio-alkanen und α,ω-Bisalkylthio-alkanen
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Publication History
Publication Date:
12 September 2002 (online)
Synthesis of α-Halogeno-ω-alkylthioalkanes and α,ω-Bisalkylthioalkanes The reaction of α,ω-dihalogenated alkanes [X(CH2)nX,,n = 3 - 10]with alkylthiolates affords α-halogeno-ω-alkylthioalkanes 1 as well as α,ω-bisalkylthioalkanes 2. Products 1 (40 examples) and 2 (22 examples) are easily isolated in good yields by flash chromatography.