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Synthesis 1990; 1990(12): 1149-1151
DOI: 10.1055/s-1990-27120
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Organic Electronic Conductors and Precursors;1 Reaction of Hexasodium Benzene-hexathiolate and Benzenehexathiol with Carbon Disulfide

A. M. Richter* , N. Beye, E. Fanghänel
  • *Technical University, Carl Schorlemmer Leuna-Merseburg, Department of Chemistry, Merseburg, DDR-4020 Germany
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Publication Date:
02 May 2002 (online)

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The reaction of hexasodium benzenehexathiolate (1) and benzenehexathiol (7) with carbon disulfide is studied. Depending on the reaction conditions and the molar ratio of 1 or 7 to carbon disulfide the 1,3-benzodithiole-2-thiones 6, the 2,6-dithioxobenzo[1,2-d: 4,5-d′]- 5, the 2,5-dithioxobenzo[1,2-d: 3,4-d′]bis[1,3]dithiole 9 or the 2,5,8-trithioxobenzotris[1,3]dithiole (2) are obtained.

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