Synfacts

Issue 08 · August 2014

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A101
SYNFORM ISSUE 2014/08 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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0779
Total Synthesis of (–)-Citrinalin B and (–)-Cyclopiamine B

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0780
Total Syntheses of Hyperforin and Papuaforins A–C

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0781
Biomimetic Synthesis of (±)-Dictazole B by Irradiation with Artificial Sunlight FREE ACCESS

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0782
Synthesis of GPR40 Agonist AM-4668

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0783
Synthesis of MK-8742 FREE ACCESS

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0784
Total Synthesis of (±)-Vaticanol A

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0785
Synthesis of (±)-Merochlorin B

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0786
Synthesis of an HDM2 Inhibitor

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0787
Synthesis of (±)-Jiadifenolide

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0788
Synthesis of Vernakalant

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0789
Synthesis of (±)-Lundurine A and B

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Synthesis of Heterocycles
z791
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0791
Pyrrolo- and Pyrazolopiperidines by Stereoselective Organocatalysis

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0792
Synthesis of Benzofuro[2,3-c]pyridines

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0793
Multicomponent Synthesis of Thiazepines

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0794
Synthesis of 3-Substituted Isoxazole Derivatives Using Copper(II) Nitrate

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0795
Synthesis of Dihydropyrroles via Sequential Heck–Suzuki Reaction

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0796
Asymmetric Synthesis of 1,3-Oxathiolan-5-ones

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0797
Synthesis of Polysubstituted Benzofurans from 2-Alkynylphenols

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0798
Three-Component Synthesis of Fully Substituted Pyrazoles

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0799
Pyridoquinazolinones by Palladium-Catalyzed C–H Bond Activation

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0800
Copper-Mediated Synthesis of Fused Cyclopropylpyrrolidines

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0801
Three-Step Synthesis of 3-Phosphonopyrroles via Hydroamination

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0802
Regioselective Synthesis of Linear and Angular Pyridoquinazolones

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0803
Michael Addition–Reductive Lactamization Route to 5-Alkyl-5-aryl-γ-lactams

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0804
Isoquinolines by Manganese-Catalyzed Annulation of Aryl Imines with Alkynes

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0805
Synthesis of Perfluoroalkyl Pyrroles and Thiophenes from Cyclopropanes

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Synthesis of Materials and Unnatural Products
z807
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0807
A Treasure Trove of Tetraphenylenes

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0808
Constructing Novel Polymer Architecture through a 1,4-Rhodium Migration

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0809
Poly(o-arylene)s from [2.2.1]Oxabicyclic Alkenes as Monomers FREE ACCESS

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0810
A Heptagon-Infused Pentacene

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0811
The Right Writhe

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0812
Mild Method for a Furan-Based o-Quinodimethane

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0813
Efficient Transannular Cyclization via Dearomatization

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0814
1,2,4,5-Tetrakis(trimethylsilyl)benzene as a 1,4-Benzdiyne Equivalent

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0815
Cu(I) or Ni(0) = [4+2]: Naphthols from Cycloaddition Catalyzed by Base Metals

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0816
Sulfonyl Compounds From Organozincs and Sulfonyl Halides via Copper(I)

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0817
Two Sides to this Story: All-cis-1,2,4,5-tetrafluoro-3-arylcyclohexanes

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0818
At Last, a Recyclable High-Performance Thermoset

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z819
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0819
Iridium-Catalyzed Asymmetric Dearomatization of Pyridines and Pyrazines FREE ACCESS

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0820
Palladium-Catalyzed Asymmetric Allylic Dearomatization of Pyrroles

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0821
Catalytic Asymmetric Aminations of 3-Bromooxindoles with Indolines

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0822
Rhodium-Catalyzed Asymmetric Ring Expansion of Cyclobutanols

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0823
Asymmetric Hydrogenation of Maleic Acid Diesters by Iridium Catalysis

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0824
Asymmetric Alkynylation of Aldehydes Catalyzed by Ar-BINMOL-Phos/Zn

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0825
Rhodium-Catalyzed Asymmetric Cycloisomerization of 1,6-Enynes

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0826
Formal 1,2-Insertion of Rh(II) Azavinyl Carbenes into Formamides

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0827
Asymmetric Intermolecular Allylic Alkylation Catalyzed by Palladium

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0828
Asymmetric Ring Opening of Oxabenzonorbornadienes with Amines

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0829
Catalytic Activity of New Ruthenium Complexes in the Mukaiyama Aldol Reaction

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0830
Asymmetric Palladium-Catalyzed Amination of Allenyl Phosphates

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0831
Enantioselective C–H Alkylation of Ferrocenes

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0832
Palladium-Catalyzed Asymmetric Hydrogenation of Indoles

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0833
Rhodium-Catalyzed Enantioselective β-Lactone Synthesis via C–H Activation

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0834
Copper-Catalyzed Enantioselective Mannich Reaction of Cyclic Aldimines

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0835
Lewis Acid/Brønsted Base Catalyzed Michael Addition to Thioamides

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0836
A Bidentate Amide for the Silver-Mediated Enantioselective Direct Aldol Reaction

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0837
Rhodium-Catalyzed Asymmetric Addition to Ketimines

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0838
Copper-Catalyzed Asymmetric Intramolecular [3+2] Annulation

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0839
Copper-Catalyzed Enantioselective Silylation of N-Sulfonylimines

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0840
NHC–Copper(I)-Catalyzed Addition of Silicon Nucleophiles to Aldimines

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0841
Chiral α-Hydroxy-β-Keto Esters via Asymmetric Carbonyl-Ene Reactions

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0842
Rhodium-Catalyzed Asymmetric Hydrogenation of Acrylosulfones

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0843
Asymmetric Synthesis of Vicinal Amino Alcohols by Rhodium Catalysis

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0844
Iron(II)-Catalyzed Diastereoselective Intramolecular Aminofluorination

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0845
Synthesis of Chiral Cyclopropylphosphonates by Ru(II)-Catalysis

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0846
Silver-Catalyzed [3+2] Cyclization of α-Imino Esters with Isocyanoacetate FREE ACCESS

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0847
Tertiary Vinylglycols via Palladium-Mediated Asymmetric Decarboxylative Cycloaddition

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0848
Stereoselective Synthesis of Oxo-Heterocycles via Rhenium Catalysis

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Metal-Mediated Synthesis
z849
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0849
Stereoselective Synthesis of syn-Homoallylic Alcohols FREE ACCESS

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0850
Selective Lithiation of Azobenzenes

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0851
Synthesis of Amino Cyclopentadienes

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0852
One-Pot Allylation–Hydrostannation Sequence

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0853
Synthesis of 5-Fluorinated Naphthols

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0854
Tandem Carbannulation of Blaise Reaction Intermediates

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0855
Trimerization of 2-Bromophenylboronic Esters via Metal-Bound Arynes

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0856
Additions of Chloromethyllithium Carbenoid to Cyclic Enones

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0857
Reductive Coupling of Aryl Iodides with CF₃CH₂I in the Presence of Copper

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0858
Cross-Coupling of 2-Azidoarylboron Pinacolate Esters with Vinyl Triflates

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0859
Directed ortho Metalation of Naphthyl-2-carbamates

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0860
Three-Component Couplings of Imines/ Nitriles, Grignard Reagents and THF

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0861
Cooperative Iron/Copper Catalysis: Borylation of Aryl Bromides

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0862
Iron-Catalyzed Cross-Coupling Reactions of Non-Activated Alkyl Halides

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Organo- and Biocatalysis
z863
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0863
Organocatalytic Atroposelective Synthesis of Axially Chiral Biaryls

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0864
Asymmetric Three-Component Strecker Reaction Catalyzed by Disulfonimide

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0865
Adjacent All-Carbon Quaternary Stereocenters via Nazarov Cyclization

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0866
Enzyme Microtuning for the Synthesis of β-Blocker Precursors

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0867
Chemoselective N-Heterocyclic Carbene Catalyzed Cross-Benzoin Reactions

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0868
Chiral Phosphoric Acid Catalyzed Aza-Petasis–Ferrier Rearrangement

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0869
Phase-Transfer-Catalyzed Nucleophilic Arylation of 3-Aryloxindoles

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0870
HYDRA – Towards ppm-Level Asymmetric Organocatalysis

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0871
Organocatalytic Oxidative Annulation of Benzamides with Alkynes

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0872
Imidazolium-Based Organic–Inorganic Silica for Asymmetric Michael Additions

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0873
Activation of Carboxylic Acids by Heterodimer Formation

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0874
Enantioselective Iodolactonization by Cooperative Activation

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0875
Phosphoric Acid Catalyzed Transfer Hydrogenation of Ethyl Ketimines

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Polymer-Supported Synthesis
z877
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0877
Ligand-Controlled Copper-Catalyzed Oxidation of Benzylamines with Oxygen FREE ACCESS

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0878
The Suzuki–Miyaura Coupling with a Polymeric Palladacycle Catalyst

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0879
Alcoholysis and Hydrolysis of Silane Using PPX Nanotube Immobilized Gold

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0880
Oxidative Hydroxylation of Arylboronic Acids Using CuFe₂O₄ NPs

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0881
A Polymer-Supported Copper Complex for Asymmetric Henry Reaction

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0882
Controlled Reduction of Alkynes with CO/H₂O Using Au/HSA-TiO₂

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0883
Asymmetric Allylation of Ketones Using a Titanium–BINOLate Complex

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0884
Borylation, Silylation, and Dehydrogenation Using Bipyridyl-Containing MOFs

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0885
Hydrogenation of Amino Acids with Rh–MoO_x/SiO₂

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0886
Imidazolium Salt Stabilized Palladium Nanoparticles for Cross-Couplings

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0887
The Suzuki–Miyaura Cross-Coupling of Heteroaromatics Using Pd⁰-AmP-MCF

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0888
Solid-Phase Synthesis of Anagrelide Sulfonyl Analogues

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0889
Enantioselective Aldol Reactions Using a PS-Supported Threonine Derivative

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0890
Reduction of Nitrobenzenes Using Dendrimer-Encapsulated [Rh₅(CO)₁₅]^–

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0891
Photocatalytic Aerobic Oxidation of Amines to Imines

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