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Synthesis 1988; 1988(10): 808-810
DOI: 10.1055/s-1988-27717
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Oxidation of Primary Aliphatic Amines to C-Nitroso Dimers

Walter W. Zajac, Jr.* , Thomas R. Walters, James M. Woods
  • *Department of Chemistry, Villanova University, Villanova, PA 19085, USA
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Publikationsdatum:
12. September 2002 (online)

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A biphasic system of ethyl acetate or dichloromethane and water containing sodium percarbonate (Na2CO3·3/2 H2O2), sodium hydrogen carbonate and N,N,N′,N′-tetraacetylethylenediamine oxidizes primary aliphatic amines to aliphatic C-nitroso dimers in most cases in good to excellent yields.

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