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Synthesis 2010(16): 2703-2704
DOI: 10.1055/s-0029-1218852
DOI: 10.1055/s-0029-1218852
SHORTPAPER
© Georg Thieme Verlag
Stuttgart ˙ New YorkA Convenient Procedure for the Preparation of Bis(dialkylamino)malononitriles
Further Information
Received
18 March 2010
Publication Date:
29 June 2010 (online)
Publication History
Publication Date:
29 June 2010 (online)
Abstract
N,N,N′,N′-Tetraalkylchloroformamidinium chlorides react with trimethylsilyl cyanide without solvent to give bis(dialkylamino)malononitriles, which can be distilled off from the reaction mixture in vacuo.
Key words
iminium salts - N,N,N′,N′-tetraalkylchloroformamidinium chlorides - trimethylsilyl cyanide - bis(dialkylamino)malononitriles
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