Synfacts
Issue 11 · November 2024
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SYNFORM
ISSUE 2024/11
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Synthesis of Natural Products
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1121
Total Synthesis of (+)-Strepsesquitriol
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1122
Synthesis of (–)-Fasicularin
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1123
Total Synthesis of (−)-Cyathin B
2
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1124
Total Synthesis of (+)-Quadrigemine H
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1125
Total Synthesis of (–)-Cyctetryptomycin A and B
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1126
Total Synthesis of (–)-Euphordraculoate A and (+)-Pedrolide
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1127
Total Synthesis of (±)-11-
O
-Debenzoyltashironin
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Synthesis of Heterocycles
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1129
Ethylene Sulfate: A Two-Carbon Synthon for a Modular Synthesis of Morpholines
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1130
Tandem Synthesis of 1,3-Oxazepine from 5-Benzylidine Meldrum's Acids and TosMIC
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1131
Substrate-Controlled
ortho
-Amination of Complex (Hetero)Arene Derivatives
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PDF (79 kb)
1132
Multi-Kilogram Synthesis of a Complex Cyclopropyl Pyrazole from (
R
)-Epichlorohydrin
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1133
Modular Diversification to Rapidly Access Substituted 1,6-Naphthyridines
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1134
Enantioselective Synthesis of 2-Oxazolidinones Using Organoselenium Catalysis
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1135
Access to 1-Azabicyclo[2.1.1]hexanes as Potential Bioisosteres for 3-Substituted Pyridines
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1136
Resolution of Atropisomers through Organocatalyzed Knoevenagel Reaction
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1137
Modular, Sustainable Syntheses of Novel N-Hetero-cyclic Compounds through Regenerative Cyclization
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1138
Versatile Two-Step Catalytic Stereoselective Approach to Chiral
anti
-2,4-Tetrahydrofuran Derivatives
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PDF (91 kb)
1139
Atom-Efficient [2+2+2] Rhodium-Mediated Cycloaddition for the Synthesis of Chiral Tetrahydroindoles
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1140
Synthesis of 1,2,4-Oxadiazole-5-thiones and Thioamides
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1141
Facile Access to γ-Functionalized α-Amino Acid Derivatives
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Synthesis of Materials and Unnatural Products
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1143
When Cycloaddition Met Mechanochemistry
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1144
A Buckybowl with a “Handle”
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1145
Nitrogen-Rich Nanographene
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1146
Iron-Catalyzed Aza-annulation via C(
sp
²)–H Activation
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1147
Alternating Radical Stitching Polymerization
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1148
Proton Transfer Anionic Polymerization
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1149
Aromaticity Featuring a B=B Bond
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1150
An Extended, Split Azulene
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1151
Cyclooligomerization of Fluorene via C–H Activation
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1152
A Forgotten Borole: 1-Boraindene
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1153
Metal-Free Syntheses of π-Extended Triazatrinaphthylenes and 2D Materials
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1154
Palladium-Catalyzed Hydroaminocarbonylative Polyaddition
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Metals in Synthesis
z1155
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1155
Silyl-Directed Borylative C–H Functionalization of Arenes
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1156
Nickel-Catalyzed Cross-Coupling of Cyclic Sulfones and Grignard Reagents
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1157
Mechanistic Investigation into Three-Component Carboamination
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1158
Palladium-Catalyzed Synthesis of
anti
-Selective Cyclopropanes
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1159
Markovnikov Hydroarylation via a Cobalt/Nickel Cocatalyzed Photochemically Induced System
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1160
Synthesis of Functionalized Indenes via Palladium/Blue Light Catalyzed Skeletal Rearrangement
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1161
Selective Functionalization of Monoactivated Bisboronates via Copper Catalysis
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1162
Secondary Phosphine Oxide/Palladium-Catalyzed α-Deuteration of Pyridine C–H Bonds
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1163
Benzoxazinone Synthesis via Double Alkyne Incorporation Using Gold Catalysis
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1164
Palladium-Catalyzed Isomerization of Propargyl Allylic Alcohols via β-Alkynyl Elimination
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1165
Negishi-Type Cross-Coupling Reaction of a CF
2
H Reagent and Aryl Thianthrenium Salts
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1166
Synthesis of Enantioenriched Organofluorides by Nickel-Catalyzed Hydroalkylation of Fluoroalkenes
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1167
Regioselective Three-Component Carboamination of Propargylic Alcohols to Access N,O-Heterocycles
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1168
Asymmetric Intramolecular Hydroamination of 2,4-Dienyl Hydrazones by Pd(0)/Brønsted Acid Cocatalysis
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1169
Synthesis of Chiral α-Alkyl Succinimides by Palladium-Catalyzed Migratory Hydroamidocarbonylation
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1170
C(sp
2
)–CN Cross-Coupling by Ligand-Enabled Gold(I)/Gold(III) Redox Catalysis
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1171
Synthesis of Isotopically Labelled Alkyl Aryl Ketones by Nickel-Catalyzed Carbonylative Cross-Coupling
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1172
Cobalt-Catalyzed Carbonylative Cyclization of Homoallylic Alcohols and Amines
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1173
Direct C(sp
2
)–H Arylation and Alkynylation of Allenes under Copper Catalysis via Hydrogen Atom Abstraction
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1174
Aromatic Ketones as Aryl Electrophiles in Metal-Catalyzed Deacylative Cross-Coupling Reactions
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1175
Stereoselective Cyclization of 1,6-Enynes via Reductive Nickel Catalysis
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1176
Palladium-Catalyzed α-Arylation of α-Vinyl Boronates
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1177
Asymmetric α‑Vinylation of γ‑Lactams
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1178
Access to α,β-Unsaturated Carboxylic Acids by Iridium-Catalyzed Transfer Dehydrogenation
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1179
Take Sulfones Instead of Carbenes: Cyclopropanation of Allylic Alcohols under Manganese Catalysis
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1180
Synthesis of 2,3-Disubstituted Indoles via Palladium Catalysis
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Polymer-Supported Synthesis
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1181
Asymmetric Michael Addition Catalyzed by a Polyisocyanide-Based Porous Polymer
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1182
Photocatalytic C–H Arylation of Heteroarenes with Arylamines Using Fe
3
O
4
Nanoparticles
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1183
Synthesis of Fluoroalkylated Indolines Using Molten-Salt Carbon Nitride Photocatalysts
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1184
Continuous-Flow C–H Amidation of 2-Phenylpyridines Catalyzed by a Cp*Rh(III) Catalyst Supported on Silica
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1185
Indole Synthesis through Intramolecular Heck Reaction with
in situ
Generated Pd Nanoparticles in PEG
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1186
CdS Nanosheets-Catalyzed Formation of Imines and Amines by Photoreductive Coupling Reactions
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1187
Mechanochemical Oxidative Heck-Type Reaction Assisted by Cyclodextrin
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1188
Controlled Hydrogenation of Alkynes Using Ni
2
P Nanoparticles Supported on Al
2
O
3
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1189
Hydrogenation of Nitriles Using Co Nanoparticles
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1190
Hydrocarboxylation of Terminal Alkenes with Formate by a ZnIn
2
S
4
Photocatalyst
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1191
RhRu Bimetallic Cluster Catalysts for Dehydrogenative Cross-Coupling of Arenes and Carboxylic Acids
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Organo- and Biocatalysis
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1193
Enzymatic Asymmetric Radical Dearomatization of Electron-Rich Arenes Towards Chiral Spirocycles
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1194
Geometric Preorganization in Small-Molecule Catalysis
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1195
Photocatalytic Azetidine Synthesis via Radical Strain Release of Azabicyclo[1.1.0]butanes
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1196
Enantioselective Borane-Catalyzed Michael Addition of 2-Alkylbenzoxazoles to Electron-Deficient Olefins
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1197
Metallomimicking Phosphorous Complex Enables Catalytic Hydrogenation
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1198
Molecular Editing of Ketones through
N
‑Heterocyclic Carbene and Photo Dual Catalysis
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1199
Heterogeneous Non-covalent Organic Framework Enables Enantio- and Periselective [6+4] Cycloaddition
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1200
The Catalytic Asymmetric Polyene Cyclization of Homofarnesol to Ambrox
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1201
Chiral Lewis Base Catalyzed Dynamic Kinetic Asymmetric Transformation of Chlorosilanes
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Innovative Drug Discovery and Development
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1203
A Novel Method to Incorporate 2,2-Difluoroethyl Group as a Lipophilic Hydrogen-Bond Donor
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1204
Skeletal Editing of Indoles and Pyrroles Enabled by a Novel, Atomic Carbon Equivalent
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1205
Enantioselective and Organocatalytic Sulfenamide
S
-Alkylation
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1206
Amination of Base-Sensitive Aryl Bromides and Divergent Amino Alcohol Arylation Using Cu-Catalysis
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1207
Process Optimization Enables Safer, Greener Synthesis of Valbenazine Ditosylate
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1208
An Enantioselective Synthesis of Azabicyclo[2.1.1]hexanes, sp
3
-Rich Motifs for Drug Design
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1209
Total Synthesis of (–)-Codeine
via
Cascade Double Heck Cyclization
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1210
Boronate-Based Prodrugs for Oxidative Release of Drugs
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1211
Novel Ru-Catalyzed Asymmetric Hydrogenation Enables 100 Kilogram-Scale Synthesis of Brivaracetam
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1212
Late-Stage Pyridine Oxidation
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Oxygen Walking
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1213
Synthesis of
meta
Benzene Isosteres
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1214
Derivatizing and Optimizing
Neo
-Clerodane through Mechanistic SAR Studies
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1215
Thiopyrylium NIR-II Photosensitizer Enables Mitochondria-Localized Dual Pyroptosis and Apoptosis
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1216
Merging Boryl Radical-Mediated Halogen-Atom Transfer and Copper Catalysis for the Alkylation of Amides
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Peptide Chemistry
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1217
Electron-Rich Triaryl Phosphine Mediated Electrochemical Synthesis of Peptides
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1218
meso
- and
l
,
l
-Diaminopimelic Acids: A Stereoselective Synthesis from α-Amino Acids
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1219
Cysteine-Directed Pd-Catalyzed β-C(sp
3
)–H Arylation of Alanine in Linear and Cyclic Peptides
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1220
Radical C–C Coupling Reaction for the Synthesis of CF
3
-Containing Amino Acids
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1221
Synthesis of α-Amino Acids via Iron-Catalyzed 1,3-Nitrogen Migration
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1222
Synthesis of Macrocyclic Peptides via Thioketalization of Cysteine-Containing Peptides
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1223
Hydroalkenylations of Olefins and Styrenes Using Iridium Catalyst via Enamine Formation
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1224
Synthesis of Aminonitriles by Asymmetric Strecker Reaction Using Organocatalysis
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1225
Catalytic Synthesis of Unnatural α/β-Amino Acids and -Peptides
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1226
Methionine-Directed C–H Glycosylation of Peptides Catalyzed by Pd(OAc)
2
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1227
Palladium-Catalyzed Cinnamylation and Decinnamylation of Complex Oligopeptides
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1228
Boronate Synthesis from Lys Derivatives
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1229
Sequential Fluorination and Amidation of Thioesters
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1230
F
CDMT-Mediated Peptide Synthesis
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Flow Chemistry
z1231
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1231
Arylation of Gaseous Alkanes in Flow
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