Synfacts

Ausgabe 11 · November 2020

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Ausgabe
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A153
SYNFORM ISSUE 2020/11 FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
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1257
Total Synthesis of (±)-Aspidofractinine FREIER ZUGRIFF

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1258
Synthesis of Glecaprevir. Part 1 FREIER ZUGRIFF

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1259
Synthesis of Glecaprevir. Part 2

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1260
Synthesis of BMS-986251

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1261
Synthesis of (±)-Walsucochinoids M and N

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1262
Synthesis of Cephanolide A

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1263
Synthesis of (–)-Daphnezomines A and B

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1264
Synthesis of Cebranopadol

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1265
Synthesis of (+)-Phomactin A

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1266
Synthesis of TAK-828F

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1267
Synthesis of MIDD0301

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1268
Synthesis of Tenofovir

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1269
Synthesis of LSZ102

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1270
Synthesis of an Arginase Inhibitor

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1271
Synthesis of (±)-Kopsinitarine E

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1272
Total Synthesis of (±)-Ginkgolide B FREIER ZUGRIFF

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1273
Synthesis of Brensocatib FREIER ZUGRIFF

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Synthesis of Heterocycles
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1275
Isolation and Structural Characterization of Three New Benzazepines

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1276
Chiral Hemiketal Formation by Organocatalytic Desymmetrization of gem-Diols

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1277
Synthesis of Spirocyclic Pyrrolidones from Diazobutyrolactams

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1278
Scalable Synthesis of Functionalized gem-Difluorocyclopropanes

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1279
C–H Bond Functionalization of Alicyclic Amines

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1280
Synthesis of 2-Formylpyrroles from Pyridinium Iodide Salts

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1281
Minisci Reaction of N-Hetarenes with Cyclopropanols as the Radical Source

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1282
Synthesis and Derivatization of N-Trifluoromethylated Indoles

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1283
Mild Regioselective Halogenation of Anilines, Anilides, and Indoles

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1284
Pd-Catalyzed Asymmetric [8+2]-Dipolar Cycloadditions: Synthesis of Ten-Membered Ring Heterocycles

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1285
Cobalt(III)-Catalyzed Synthesis of Isoquinolinones and Pyridinones by Annulative Vinylene Transfer

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1286
Chiral N,O-Acetals by Asymmetric Hydrogenation of Cationic Intermediates

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1287
Metal-Free [5+1]-Cycloaddition Route to Pyrazine 1-Oxides and Pyrazines

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1288
Two-Step Synthesis of Functionalized Benzoxazoles

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Synthesis of Materials and Unnatural Products
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1289
A Missing Member of the Cycloarene Family: Quintulene

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1290
Amide–Alkene Isosterism: Synthesis of Olefin-Containing Foldamers

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1291
Getting the SuFEx Right for Sulfamides

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1292
Reductively Aminate, Reuse, Recycle

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1293
Insert COins Here

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1294
Oxygen Chelation Makes it Exclusive: Fluorene-Based Spirocycles via Aryl Halide Cross-Coupling

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1295
Oxidative Dealkylation Strategy toward Functionalized Phenalenones

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1296
Synthesis of as-Indacenoterrylene, a C₇₀ Fragment with NIR absorption

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1297
Air- and Moisture-Tolerant Synthesis of Catechol Boronic Esters

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1298
Suzuki–Miyaura to the Rescue! Expanding the Scope for Tetraarylethylene Synthesis

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1299
Sticking Together: Fused Porphyrins Deliver Protection against Photodegradation to Pentacenes

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1300
The Coronation of Naphthalene Diimides: π-Extended Helicenes by Oxidative Cyclization

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Metals in Synthesis
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1301
Asymmetric γ-Borylation of Aliphatic Amides and Esters FREIER ZUGRIFF

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1302
Gold-Catalyzed Carbene Transfer towards the C–H Functionalization of N-Heterocycles

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1303
Dynamic Kinetic Resolution Strategy for the Asymmetric Nickel-Catalyzed Capture of Transient Cyclic Allenes FREIER ZUGRIFF

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1304
Visible-Light-Promoted Copper-Catalyzed Difunctionalization of Alkenes with Iodoform

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1305
Chlorocarbonylation of Aryl (Pseudo)Halides via Pd-Catalysis

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1306
Synthesis of δ- and ε-Lactones Through γ-C(sp³)–H Activation of β-Disubstituted Carboxylic Acids

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1307
Ruthenium-Catalyzed Synthesis of Cyclic Tetrasubstituted Olefins

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1308
Synthesis of Cyclopropanes by Double C–H Activation

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1309
Synthesis of C-Aryl Glycosides by Catellani Reaction

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1310
Intermolecular Pd-Catalyzed Carbofunctionalization of Internal Alkynes with trans-Selectivity

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1311
Rh-Catalyzed Three-Component Synthesis of α,α,α-Trisubstituted Esters by C(sp²)–C(sp³) Bond Cleavage

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1312
Photocontrolled Hydroboration of α,β-Unsaturated Ketones

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1313
gem-Hydrogenation of Internal Alkynes by Grubbs Metathesis

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1314
Cobalt-Catalyzed Dienylation of Quinoline-N-Oxides: C8-Selective Alkenylation

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1315
Synthesis of Benzylic Ketones through Electrochemical Oxidation of Aryl Alkenes

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1316
Nickel-Catalyzed Hydroarylation of Alkenes

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1317
Synthesis of Trisubstituted Hydroxylamines

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1318
Regioselective Alkyne Cyclotrimerization Enabled by Hemilability of Salen Ligand

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1319
Asymmetric Allylation of Terminal Alkynes by Rhodium/Copper Catalysis

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1320
Switching Reactivity: Bromoalkynylation of Alkynes and Hydroalkynylation of Haloalkynes via Gold Catalysis

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1321
Palladium-Catalyzed Stereoselective β-Arylation of Acyclic Aliphatic Amides

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1322
Regio- and Enantioselective Synthesis of Chiral Allylic Sulfones

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1323
Sulfinyl Nitrene Based Synthesis of Sulfoximines and Sulfonimidamides

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1324
Asymmetric Synthesis of α‑Alkylated Pyrrolidinones from Homoallylic Carbamoyl Chlorides

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1325
Carbon Dioxide and Ammonia as Cyanide Source in Nickel-Catalyzed Reductive Cyanation of Aryl Chlorides

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1326
Design of a Catalyst Suitable for Aryl Aminations at Room Temperature

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1327
Titanium-Catalyzed Asymmetric Pauson–Khand Type Reaction FREIER ZUGRIFF

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1328
Synthesis of Chiral Alkenylphosphine Oxides

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Polymer-Supported Synthesis
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1329
A Single-Atom Cobalt Catalyst Supported on SBA-15 for Hydrodeoxygenation and Hydrogenation FREIER ZUGRIFF

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1330
Enantioselective Addition of Dialkylzinc to Aldehydes on a Heterogeneous Magnetic Nanoparticle Catalyst

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1331
Photocatalytic C–C Bond Cleavage of Lignin Model Compounds on Silver-Doped Cadmium Sulfide NPs

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1332
Oxidative Amine Coupling and Thioamide Cyclization with a Photocatalytic Covalent Organic Framework

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1333
Hydrodeoxygenation of 4-Hydroxyacetophenones on Immobilized Fe–Ru Bimetallic Nanoparticles

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1334
Synthesis of 2-Amino-3-cyano-4H-chromenes on Graphene Oxide-Supported Piperazine

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1335
Oxidation of Sugar Alcohols Catalyzed by a Polymeric N-Heterocyclic Carbene–Iridium Complex

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1336
Parts Per Million Pd/C-Catalyzed Reductive Aminations in an Aqueous Micellar Medium

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1337
Aerobic C–C Bond Cleavage of Vicinal Diols Promoted by Heterogeneous Carbon Nitride CN620

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1338
Graphite-Supported Cu–Ag Nanoparticle Catalysts for Oxidation and Chan–Lam Coupling

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1339
Cyclopropanation of Olefines Catalyzed N-doped Graphene-Supported Iron Nanoparticles

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Organo- and Biocatalysis
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1341
Chemoenzymatic Dynamic Kinetic Resolution at Normally Static Stereogenic Centers FREIER ZUGRIFF

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1342
TEMPO-Catalyzed Di- and Trifluoromethoxylation of Arenes

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1343
Enzyme-Dependent Oxygenation Permits Highly Selective Synthesis of Diterpenes

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1344
Synthesis of Complex Isoprenoid Scaffolds by a Monodomain Class II Terpene Cyclase

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1345
Thiourea-Stabilized Carboxylic Acids Permit [4+2] Cycloadditions of Acetals and (Bis)homoallylic Alcohols

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1346
Organocatalytic Oxygen Reduction: Dicarbenium Ions as Catalysts

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1347
Organic Photoredox Catalyzed Deoxyfluorination of Electron-Rich Arenes

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1348
A Dual Organocatalytic Approach to Chiral S-Heterocycles

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1349
Radical N-Heterocyclic Carbene Catalysis for the Synthesis of Hindered Alkyl Ketones from Aldehydes

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1350
Chiral Imidazole-Catalyzed Synthesis of Remdesivir through Dynamic Kinetic Resolution

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1351
Purely Organocatalytic C–H Insertion and Cyclopropanation Reactions with α-Diazo Esters

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Chemistry in Medicine and Biology
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1353
A PROTAC for KRAS G12C Degradation FREIER ZUGRIFF

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1354
PEARL-seq: A Workflow for Analyzing Small Molecule–RNA Interactions

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1355
Macropinocytosis is Key to Peptidomimetic Uptake in Cancer Cells

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1356
Natural Products in Drug Discovery

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1357
Copper Sensing by Electrophile Activation

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1358
Introducing Phosphorylation-Inducing Chimeric Small Molecules (PHICS)

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1359
Non-nucleotide cGAMP Mimetics with Powerful Antitumor Activity

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1360
Total Synthetic Lankacidin Antibiotics

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1361
A Mild and General Synthesis of Substituted Anilines

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1362
A Tool to Observe Cellular Apposition

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1363
One, Two, Three – Nucleosides

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1364
Bioluminescence Seeing Red

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1365
The First Contraceptive FREIER ZUGRIFF

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1366
Pumping and Probing for the Optimal Dienophile

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Peptide Chemistry
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1367
Palladium-Catalyzed C(sp³)–H Arylation of Peptides Assisted by Unmodified Asparagine FREIER ZUGRIFF

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1368
Ni-Catalyzed Decarboxylative Borylation toward α-Aminoboronates and Peptide-Boronic Acids

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1369
Synthesis of Peptides Containing α,α-Difluoro-β-amino Acids from α,α-Difluoro Lactams

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1370
Transamination for Synthesis of Unprotected Glycine Derivatives

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1371
Modification of Tryptophan by Using Triarylbismuthines and Copper(II) Acetate

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1372
Photoredox-Catalyzed Synthesis of α-Amino Acid Derivatives

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PDF (80 kb)
1373
Chiral Phosphoric Acid-Catalyzed Synthesis of α-Amino Acid Derivatives

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1374
Cooperative Catalysis for the Synthesis of β-Prolines

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1375
Synthesis of Cyclic Peptides by Palladium-Catalyzed Intramolecular C(sp³)–H Arylation

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1376
Photoinduced α-C(sp³)–H Functionalization of Amino Acids and Peptides

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1377
Dipeptide Synthesis from S-2-Formyl-4-Nitrophenyl Thioesters and Amino Acid Salts FREIER ZUGRIFF

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1378
Decarboxylative Carbonylation of α-Amino Acids

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Flow Chemistry
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1379
Asymmetric C–H Functionalization in Flow by an Immobilized Rhodium Carboxylate Catalyst

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1380
Iodine–Lithium Exchange Reaction of Benzylic Iodides

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1381
Iridium-Photocatalyzed Formation of Tetrahydroquinolines

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